AU2012340368B2 - Mesoporous titanium dioxide nanoparticles and process for their production - Google Patents

Mesoporous titanium dioxide nanoparticles and process for their production Download PDF

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Publication number
AU2012340368B2
AU2012340368B2 AU2012340368A AU2012340368A AU2012340368B2 AU 2012340368 B2 AU2012340368 B2 AU 2012340368B2 AU 2012340368 A AU2012340368 A AU 2012340368A AU 2012340368 A AU2012340368 A AU 2012340368A AU 2012340368 B2 AU2012340368 B2 AU 2012340368B2
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temperature
aqueous solution
hours
titanium
range
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AU2012340368A1 (en
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Guoyi Fu
Mark Watson
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Tronox LLC
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Tronox LLC
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C01G23/0536—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts
    • C01G23/0538—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts in the presence of seeds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B1/00—Nanostructures formed by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
    • B82B3/00—Manufacture or treatment of nanostructures by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
    • B82B3/0009—Forming specific nanostructures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C01G23/0536—Producing by wet processes, e.g. hydrolysing titanium salts by hydrolysing chloride-containing salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/08—Drying; Calcining ; After treatment of titanium oxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/60—Compounds characterised by their crystallite size
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C01P2004/34—Spheres hollow
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/53—Particles with a specific particle size distribution bimodal size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/14—Pore volume
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C01P2006/17—Pore diameter distribution
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Nanotechnology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • General Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicinal Preparation (AREA)
AU2012340368A 2011-11-16 2012-11-15 Mesoporous titanium dioxide nanoparticles and process for their production Ceased AU2012340368B2 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US13/297,869 2011-11-16
US13/297,869 US8900705B2 (en) 2011-11-16 2011-11-16 Mesoporous titanium dioxide nanoparticles exhibiting bimodal pore size distributions and process for their production
PCT/US2012/065317 WO2013074812A1 (en) 2011-11-16 2012-11-15 Mesoporous titanium dioxide nanoparticles and process for their production

Publications (2)

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AU2012340368A1 AU2012340368A1 (en) 2014-05-29
AU2012340368B2 true AU2012340368B2 (en) 2016-01-07

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AU2012340368A Ceased AU2012340368B2 (en) 2011-11-16 2012-11-15 Mesoporous titanium dioxide nanoparticles and process for their production

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US (2) US8900705B2 (enExample)
EP (1) EP2780287B1 (enExample)
JP (1) JP6290786B2 (enExample)
KR (2) KR102072039B1 (enExample)
CN (1) CN103998379B (enExample)
AU (1) AU2012340368B2 (enExample)
BR (1) BR112014011852B1 (enExample)
DK (1) DK2780287T3 (enExample)
ES (1) ES2784157T3 (enExample)
IN (1) IN2014DN04773A (enExample)
PL (1) PL2780287T3 (enExample)
RU (1) RU2615402C2 (enExample)
SI (1) SI2780287T1 (enExample)
TW (1) TWI504567B (enExample)
UA (1) UA115134C2 (enExample)
WO (1) WO2013074812A1 (enExample)
ZA (1) ZA201403561B (enExample)

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WO2014042238A1 (ja) 2012-09-14 2014-03-20 田辺三菱製薬株式会社 スルホンアミド化合物
CN103771511B (zh) * 2014-02-20 2015-04-29 安徽工业大学 一种锐钛矿二氧化钛纳米晶溶胶的制备方法
US11223042B2 (en) 2014-03-31 2022-01-11 Tronox Llc Lithium-intercalated titanium dioxide, lithium titanate particles made therefrom, and related methods
EP3250511B1 (en) 2015-01-28 2022-07-06 Brenta S.r.l. Totally-mesoporous zirconia nanoparticles, use and method for producing thereof
EP3262193A2 (en) 2015-02-26 2018-01-03 The Broad Institute Inc. T cell balance gene expression, compositions of matters and methods of use thereof
SG11201706996RA (en) * 2015-03-18 2017-09-28 Phinergy Ltd Metal oxide particles and method of producing thereof
DE102016110374A1 (de) * 2016-06-06 2017-12-07 Huntsman P&A Germany Gmbh Titandioxid-Sol, Verfahren zu dessen Herstellung und daraus gewonnene Produkte
CN107792878B (zh) * 2017-10-26 2019-09-13 福州大学 一种分等级结构二氧化钛（b）的制备方法及其在锂离子电池中的应用
CN108097181B (zh) * 2017-12-19 2020-05-19 东北大学 一种制备氧化铟壳结构的方法及产品
WO2020170917A1 (ja) * 2019-02-19 2020-08-27 昭和電工株式会社 酸化チタン

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Also Published As

Publication number Publication date
RU2615402C2 (ru) 2017-04-04
EP2780287A1 (en) 2014-09-24
KR102072039B1 (ko) 2020-01-31
EP2780287B1 (en) 2020-02-12
US20130122298A1 (en) 2013-05-16
DK2780287T3 (da) 2020-03-09
PL2780287T3 (pl) 2020-07-27
BR112014011852A2 (pt) 2017-05-02
UA115134C2 (uk) 2017-09-25
KR102190185B1 (ko) 2020-12-11
EP2780287A4 (en) 2015-07-08
RU2014123687A (ru) 2015-12-27
US8900705B2 (en) 2014-12-02
AU2012340368A1 (en) 2014-05-29
ES2784157T3 (es) 2020-09-22
WO2013074812A1 (en) 2013-05-23
TWI504567B (zh) 2015-10-21
ZA201403561B (en) 2016-02-24
BR112014011852B1 (pt) 2021-06-29
TW201328980A (zh) 2013-07-16
JP2014533650A (ja) 2014-12-15
CN103998379B (zh) 2016-08-24
IN2014DN04773A (enExample) 2015-05-15
JP6290786B2 (ja) 2018-03-07
CN103998379A (zh) 2014-08-20
US9260318B2 (en) 2016-02-16
KR20200015640A (ko) 2020-02-12
SI2780287T1 (sl) 2020-08-31
US20150057151A1 (en) 2015-02-26
KR20130054177A (ko) 2013-05-24

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