ZA200202941B - Recovery of nickel and cobalt values from a sulfidic flotation concentrate by chloride assisted oxidative pressure leaching in sulfuric acid. - Google Patents

Recovery of nickel and cobalt values from a sulfidic flotation concentrate by chloride assisted oxidative pressure leaching in sulfuric acid.

Info

Publication number
ZA200202941B
ZA200202941B ZA200202941A ZA200202941A ZA200202941B ZA 200202941 B ZA200202941 B ZA 200202941B ZA 200202941 A ZA200202941 A ZA 200202941A ZA 200202941 A ZA200202941 A ZA 200202941A ZA 200202941 B ZA200202941 B ZA 200202941B
Authority
ZA
South Africa
Prior art keywords
nickel
flotation concentrate
recovery
sulfuric acid
pressure leaching
Prior art date
Application number
ZA200202941A
Other languages
English (en)
Inventor
Derek George Eagland Kerfoot
Eberhard Krause
Bruce John Love
Avinash Singhal
Original Assignee
Inco Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Inco Ltd filed Critical Inco Ltd
Publication of ZA200202941B publication Critical patent/ZA200202941B/xx

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0453—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B23/0461—Treatment or purification of solutions, e.g. obtained by leaching by chemical methods
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0407—Leaching processes
    • C22B23/0415—Leaching processes with acids or salt solutions except ammonium salts solutions
    • C22B23/0423—Halogenated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00—Obtaining nickel or cobalt
    • C22B23/04—Obtaining nickel or cobalt by wet processes
    • C22B23/0407—Leaching processes
    • C22B23/0415—Leaching processes with acids or salt solutions except ammonium salts solutions
    • C22B23/043—Sulfurated acids or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Environmental & Geological Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Electrolytic Production Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Extraction Or Liquid Replacement (AREA)
ZA200202941A 2000-09-18 2002-04-15 Recovery of nickel and cobalt values from a sulfidic flotation concentrate by chloride assisted oxidative pressure leaching in sulfuric acid. ZA200202941B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US09/664,475 US6428604B1 (en) 2000-09-18 2000-09-18 Hydrometallurgical process for the recovery of nickel and cobalt values from a sulfidic flotation concentrate

Publications (1)

Publication Number Publication Date
ZA200202941B true ZA200202941B (en) 2003-04-15

Family

ID=24666118

Family Applications (1)

Application Number Title Priority Date Filing Date
ZA200202941A ZA200202941B (en) 2000-09-18 2002-04-15 Recovery of nickel and cobalt values from a sulfidic flotation concentrate by chloride assisted oxidative pressure leaching in sulfuric acid.

Country Status (13)

Country Link
US (2) US6428604B1 (pt)
EP (1) EP1325165B1 (pt)
JP (1) JP3946633B2 (pt)
CN (1) CN1210417C (pt)
AT (1) ATE338833T1 (pt)
AU (1) AU774519B2 (pt)
BR (1) BR0107217A (pt)
CA (1) CA2376883C (pt)
DE (1) DE60122914T2 (pt)
FI (1) FI123376B (pt)
RU (1) RU2221881C1 (pt)
WO (1) WO2002024966A1 (pt)
ZA (1) ZA200202941B (pt)

Families Citing this family (61)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1303641B1 (en) * 2000-07-25 2005-12-28 Phelps Dodge Corporation Method for recovery of copper from sulfidic ore materials using super-fine grinding and medium temperature pressure leaching
US6428604B1 (en) * 2000-09-18 2002-08-06 Inco Limited Hydrometallurgical process for the recovery of nickel and cobalt values from a sulfidic flotation concentrate
US20050126923A1 (en) * 2001-07-25 2005-06-16 Phelps Dodge Corporation Process for recovery of copper from copper-bearing material using medium temperature pressure leaching, direct electrowinning and solvent/solution extraction
US7476308B2 (en) * 2001-07-25 2009-01-13 Phelps Dodge Corporation Process for multiple stage direct electrowinning of copper
US6863825B2 (en) 2003-01-29 2005-03-08 Union Oil Company Of California Process for removing arsenic from aqueous streams
US20040156765A1 (en) * 2003-02-12 2004-08-12 Nichromet Extraction Inc. Gold and silver recovery from polymetallic sulfides by treatment with halogens
CA2568144A1 (en) * 2004-05-21 2005-12-01 Wmc Resources Ltd Recovery of nickel
EA010942B1 (ru) * 2004-10-29 2008-12-30 Фелпс Додж Корпорейшн Способ извлечения меди из медьсодержащего материала
US7736487B2 (en) 2004-10-29 2010-06-15 Freeport-Mcmoran Corporation Process for recovery of copper from copper-bearing material using pressure leaching, direct electrowinning and solution extraction
CN101175863A (zh) * 2005-05-13 2008-05-07 Bhp比利通Ssm技术有限公司 含镍氧化矿石堆浸的改进方法
BRPI0616811B1 (pt) * 2005-10-03 2014-05-20 Outotec Oyj Processo para a recuperação de Níquel a partir de um material contendo Sulfeto de Níquel
BRPI0505544B1 (pt) * 2005-11-10 2014-02-04 Processo de lixiviação combinada
US7572317B2 (en) * 2005-11-10 2009-08-11 Barrick Gold Corporation Thiosulfate generation in situ in precious metal recovery
US8066874B2 (en) 2006-12-28 2011-11-29 Molycorp Minerals, Llc Apparatus for treating a flow of an aqueous solution containing arsenic
US20080308429A1 (en) * 2007-06-18 2008-12-18 Cvrd Inco Limited Method for improving cathode morphology
US7998441B2 (en) * 2007-09-20 2011-08-16 Cvrd Inco Limited Method for selective removal of cadmium
US8349764B2 (en) 2007-10-31 2013-01-08 Molycorp Minerals, Llc Composition for treating a fluid
US8252087B2 (en) 2007-10-31 2012-08-28 Molycorp Minerals, Llc Process and apparatus for treating a gas containing a contaminant
CN101760616B (zh) * 2008-12-02 2011-08-10 中国恩菲工程技术有限公司 含钴矿石的浸出方法
CN101705371B (zh) * 2009-11-20 2011-04-06 北京矿冶研究总院 一种硫化铜钴矿中提取钴的方法
RU2444573C2 (ru) * 2010-01-20 2012-03-10 Открытое акционерное общество "Кольская горно-металлургическая компания" Способ производства концентрата драгоценных металлов из сульфидного медно-никелевого сырья
US20130001137A1 (en) * 2010-01-28 2013-01-03 Mcmaster University Nanoparticle flotation collectors
FI122188B (fi) * 2010-03-18 2011-09-30 Outotec Oyj Hydrometallurginen menetelmä metallisen nikkelin valmistamiseksi
JP5445777B2 (ja) * 2010-07-28 2014-03-19 住友金属鉱山株式会社 低品位ニッケル酸化鉱石からのフェロニッケル製錬原料の製造方法
CN102002586B (zh) * 2010-12-04 2012-09-26 金川集团有限公司 一种含镍高钴硫化物浸出工艺
US9447480B2 (en) * 2011-01-25 2016-09-20 The University Of Queensland Method of ore processing
US10662503B2 (en) * 2011-01-25 2020-05-26 The University Of Queensland Method of ore processing using mixture including acidic leach solution and oxidizing agent
US9233863B2 (en) 2011-04-13 2016-01-12 Molycorp Minerals, Llc Rare earth removal of hydrated and hydroxyl species
CN102206834B (zh) * 2011-05-03 2012-12-26 四川省尼科国润新材料有限公司 一种用低冰镍直接生产电解镍的方法
CN102367176A (zh) * 2011-07-01 2012-03-07 王嘉兴 用废渣铜泥制备硫化铜，磷酸铜和磷酸钠的方法
CN102344163A (zh) * 2011-07-01 2012-02-08 王嘉兴 用废渣铜泥制备硫化铜，碳酸铜和氯化钠的方法
CN102367173A (zh) * 2011-07-01 2012-03-07 王嘉兴 用废渣铜泥制备硫化铜和氯化钠的方法
CN102344118A (zh) * 2011-07-01 2012-02-08 王嘉兴 用废渣铜泥制备硫化铜，氢氧化铜和氯化钠的方法
CN102367175A (zh) * 2011-07-01 2012-03-07 王嘉兴 用废渣铜泥制备硫化铜，氢氧化铜和氯化钠的方法
CN102367179A (zh) * 2011-07-01 2012-03-07 王嘉兴 用废渣铜泥制备硫化铜，氯化铜和氯化钠的方法
FI20110279A0 (fi) 2011-08-29 2011-08-29 Outotec Oyj Menetelmä metallien talteenottamiseksi niitä sisältävästä materiaalista
JP5800254B2 (ja) * 2011-12-26 2015-10-28 住友金属鉱山株式会社 硫酸コバルトの製造方法
JP5842684B2 (ja) * 2012-03-13 2016-01-13 住友金属鉱山株式会社 湿式製錬方法
JP5424139B2 (ja) * 2012-03-19 2014-02-26 住友金属鉱山株式会社 製鉄用ヘマタイトの製造方法
FI124883B (fi) 2012-12-20 2015-03-13 Outotec Oyj Menetelmä ja laitteisto metallikiven happogranuloimiseksi
CN103272700B (zh) * 2013-06-07 2014-11-05 浙江华友钴业股份有限公司 一种从铜钴矿酸浸冶炼渣中浮选回收铜钴的方法
CN103386359A (zh) * 2013-07-19 2013-11-13 广州有色金属研究院 一种氧化铜钴矿的选矿方法
JP5440823B1 (ja) 2013-09-18 2014-03-12 住友金属鉱山株式会社 製鉄用ヘマタイトの製造方法
CN103725887A (zh) * 2013-12-13 2014-04-16 金川集团股份有限公司 一种浸出海绵铜的方法
MX370462B (es) 2014-03-07 2019-12-13 Secure Natural Resources Llc Oxido de cerio (iv) con propiedades de remocion de arsenico excepcionales.
JP5884870B1 (ja) * 2014-08-13 2016-03-15 住友金属鉱山株式会社 ニッケルの回収方法
US10457565B2 (en) 2014-09-18 2019-10-29 Sumitomo Metal Mining Co., Ltd. Production method for hematite for iron production
CA2971222C (en) * 2014-12-19 2021-06-22 Flsmidth A/S Methods for rapidly leaching chalcopyrite
RU2613823C1 (ru) * 2015-12-18 2017-03-21 Федеральное государственное бюджетное учреждение науки Институт химии и технологии редких элементов и минерального сырья им. И.В. Тананаева Кольского научного центра Российской академии наук (ИХТРЭМС КНЦ РАН) Способ получения концентрата драгоценных металлов из медно-никелевого файнштейна
WO2017197417A1 (en) * 2016-05-09 2017-11-16 Mintek Method of recovering a target metal
JP7062996B2 (ja) * 2017-03-29 2022-05-09 住友金属鉱山株式会社 チオン酸を含む溶液の保存方法および定量方法、ならびにチオン酸を含む試料溶液およびその作製方法
JP6957974B2 (ja) * 2017-05-23 2021-11-02 住友金属鉱山株式会社 塩素浸出方法、電気ニッケルの製造方法
JP2020522622A (ja) * 2017-06-08 2020-07-30 アーバン マイニング プロプライエタリー リミテッド 使用済みのリチウムベースのバッテリー及びその他のフィードからコバルト、リチウム、及びその他の金属を回収するプロセス
CN108118149B (zh) * 2017-12-14 2019-07-19 中南大学 一种用硫化镍精矿制备动力电池正极材料前驱体的方法
CN108103311A (zh) * 2017-12-14 2018-06-01 中南大学 一种铜镍混合矿的湿法冶炼方法
AU2019428963B2 (en) * 2019-02-13 2023-08-03 KEMCO (Korea Energy Materials Company) Economical method, using combination of wet and dry processes, for smelting nickel from nickel sulfide ores
CN112680602A (zh) * 2020-12-18 2021-04-20 衢州华友钴新材料有限公司 一种提升含铜硫化矿浸出效率的处理方法
CN113957264A (zh) * 2021-09-13 2022-01-21 广东邦普循环科技有限公司 一种由低冰镍制备硫酸镍的方法
WO2023092480A1 (zh) * 2021-11-26 2023-06-01 深圳市坤鹏冶金工程技术有限公司 一种从高冰镍中提取硫酸镍的方法
WO2024103106A1 (en) * 2022-11-14 2024-05-23 Hydromet WA Pty Limited "method for the preferential leach of value metals from sulphide concentrates"
CN115818739B (zh) * 2022-12-22 2024-07-09 广西中伟新能源科技有限公司 使用高冰镍制备硫酸镍的方法

Family Cites Families (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4039406A (en) 1973-08-10 1977-08-02 Noranda Mines Limited Recovering copper from concentrates with insoluble sulfate forming leach
JPS50115614A (pt) * 1974-02-16 1975-09-10
US3981962A (en) * 1975-06-30 1976-09-21 The United States Of America As Represented By The Secretary Of The Interior Decomposition leach of sulfide ores with chlorine and oxygen
CA1092056A (en) 1977-10-11 1980-12-23 Victor A. Ettel Electrowinning cell with bagged anode
CA1107678A (en) 1978-04-12 1981-08-25 Kohur N. Subramanian Nickel recovery from sulfur-deficient mattes
CA1125228A (en) 1979-10-10 1982-06-08 Daniel P. Young Process for electrowinning nickel or cobalt
US4384940A (en) * 1982-01-21 1983-05-24 Inco Limited Chlorine leaching of nickel-cobalt-iron sulphides
NO833784L (no) * 1983-10-18 1985-04-19 Thomas Thomassen Autoklav-klorluting av kobbersulfidkonsentrater
ZA872869B (pt) * 1986-04-24 1987-10-12
CA2071626C (en) 1991-10-25 2001-08-14 Ian James Corrans Activation of a mineral species
US5431788A (en) 1993-06-28 1995-07-11 Cominco Engineering Services Ltd. Chloride assisted hydrometallurgical copper extraction
US5902474A (en) 1993-07-29 1999-05-11 Cominco Engineering Services Ltd. Chloride assisted hydrometallurgical extraction of metal
US5874055A (en) 1993-07-29 1999-02-23 Cominco Engineering Services Ltd. Chloride assisted hydrometallurgical extraction of metal
US5650057A (en) 1993-07-29 1997-07-22 Cominco Engineering Services Ltd. Chloride assisted hydrometallurgical extraction of metal
US5855858A (en) 1993-07-29 1999-01-05 Cominco Engineering Services Ltd. Process for the recovery of nickel and/or cobalt from an ore or concentrate
US5378262A (en) * 1994-03-22 1995-01-03 Inco Limited Process for the extraction and separation of nickel and/or cobalt
CA2137124C (en) * 1994-12-01 1999-03-16 Tao Xue Pressure leaching of nickel and cobalt sulphides with chlorine under controlled redox potential conditions
GB9503877D0 (en) 1995-02-27 1995-04-19 Sherritt Inc Recovery of copper from sulphidic concentrates
AUPN191395A0 (en) * 1995-03-22 1995-04-27 M.I.M. Holdings Limited Atmospheric mineral leaching process
FI98073C (fi) * 1995-08-14 1997-04-10 Outokumpu Eng Oy Menetelmä nikkelin talteenottamiseksi hydrometallurgisesti kahdesta eri nikkelikivestä
AUPN476695A0 (en) 1995-08-14 1995-09-07 Dominion Mining Limited Method of processing a copper mineral species
JPH10140257A (ja) 1996-11-07 1998-05-26 Sumitomo Metal Mining Co Ltd 塩素浸出電解採取法によるニッケルの湿式精錬方法
US5993514A (en) * 1997-10-24 1999-11-30 Dynatec Corporation Process for upgrading copper sulphide residues containing nickel and iron
US6428604B1 (en) * 2000-09-18 2002-08-06 Inco Limited Hydrometallurgical process for the recovery of nickel and cobalt values from a sulfidic flotation concentrate

Also Published As

Publication number Publication date
BR0107217A (pt) 2002-07-09
JP2004509232A (ja) 2004-03-25
EP1325165B1 (en) 2006-09-06
CA2376883C (en) 2002-12-03
AU3716901A (en) 2002-04-02
ATE338833T1 (de) 2006-09-15
US6428604B1 (en) 2002-08-06
CN1210417C (zh) 2005-07-13
FI123376B (fi) 2013-03-15
US20030033906A1 (en) 2003-02-20
CA2376883A1 (en) 2002-03-28
CN1392902A (zh) 2003-01-22
EP1325165A1 (en) 2003-07-09
AU774519B2 (en) 2004-07-01
WO2002024966A1 (en) 2002-03-28
FI20020784A (fi) 2002-04-23
US6569224B2 (en) 2003-05-27
RU2002113102A (ru) 2004-01-27
JP3946633B2 (ja) 2007-07-18
DE60122914T2 (de) 2007-04-26
DE60122914D1 (de) 2006-10-19
RU2221881C1 (ru) 2004-01-20

Similar Documents

Publication Publication Date Title
ZA200202941B (en) Recovery of nickel and cobalt values from a sulfidic flotation concentrate by chloride assisted oxidative pressure leaching in sulfuric acid.
CA2624609C (en) Processing of nickel sulphide ore or concentrates with sodium chloride
EP0924307B1 (en) Solvent extraction of cobalt and nickel values from a magnesium containing solution
RU98100436A (ru) Способ извлечения металла
AP1658A (en) Process for direct electrowinning of copper.
RU2000106438A (ru) Способ извлечения металла из руды или концентрата
AU2011228956B2 (en) Method of processing nickel bearing raw material
GB1374851A (en) Hydrometallurgical process for extraction of copper and sulphur from copper-iron sulphides
JP2014070262A (ja) ニッケルスラッジの処理方法
CA2295468A1 (en) Separation and concentration method
CN112195344A (zh) 一种从高浸渣浮选尾矿水中萃取回收锌的方法
CN100366767C (zh) 用氯化物浸析和萃取回收金属的方法
US3463710A (en) Electrolytic recovery of copper from copper cyanide leaching solutions
CA2454854A1 (en) Method of recovering sulfur from leaching residue under atmospheric pressure
GB1407520A (en) Electrolytic hydrometallurgical process to recover copper from sulphide ore concentrates
US5807421A (en) Hydrometallurgical extraction process
GB1396470A (en) Process for separating oxidic ores containing nickel and or copper and or cobalt
Sole et al. The potential for recovery of cobalt from copper leach solutions
JPS56136940A (en) Recovering method for copper, nickel and cobalt in solution leached from manganese nodule with sulfuric acid
Lindermann et al. The BATENUS process for recycling battery waste
EP1252345A4 (en) SOLVENT EXTRACTION OF POLLUTANT METALS FROM VALUABLE METAL-SULPHATE SOLUTIONS
RU1770426C (ru) Способ переработки пылей от заточки твердосплавного инструмента, содержащих вольфрам
AU755776B2 (en) Process for the extraction of nickel and/or cobalt values from a solution
SU1678869A1 (ru) Способ осаждени сульфидов меди и никел
CN116162802A (zh) 利用红土镍矿型高冰镍提取镍钴的方法