BR0109300A - Processo para a fabricação de um produto de zeólito, produto de zeólito, e, composição detergente - Google Patents

Processo para a fabricação de um produto de zeólito, produto de zeólito, e, composição detergente

Info

Publication number
BR0109300A
BR0109300A BR0109300-2A BR0109300A BR0109300A BR 0109300 A BR0109300 A BR 0109300A BR 0109300 A BR0109300 A BR 0109300A BR 0109300 A BR0109300 A BR 0109300A
Authority
BR
Brazil
Prior art keywords
zeolite
alumina
gel
mixture
total batch
Prior art date
Application number
BR0109300-2A
Other languages
English (en)
Inventor
Daniel J Micco
Richard J Hinchey
Original Assignee
Pq Holding Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pq Holding Inc filed Critical Pq Holding Inc
Publication of BR0109300A publication Critical patent/BR0109300A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/14—Type A
    • C01B39/16—Type A from aqueous solutions of an alkali metal aluminate and an alkali metal silicate excluding any other source of alumina or silica but seeds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/023—Preparation of physical mixtures or intergrowth products of zeolites chosen from group C01B39/04 or two or more of groups C01B39/14 - C01B39/48
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/14—Type A
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/128—Aluminium silicates, e.g. zeolites
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00—Chemistry of inorganic compounds
    • Y10S423/21—Faujasite, e.g. X, Y, CZS-3, ECR-4, Z-14HS, VHP-R
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00—Chemistry of inorganic compounds
    • Y10S423/24—LTA, e.g. A, alpha, ZK-4, ZK-21, ZK-22

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Detergent Compositions (AREA)

Abstract

"PROCESSO PARA A FABRICAçãO DE UM PRODUTO DE ZEóLITO, PRODUTO DE ZEóLITO, E, COMPOSIçãO DETERGENTE". Um zeólito A ou uma mistura de A/X tendo um LCC > 70 g de líquido/100 g de zeólito (hidratado) e um CER de água fria > 200 mg de CaCO~ 3~/g de zeólito anidro (hidratado). O produto zeólito pode ter um tamanho de cristal de 0,1 a 0,7 mícron, uma densidade em massa de 0,19 a 0,37 g/ml e um tamanho de partícula médio de 1 a 5 mícrons. Um processo para produzir o zeólito A ou misturas de A/X é também reivindicado incluindo a mistura de uma solução de silicato de sódio, uma solução de aluminato de sódio, e um gel iniciador de aluminossilicato amorfo em um vaso de mistura para criar um gel de síntese de aluminossilicato, e cristalizando-se o gel de síntese de, aluminossilicato para formar cristais de zeólito. A solução de aluminato de sódio pode ser adicionada gradualmente pelo menos à solução de silicato de sódio em uma taxa de cerca de 1 a 5% da batelada total de alumina por minuto, e/ou um percentual da batelada total de alumina pode ser adicionado como pó de triidrato de alumina (ATH). A quantidade da batelada total de alumina adicionada como uma fonte não dissolvida de alumina solúvel é a presença ou ausência do gel iniciador ou "semente" determina se o produto zeólito resultante é uma mistura de A/X ou apenas o zeólito A. Um processo para aumentar o rendimento de uma mistura de síntese é igualmente reivindicado, compreendendo o fornecimento de alumina não dissolvida em substancial excesso de exigências estequiométricas em uma etapa de cristalização primária, produzindo uma lama de zeólito A cristalino em um líquido mãe enriquecido com alumina, e então adicionando-se silicato solúvel para iniciar um segundo estágio de cristalização muito rápido. Os detergentes contendo os zeólitos desta invenção são reivindicados.
BR0109300-2A 2000-03-17 2001-03-15 Processo para a fabricação de um produto de zeólito, produto de zeólito, e, composição detergente BR0109300A (pt)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US19018500P 2000-03-17 2000-03-17
US21307600P 2000-06-21 2000-06-21
US24663200P 2000-11-08 2000-11-08
PCT/US2001/008107 WO2001070629A2 (en) 2000-03-17 2001-03-15 Process for manufacture of zeolites and zeolite mixtures having enhanced cation exchange properties, products produced thereby, and detergent compositions formulated therewith

Publications (1)

Publication Number Publication Date
BR0109300A true BR0109300A (pt) 2002-12-24

Family

ID=27392703

Family Applications (1)

Application Number Title Priority Date Filing Date
BR0109300-2A BR0109300A (pt) 2000-03-17 2001-03-15 Processo para a fabricação de um produto de zeólito, produto de zeólito, e, composição detergente

Country Status (13)

Country Link
US (2) US6641796B2 (pt)
EP (1) EP1265814B1 (pt)
JP (1) JP4023779B2 (pt)
KR (1) KR100488611B1 (pt)
CN (1) CN1223400C (pt)
AT (1) ATE266603T1 (pt)
AU (1) AU2001243638A1 (pt)
BR (1) BR0109300A (pt)
CA (1) CA2402679C (pt)
DE (1) DE60103260T2 (pt)
ES (1) ES2221891T3 (pt)
HK (1) HK1051993A1 (pt)
WO (1) WO2001070629A2 (pt)

Families Citing this family (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2380231A (en) * 2001-09-26 2003-04-02 Reckitt Benckiser Nv Corrosion inhibitors for tin plated aerosol canisters
US6667023B2 (en) * 2002-03-01 2003-12-23 Akzo Nobel N.V. Preparation of MFI type crystalline zeolitic aluminosilicate
US7014837B2 (en) * 2003-09-16 2006-03-21 E. I. Dupont De Nemours And Company Process for the production of nan-sized zeolite A
DE202004003708U1 (de) 2004-03-10 2005-07-28 Ramsauer, Dieter Verstelleinrichtung für Dreh- und Klappriegel
US7442365B1 (en) * 2004-06-14 2008-10-28 Uop Llc Process for preparing molecular sieve beads
US20060140853A1 (en) 2004-12-27 2006-06-29 Council Of Scientific And Industrial Research Process for preparing detergent builder zeolite-a from kimberlite tailings
DE102005013051A1 (de) * 2005-03-18 2006-09-21 BSH Bosch und Siemens Hausgeräte GmbH Kondensations-Wäschetrockner
US20090087492A1 (en) * 2006-03-14 2009-04-02 Merck & Co., Inc. Processes and Apparatuses for the Production of Crystalline Organic Microparticle Compositions by Micro-Milling and Crystallization on Micro-Seed and Their Use
US8338329B2 (en) 2009-11-13 2012-12-25 Zeotech Corporation Fluid filtration medium
US9174197B2 (en) 2009-11-13 2015-11-03 Zeotech Corporation Fluid filtration medium
US9228785B2 (en) 2010-05-04 2016-01-05 Alexander Poltorak Fractal heat transfer device
ME03294B (me) * 2011-02-11 2019-07-20 Zs Pharma Inc Primena cirkonijum silikata za tretman hiperkalemije
RU2452688C1 (ru) * 2011-02-22 2012-06-10 Учреждение Российской академии наук Институт геологии и минералогии им. В.С. Соболева Сибирского отделения РАН (Институт геологии и минералогии СО РАН, ИГМ СО РАН) СПОСОБ ПОЛУЧЕНИЯ ЦЕОЛИТА NaА ИЛИ NaХ (ВАРИАНТЫ)
US20130005564A1 (en) * 2011-06-30 2013-01-03 Uop Llc Synthesis of crystalline long-ranged ordered materials from preformed amorphous solids
CN102557067B (zh) * 2011-12-19 2013-11-20 吉林大学 在纯钠硅铝酸盐体系中制备低硅Na-A/X共结晶沸石的方法
US9458023B2 (en) * 2012-09-20 2016-10-04 Pq Corporation Use of aqueous alkali aluminosilicate for profile modification, water control and stabilization
CN102992342A (zh) * 2012-12-05 2013-03-27 中国日用化学工业研究院 一种用于洗涤剂助剂的复合沸石的制备方法
CN103657436B (zh) * 2013-12-31 2016-06-01 南京工业大学 一种高强度的中空纤维分子筛膜及其制备方法
CN104649291B (zh) * 2014-11-21 2017-01-18 中国铝业股份有限公司 一种沸石制备方法
US10502700B2 (en) * 2016-07-12 2019-12-10 United States Gypsum Company Methods for analyzing respirable particles in bulk materials
US10830545B2 (en) 2016-07-12 2020-11-10 Fractal Heatsink Technologies, LLC System and method for maintaining efficiency of a heat sink
CN106276947B (zh) * 2016-08-16 2018-07-31 中国铝业股份有限公司 A型及x型混合晶体沸石、其制备方法、制备装置和用途
CN107999047B (zh) * 2016-10-28 2020-05-19 中国石油化工股份有限公司 含硼水合氧化铝组合物和成型体及制备方法和应用以及催化剂及制备方法
CN109790040B (zh) * 2017-07-14 2021-09-21 北京大学深圳研究生院 一种层级结构多级孔沸石及其制备方法
US11014821B2 (en) 2018-07-09 2021-05-25 Zeolyfe, LLC Methods for preparation of CHA Zeolite at ambient pressure
JP2022074143A (ja) * 2020-11-02 2022-05-17 三菱ケミカル株式会社 ゼオライト及びゼオライトの製造方法、並びに組成物
CN112592720A (zh) * 2020-12-15 2021-04-02 中国矿业大学 一种以粉煤灰为原料制备复合型固化剂的方法及其在修复矿区土壤中的应用
CN112850739B (zh) * 2021-03-12 2023-07-25 许昌学院 一种大晶粒ltj沸石及其制备方法
CN113371730A (zh) * 2021-06-02 2021-09-10 昊华化工科技集团股份有限公司 一种改性钙低硅沸石分子筛及其制备方法
CN113943008B (zh) * 2021-12-01 2023-06-23 南宁师范大学 Zsm-5分子筛的制备方法
CN114644343B (zh) * 2022-04-13 2023-02-28 贵州大学 一种电解锰渣制备纯相x型沸石的方法
CN116119679B (zh) * 2023-01-17 2024-08-27 西南科技大学 一种高纯4a沸石及其室温常压合成方法

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3574538A (en) 1968-10-17 1971-04-13 Grace W R & Co Process for preparing high silica faujasite
US3808326A (en) 1971-03-19 1974-04-30 Grace W R & Co Preparation of zeolites
US4605509A (en) 1973-05-11 1986-08-12 The Procter & Gamble Company Detergent compositions containing sodium aluminosilicate builders
US4274975A (en) 1974-03-11 1981-06-23 The Procter & Gamble Company Detergent composition
US4102977A (en) * 1975-11-18 1978-07-25 Mizusawa Kagaku Kogyo Kabushiki Kaisha Process for the preparation of alkali aluminosilicate detergent builder
DE2651485A1 (de) * 1976-11-11 1978-05-24 Degussa Kristallines zeolithpulver des typs a i
FR2376073A1 (fr) * 1976-12-30 1978-07-28 Rhone Poulenc Ind Nouveau silico-aluminate alcalin cristallin de type 4 a ainsi que son procede d'obtention et application
FR2392932A1 (fr) * 1977-06-03 1978-12-29 Rhone Poulenc Ind Procede de fabrication d'un silico-aluminate alcalin cristallin, produit obtenu et application
US4173622A (en) * 1978-01-03 1979-11-06 Fmc Corporation Zeolite A crystals of uniformly small particle size and the manufacture thereof
US4264562A (en) * 1978-12-20 1981-04-28 J. M. Huber Corporation Method of producing zeolite Y
US4235856A (en) * 1978-12-20 1980-11-25 J. M. Huber Corporation Method of producing a zeolite of controlled particle size
US4340573A (en) 1979-01-03 1982-07-20 W. R. Grace & Co. Preparation of zeolites
NZ208048A (en) * 1983-05-26 1986-10-08 Mobil Oil Corp Method for synthesising zeolites,incorporating alumina source of limited solubility
US4752341A (en) * 1986-08-11 1988-06-21 Pq Corporation Pigment system for paper
DE59308266D1 (de) 1992-05-13 1998-04-23 Ciba Geigy Ag Stabilisierte chlorhaltige Polymerzusammensetzungen
DE4309656A1 (de) * 1993-03-25 1994-09-29 Henkel Kgaa Verfahren zur Herstellung von feinstteiligen zeolithischen Alkalimetallaluminiumsilicaten
US5366720A (en) 1993-12-23 1994-11-22 Uop Process for preparing low silica forms of zeolites having the faujasite type structure
IT1284078B1 (it) 1996-06-27 1998-05-08 Condea Augusta Spa Materiale cristallino microporoso, procedimento per la preparazione e uso in composizioni detergenti
US5948383A (en) 1997-03-26 1999-09-07 Engelhard Corporation Hybrid zeolite-silica compositions
JP2002535444A (ja) 1999-01-21 2002-10-22 ザ、プロクター、エンド、ギャンブル、カンパニー ハイブリッドゼオライトビルダーを含む改良洗剤組成物
US6096820A (en) * 1999-07-29 2000-08-01 Pq Corporation Aluminosilicate stabilized halogenated polymers
US6451283B1 (en) * 2000-03-23 2002-09-17 Engelhard Corporation Macroscopic aggregates of microcrystalline zeolites
US6416732B1 (en) * 2000-03-23 2002-07-09 Engelhard Corporation Method of forming aluminosilicate zeolites
US6387873B1 (en) * 2000-04-05 2002-05-14 The Procter & Gamble Company Detergent composition with improved calcium sequestration capacity
EP1345852B1 (en) * 2000-12-28 2006-08-30 Kao Corporation Fine zeolite particle

Also Published As

Publication number Publication date
WO2001070629B1 (en) 2002-02-07
EP1265814A2 (en) 2002-12-18
KR100488611B1 (ko) 2005-05-11
US6641796B2 (en) 2003-11-04
EP1265814B1 (en) 2004-05-12
ATE266603T1 (de) 2004-05-15
WO2001070629A3 (en) 2001-12-06
JP4023779B2 (ja) 2007-12-19
DE60103260D1 (de) 2004-06-17
CA2402679A1 (en) 2001-09-27
KR20030008218A (ko) 2003-01-24
WO2001070629A2 (en) 2001-09-27
ES2221891T3 (es) 2005-01-16
US20030050219A1 (en) 2003-03-13
AU2001243638A1 (en) 2001-10-03
CN1420845A (zh) 2003-05-28
HK1051993A1 (en) 2003-08-29
US20010053741A1 (en) 2001-12-20
DE60103260T2 (de) 2005-05-19
CA2402679C (en) 2007-12-04
JP2003528022A (ja) 2003-09-24
CN1223400C (zh) 2005-10-19

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Legal Events

Date Code Title Description
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B11B Dismissal acc. art. 36, par 1 of ipl - no reply within 90 days to fullfil the necessary requirements