BR112014007130A2 - partículas de polímero e método para produção - Google Patents
partículas de polímero e método para produção Download PDFInfo
- Publication number
- BR112014007130A2 BR112014007130A2 BR112014007130-6A BR112014007130A BR112014007130A2 BR 112014007130 A2 BR112014007130 A2 BR 112014007130A2 BR 112014007130 A BR112014007130 A BR 112014007130A BR 112014007130 A2 BR112014007130 A2 BR 112014007130A2
- Authority
- BR
- Brazil
- Prior art keywords
- polyamide resin
- polymer
- polyamide
- acid
- particles
- Prior art date
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- 239000002245 particle Substances 0.000 title claims abstract description 275
- 229920000642 polymer Polymers 0.000 title claims abstract description 236
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 46
- 229920006122 polyamide resin Polymers 0.000 claims abstract description 139
- 239000002904 solvent Substances 0.000 claims abstract description 96
- 229920006152 PA1010 Polymers 0.000 claims abstract description 75
- 239000004952 Polyamide Substances 0.000 claims abstract description 71
- 229920002647 polyamide Polymers 0.000 claims abstract description 71
- 238000000034 method Methods 0.000 claims abstract description 66
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- 238000005191 phase separation Methods 0.000 claims abstract description 23
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- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 53
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- 125000003158 alcohol group Chemical group 0.000 claims description 26
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims description 21
- 239000001632 sodium acetate Substances 0.000 claims description 21
- 235000017281 sodium acetate Nutrition 0.000 claims description 21
- 239000002253 acid Substances 0.000 claims description 20
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 17
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims description 15
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 15
- 238000001228 spectrum Methods 0.000 claims description 15
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 claims description 14
- 150000007513 acids Chemical class 0.000 claims description 12
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- 229920002125 Sokalan® Polymers 0.000 claims description 11
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- 238000012360 testing method Methods 0.000 claims description 11
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 10
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 claims description 10
- 238000009835 boiling Methods 0.000 claims description 9
- 238000001816 cooling Methods 0.000 claims description 9
- 229910052757 nitrogen Inorganic materials 0.000 claims description 9
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 9
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- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 7
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- 238000000354 decomposition reaction Methods 0.000 claims description 6
- 229920013821 hydroxy alkyl cellulose Polymers 0.000 claims description 6
- 229920001515 polyalkylene glycol Polymers 0.000 claims description 6
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- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 6
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 6
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 5
- CYSGHNMQYZDMIA-UHFFFAOYSA-N 1,3-Dimethyl-2-imidazolidinon Chemical compound CN1CCN(C)C1=O CYSGHNMQYZDMIA-UHFFFAOYSA-N 0.000 claims description 5
- FXHOOIRPVKKKFG-UHFFFAOYSA-N N,N-Dimethylacetamide Chemical compound CN(C)C(C)=O FXHOOIRPVKKKFG-UHFFFAOYSA-N 0.000 claims description 5
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 5
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 5
- 238000010494 dissociation reaction Methods 0.000 claims description 5
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- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 5
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 5
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- 238000000333 X-ray scattering Methods 0.000 claims description 4
- 125000003368 amide group Chemical group 0.000 claims description 4
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 4
- 125000001033 ether group Chemical group 0.000 claims description 4
- 238000002798 spectrophotometry method Methods 0.000 claims description 4
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- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 16
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- 230000000052 comparative effect Effects 0.000 description 12
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- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 10
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- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 9
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- 238000002441 X-ray diffraction Methods 0.000 description 8
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 8
- 239000003963 antioxidant agent Substances 0.000 description 8
- 235000006708 antioxidants Nutrition 0.000 description 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 8
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 8
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 8
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- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 7
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- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
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Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/JP2011/071954 WO2012043509A1 (ja) | 2010-09-28 | 2011-09-27 | ポリマー微粒子およびその製造方法 |
| JPPCT/JP2011/071954 | 2011-09-27 | ||
| JP2012-067571 | 2012-03-23 | ||
| JP2012067571A JP5541586B2 (ja) | 2011-09-27 | 2012-03-23 | ポリアミド１０１０樹脂粒子およびその製造方法 |
| PCT/JP2012/067693 WO2013046860A1 (ja) | 2011-09-27 | 2012-07-11 | ポリアミド１０１０樹脂粒子およびその製造方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR112014007130A2 true BR112014007130A2 (pt) | 2020-10-27 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR112014007130-6A BR112014007130A2 (pt) | 2011-09-27 | 2012-07-11 | partículas de polímero e método para produção |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US9617395B2 (enExample) |
| EP (1) | EP2743290A4 (enExample) |
| JP (1) | JP5541586B2 (enExample) |
| KR (1) | KR20140080478A (enExample) |
| CN (1) | CN103748143B (enExample) |
| AU (1) | AU2012313453A1 (enExample) |
| BR (1) | BR112014007130A2 (enExample) |
| TW (1) | TWI527846B (enExample) |
| WO (1) | WO2013046860A1 (enExample) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9493611B2 (en) | 2012-09-14 | 2016-11-15 | Toray Industries, Inc. | Polyamide resin composition and molded product |
| KR20160014575A (ko) * | 2013-05-31 | 2016-02-11 | 도레이 카부시키가이샤 | 에틸렌-비닐 알코올계 공중합체 미립자 및 그것을 함유하는 분산액과 수지 조성물 및 그 미립자의 제조 방법 |
| JP6291222B2 (ja) * | 2013-11-19 | 2018-03-14 | Ｊｘｔｇエネルギー株式会社 | プリプレグ、繊維強化複合材料及び粒子含有樹脂組成物 |
| JP6291221B2 (ja) * | 2013-11-19 | 2018-03-14 | Ｊｘｔｇエネルギー株式会社 | プリプレグ、繊維強化複合材料及び粒子含有樹脂組成物 |
| EP3153541A4 (en) * | 2014-06-09 | 2018-01-10 | Toray Industries, Inc. | Method for producing polymer microparticles |
| CN104149219B (zh) * | 2014-07-31 | 2017-04-26 | 中国科学院重庆绿色智能技术研究院 | 一体化粉体球化及分级方法 |
| WO2016016019A1 (fr) * | 2014-08-01 | 2016-02-04 | Cartier International Ag | Composant horloger avec une surface comportant de la fibroïne de soie |
| CN105440663B (zh) * | 2014-08-07 | 2018-08-24 | 中国科学院理化技术研究所 | 一种选择性激光烧结用尼龙微粉的制备方法 |
| CN104262646B (zh) * | 2014-09-12 | 2017-07-21 | 中国科学院化学研究所 | 形貌可控的长碳链聚酰胺粉末基体及形貌可控的高导电复合粉末材料 |
| CN107109036B (zh) | 2014-10-29 | 2019-10-25 | 住友精化株式会社 | 聚酯系弹性体的水性分散体和其制造方法 |
| CN106674553B (zh) * | 2015-11-11 | 2020-02-11 | 中国科学院理化技术研究所 | 一种聚酰胺多孔微球及其制备方法 |
| CN106751767B (zh) * | 2015-11-24 | 2019-09-24 | 中国科学院理化技术研究所 | 一种选择性激光烧结用尼龙合金复合微粉及其制备方法 |
| CN108699255A (zh) | 2016-05-10 | 2018-10-23 | 株式会社吴羽 | 聚酰胺微粒及其制造方法以及聚酰胺微粒组合物 |
| EP3489281B1 (en) | 2016-07-22 | 2023-04-19 | Sekisui Plastics Co., Ltd. | Generally spherical resin particles formed of thermoplastic resin, method for producing same and use of same |
| CN108720547B (zh) * | 2017-04-25 | 2024-02-13 | 佛山市顺德区美的电热电器制造有限公司 | 不粘涂层及其制备方法以及锅具和煮食设备 |
| EP3808795A4 (en) * | 2018-06-14 | 2022-03-09 | Nippon Soda Co., Ltd. | Method for producing polyamide 4 particles |
| CN109171647B (zh) * | 2018-08-14 | 2021-06-11 | 上海常仁信息科技有限公司 | 能够皮肤检测的健康机器人 |
| JP7055784B2 (ja) * | 2018-12-13 | 2022-04-18 | キヤノン化成株式会社 | 霧化塗布用表面反射防止塗料および表面反射防止塗膜 |
| EP4108710A4 (en) * | 2020-02-21 | 2023-12-06 | Toray Industries, Inc. | FIBER-REINFORCED COMPOSITE MOLDED ARTICLE AND ASSOCIATED MOLDING METHOD |
| CN113337105B (zh) * | 2020-03-02 | 2022-09-23 | 中国科学院化学研究所 | 一种聚合物粉体及其制备方法 |
| CN113354942B (zh) * | 2020-03-02 | 2022-10-18 | 中国科学院化学研究所 | 一种聚合物粉体及其制备方法 |
| US11643503B2 (en) * | 2020-07-10 | 2023-05-09 | Xerox Corporation | Highly spherical polyamide microparticles and synthesis methods related thereto |
| CN112300415A (zh) * | 2020-11-19 | 2021-02-02 | 广东聚石科技研究有限公司 | 一种球形尼龙粉末及其制备方法和应用 |
| CN116490543B (zh) * | 2020-11-30 | 2025-03-28 | 东丽株式会社 | 聚酰胺微粒及其制造方法 |
| WO2023118015A1 (en) * | 2021-12-21 | 2023-06-29 | Basf Se | Environmental attributes for care composition ingredients |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4081430A (en) * | 1975-10-20 | 1978-03-28 | Mitsubishi Rayon Co., Ltd. | Aromatic polyamide crystalline complex and the method for producing the same |
| DE102004020453A1 (de) * | 2004-04-27 | 2005-11-24 | Degussa Ag | Polymerpulver mit Polyamid, Verwendung in einem formgebenden Verfahren und Formkörper, hergestellt aus diesem Polymerpulver |
| JP2006328208A (ja) * | 2005-05-26 | 2006-12-07 | Daicel Degussa Ltd | 真球状熱可塑性樹脂微粒子の製造法 |
| DE102005053071A1 (de) * | 2005-11-04 | 2007-05-16 | Degussa | Verfahren zur Herstellung von ultrafeinen Pulvern auf Basis Polymaiden, ultrafeinen Polyamidpulver sowie deren Verwendung |
| DE102006015791A1 (de) | 2006-04-01 | 2007-10-04 | Degussa Gmbh | Polymerpulver, Verfahren zur Herstellung und Verwendung eines solchen Pulvers und Formkörper daraus |
| WO2009142231A1 (ja) * | 2008-05-21 | 2009-11-26 | 東レ株式会社 | ポリマー微粒子の製造方法 |
| JP5306847B2 (ja) * | 2009-02-16 | 2013-10-02 | ユニチカ株式会社 | 環境配慮型熱可塑性樹脂組成物 |
| EP2404955A4 (en) * | 2009-03-05 | 2013-07-03 | Ube Industries | POLYAMIDE PARTICLES AND MANUFACTURING METHOD THEREFOR |
| JP2011094128A (ja) * | 2009-09-30 | 2011-05-12 | Toray Ind Inc | ポリアミド微粒子の製造方法 |
| EP2374835B1 (en) * | 2010-04-07 | 2013-12-25 | Evonik Degussa GmbH | Polyamide 1010 powder and its use in personal care products |
| JP5365573B2 (ja) | 2010-04-14 | 2013-12-11 | 宇部興産株式会社 | 吸着材 |
| JP5641044B2 (ja) | 2010-04-20 | 2014-12-17 | 宇部興産株式会社 | ポリアミド微粒子及びその製造方法並びにそれを用いた光学フィルム及び液晶表示装置 |
| JP5403065B2 (ja) * | 2010-09-28 | 2014-01-29 | 東レ株式会社 | ポリマー微粒子の製造方法 |
-
2012
- 2012-03-23 JP JP2012067571A patent/JP5541586B2/ja not_active Expired - Fee Related
- 2012-07-11 EP EP12837041.8A patent/EP2743290A4/en not_active Withdrawn
- 2012-07-11 WO PCT/JP2012/067693 patent/WO2013046860A1/ja not_active Ceased
- 2012-07-11 US US14/345,448 patent/US9617395B2/en not_active Expired - Fee Related
- 2012-07-11 CN CN201280041329.1A patent/CN103748143B/zh not_active Expired - Fee Related
- 2012-07-11 BR BR112014007130-6A patent/BR112014007130A2/pt not_active IP Right Cessation
- 2012-07-11 KR KR1020147003389A patent/KR20140080478A/ko not_active Withdrawn
- 2012-07-11 AU AU2012313453A patent/AU2012313453A1/en not_active Abandoned
- 2012-09-26 TW TW101135208A patent/TWI527846B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| TW201323489A (zh) | 2013-06-16 |
| US9617395B2 (en) | 2017-04-11 |
| AU2012313453A1 (en) | 2014-05-15 |
| TWI527846B (zh) | 2016-04-01 |
| WO2013046860A1 (ja) | 2013-04-04 |
| EP2743290A1 (en) | 2014-06-18 |
| JP5541586B2 (ja) | 2014-07-09 |
| US20140349113A1 (en) | 2014-11-27 |
| JP2013072086A (ja) | 2013-04-22 |
| EP2743290A4 (en) | 2015-03-25 |
| CN103748143A (zh) | 2014-04-23 |
| CN103748143B (zh) | 2016-06-29 |
| KR20140080478A (ko) | 2014-06-30 |
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