AR044616A1 - Proceso de extraccion para la remocion de impurezas de solucion madre en la sintesis de acido carboxilico - Google Patents

Proceso de extraccion para la remocion de impurezas de solucion madre en la sintesis de acido carboxilico

Info

Publication number
AR044616A1
AR044616A1 ARP040101945A ARP040101945A AR044616A1 AR 044616 A1 AR044616 A1 AR 044616A1 AR P040101945 A ARP040101945 A AR P040101945A AR P040101945 A ARP040101945 A AR P040101945A AR 044616 A1 AR044616 A1 AR 044616A1
Authority
AR
Argentina
Prior art keywords
stream
solvent
stock solution
zone
aqueous
Prior art date
Application number
ARP040101945A
Other languages
English (en)
Original Assignee
Eastman Chem Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eastman Chem Co filed Critical Eastman Chem Co
Publication of AR044616A1 publication Critical patent/AR044616A1/es

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00Regeneration or reactivation of catalysts, in general
    • B01J38/04Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/06Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst using steam
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00Regeneration or reactivation of catalysts, in general
    • B01J38/04Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S423/00Chemistry of inorganic compounds
    • Y10S423/09Reaction techniques
    • Y10S423/14Ion exchange; chelation or liquid/liquid ion extraction

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Catalysts (AREA)

Abstract

Reivindicación 1: Un proceso para recuperar un catalizador de metal de una solución madre, dicho proceso comprende los siguientes pasos: a) evaporar dicha solución madre que comprende un ácido carboxílico, dicho catalizador de metal, impurezas, agua y un disolvente en una primera zona de evaporación para producir una corriente de vapor y una corriente de solución madre concentrada; b) evaporar dicha corriente de solución madre concentrada en una segunda zona de evaporación para formar una corriente rica en disolvente y una corriente de solución madre superconcentrada; c) separar impurezas orgánicas con una solución de agua-disolvente de dicha corriente de solución madre superconcentrada en una zona de separación de sólido-líquido para formar una corriente acuosa y una segunda corriente acuosa; d) mezclar en una zona de mezclado agua y opcionalmente un disolvente de extracción con dicha corriente acuosa y dicha segunda corriente acuosa para formar una mezcla acuosa; e) agregar un disolvente de extracción a dicha mezcla acuosa en una zona de extracción para formar una corriente de extracto y una corriente de refinado; y f) opcionalmente separar dicha corriente de extracto en una zona de separación para formar una corriente de impurezas orgánicas de alto punto de ebullición y una corriente de disolvente de extracción recuperado.
ARP040101945A 2003-06-05 2004-06-04 Proceso de extraccion para la remocion de impurezas de solucion madre en la sintesis de acido carboxilico AR044616A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US10/455,016 US7410632B2 (en) 2003-06-05 2003-06-05 Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid

Publications (1)

Publication Number Publication Date
AR044616A1 true AR044616A1 (es) 2005-09-21

Family

ID=33159561

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP040101945A AR044616A1 (es) 2003-06-05 2004-06-04 Proceso de extraccion para la remocion de impurezas de solucion madre en la sintesis de acido carboxilico

Country Status (15)

Country Link
US (1) US7410632B2 (es)
EP (2) EP2292581B1 (es)
JP (1) JP2004358466A (es)
KR (1) KR101169466B1 (es)
CN (1) CN1572765B (es)
AR (1) AR044616A1 (es)
BR (1) BRPI0401884A (es)
CA (1) CA2466999C (es)
ES (1) ES2437854T3 (es)
MX (1) MXPA04005328A (es)
MY (1) MY142041A (es)
PL (1) PL2292581T3 (es)
PT (1) PT2292581E (es)
RU (1) RU2345980C2 (es)
TW (1) TW200513454A (es)

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Also Published As

Publication number Publication date
KR101169466B1 (ko) 2012-07-30
TW200513454A (en) 2005-04-16
MXPA04005328A (es) 2007-11-14
RU2345980C2 (ru) 2009-02-10
RU2004117063A (ru) 2006-01-10
CA2466999A1 (en) 2004-12-05
JP2004358466A (ja) 2004-12-24
US20040244536A1 (en) 2004-12-09
CN1572765B (zh) 2013-04-17
PL2292581T3 (pl) 2014-03-31
KR20040108594A (ko) 2004-12-24
PT2292581E (pt) 2013-12-16
EP1484307A1 (en) 2004-12-08
CN1572765A (zh) 2005-02-02
BRPI0401884A (pt) 2005-01-18
CA2466999C (en) 2009-08-18
EP2292581B1 (en) 2013-09-25
US7410632B2 (en) 2008-08-12
ES2437854T3 (es) 2014-01-14
MY142041A (en) 2010-08-30
EP2292581A1 (en) 2011-03-09

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