YU45244B - Process for recrystallisation of octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine and hexahydro-1,3,5-trinitro-1,3,5-triazinedd - Google Patents

Process for recrystallisation of octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine and hexahydro-1,3,5-trinitro-1,3,5-triazinedd

Info

Publication number
YU45244B
YU45244B YU423/85A YU42385A YU45244B YU 45244 B YU45244 B YU 45244B YU 423/85 A YU423/85 A YU 423/85A YU 42385 A YU42385 A YU 42385A YU 45244 B YU45244 B YU 45244B
Authority
YU
Yugoslavia
Prior art keywords
triazinedd
tetrazocine
tetranitro
trinitro
recrystallisation
Prior art date
Application number
YU423/85A
Other languages
English (en)
Other versions
YU42385A (en
Inventor
L Svesol
J O Nydqvist
L Westiling
Original Assignee
Bofors Ab
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bofors Ab filed Critical Bofors Ab
Publication of YU42385A publication Critical patent/YU42385A/xx
Publication of YU45244B publication Critical patent/YU45244B/xx

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D257/00Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms
    • C07D257/02Heterocyclic compounds containing rings having four nitrogen atoms as the only ring hetero atoms not condensed with other rings
    • CCHEMISTRY; METALLURGY
    • C06EXPLOSIVES; MATCHES
    • C06BEXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B25/00Compositions containing a nitrated organic compound
    • C06B25/34Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D251/00Heterocyclic compounds containing 1,3,5-triazine rings
    • C07D251/02Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
    • C07D251/12Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D251/26Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
    • C07D251/40Nitrogen atoms
    • C07D251/54Three nitrogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Saccharide Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Peptides Or Proteins (AREA)
  • Liquid Crystal Substances (AREA)
YU423/85A 1984-04-04 1985-03-18 Process for recrystallisation of octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine and hexahydro-1,3,5-trinitro-1,3,5-triazinedd YU45244B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE8401857A SE451718B (sv) 1984-04-04 1984-04-04 Sett att omkristallisera sprengemnena oktogen och hexogen

Publications (2)

Publication Number Publication Date
YU42385A YU42385A (en) 1988-10-31
YU45244B true YU45244B (en) 1992-05-28

Family

ID=20355439

Family Applications (1)

Application Number Title Priority Date Filing Date
YU423/85A YU45244B (en) 1984-04-04 1985-03-18 Process for recrystallisation of octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine and hexahydro-1,3,5-trinitro-1,3,5-triazinedd

Country Status (16)

Country Link
US (1) US4638065A (de)
JP (1) JPS60226500A (de)
AR (1) AR240789A1 (de)
AU (1) AU567609B2 (de)
BR (1) BR8501575A (de)
CA (1) CA1243672A (de)
DE (1) DE3510761C2 (de)
ES (1) ES8608325A1 (de)
FR (1) FR2562538B1 (de)
GB (1) GB2156805B (de)
IN (1) IN163711B (de)
IT (1) IT1181872B (de)
NO (1) NO160775B (de)
RO (1) RO93878B (de)
SE (1) SE451718B (de)
YU (1) YU45244B (de)

Families Citing this family (34)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3527200A1 (de) * 1985-07-30 1987-03-19 Horst Dipl Ing Hommel Verfahren zum herstellen von sphaerolitischem kristallisat hoher schuett- und packungsdichte, insbesondere von kugelig kristallisiertem nitroguanidin
DE3605634A1 (de) * 1986-02-21 1987-08-27 Messerschmitt Boelkow Blohm Verfahren zur behandlung kristalliner sprengstoffe fuer hochleistungssprengladungen
DE3617408C1 (de) * 1986-05-23 1987-06-11 Dynamit Nobel Ag Verfahren zur Herstellung von feinkoernigem beta-Oktogen
DE3878580T2 (de) * 1987-04-22 1993-06-09 Nobel Kemi Ab Verfahren zur herstellung von kristallinen explosivstoffen.
DE4237580C1 (de) * 1992-11-06 1994-03-17 Wasagchemie Sythen Gmbh Aufbereitung wachshaltiger Explosivstoffe
SE504054C2 (sv) * 1995-01-27 1996-10-28 Bofors Explosives Ab Flödesschema över återvinning av sprängämne
WO1998027072A1 (en) * 1996-12-17 1998-06-25 Cordant Technologies, Inc. Salting-out process of crystallizing 2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.0?5,903,11¿]-dodecane
US6214988B1 (en) 1999-01-03 2001-04-10 Schlumberger Technology Corporation Process for making an HMX product
US6201117B1 (en) 1999-05-26 2001-03-13 Schlumberger Technology Corporation Process for making a 1,3,5,7-tetraalkanoyl-1,3,5,7-tetraazacyclooctane
US6194571B1 (en) 1999-05-26 2001-02-27 Schlumberger Technology Corporation HMX compositions and processes for their preparation
US6265573B1 (en) 1999-05-26 2001-07-24 Schlumberger Technology Corporation Purification process
US6428724B1 (en) 1999-05-26 2002-08-06 Schlumberger Technology Corporation Granulation process
JP4530528B2 (ja) * 2000-12-11 2010-08-25 旭化成ケミカルズ株式会社 粉状火薬組成物の製法
NO318866B1 (no) * 2003-10-06 2005-05-18 Dyno Nobel Asa Pressbar plastisk bundet sprengstoffkomposisjon
FR2887544B1 (fr) * 2005-06-02 2008-07-18 Saint Louis Inst Particules d'explosif peu sensibles aux chocs et procede de traitement associe
GB2426755B (en) * 2005-06-02 2009-07-22 Saint Louis Inst Crystalline explosive form and preparation process thereof
FR2886641A1 (fr) * 2005-06-02 2006-12-08 Saint Louis Inst Particules d'explosif peu sensibles aux chocs et procede de traitement associe
US20060272756A1 (en) * 2005-06-06 2006-12-07 Schlumberger Technology Corporation RDX Composition and Process for Its Manufacture
JP2008189515A (ja) * 2007-02-05 2008-08-21 Nippon Koki Co Ltd 鈍感化爆薬組成物およびその製造方法
JP5253762B2 (ja) * 2007-06-07 2013-07-31 日本工機株式会社 Rdxの球状化方法
JP2009051692A (ja) * 2007-08-27 2009-03-12 Nippon Koki Co Ltd 多面体化したrdx、rdxの多面体化方法、球状化rdxの製造方法
US8002917B2 (en) 2009-02-09 2011-08-23 The United States Of America As Represented By The Secretary Of The Army Adjusting yield of a manufacturing process for energetic compounds through solubility modification
CN101955469A (zh) * 2010-09-17 2011-01-26 北京理工大学 一种奥克托今与黑索今混合物分离方法
CN101973947B (zh) * 2010-09-25 2015-12-09 北京理工大学 一种用结晶控制技术制备球形化黑索今的方法
JP5993241B2 (ja) * 2012-08-02 2016-09-14 中国化薬株式会社 Rdxの製造方法
CN102887865A (zh) * 2012-09-22 2013-01-23 山西北化关铝化工有限公司 特质黑索今的制备方法
CN102887870B (zh) * 2012-09-22 2015-07-15 山西北化关铝化工有限公司 导爆管用奥克托今
CN102887866B (zh) * 2012-09-22 2015-08-12 山西北化关铝化工有限公司 改性黑索今的生产方法
CN103044173B (zh) * 2012-12-06 2015-03-04 中国工程物理研究院化工材料研究所 一种有序多孔含能晶体材料的制备方法
CN103936534B (zh) * 2014-05-09 2016-07-06 北京理工大学 一种特质细化hmx晶体及制备方法
CN104294366B (zh) * 2014-10-11 2017-01-18 中北大学 一种厘米级奥克托今单晶的培养方法
RU2670231C1 (ru) * 2017-11-15 2018-10-19 Акционерное общество "Федеральный научно-производственный центр "Алтай" Способ перекристаллизации октогена
KR101999744B1 (ko) * 2017-12-29 2019-07-12 주식회사 한화 사이클로 트리메틸렌 트리나이트라민의 제조 방법
CN114230534B (zh) * 2021-11-23 2023-11-24 中北大学 一种声共振辅助溶剂侵蚀技术制备黑索今球晶方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA816157A (en) * 1969-06-24 D. Evans Albert Crystallization of fine hmx
US2656355A (en) * 1953-10-20 Purification of cyclonite
US2434230A (en) * 1948-01-06 Method of preparing i
DE681848C (de) * 1937-04-11 1939-09-15 Edmund Von Herz Verfahren zur Gewinnung von reinem Cyclotrimethylentrinitramin
US2959587A (en) * 1943-07-16 1960-11-08 John R Johnson Sensitivity control during purification of crude cyclonite
US3133054A (en) * 1962-03-07 1964-05-12 Eastman Kodak Co Processing of hmx
US3297681A (en) * 1964-02-26 1967-01-10 Eastman Kodak Co Crystallization of fine hmx
AU6718365A (en) * 1965-11-29 1967-06-01 Eastman Kodakcompany Crystallization of fine hmx
JPS4714112Y1 (de) * 1969-07-08 1972-05-22
US4092383A (en) * 1977-08-15 1978-05-30 The United States Of America As Represented By The Secretary Of The Navy Modification of ballistic properties of HMX by spray drying

Also Published As

Publication number Publication date
AU567609B2 (en) 1987-11-26
US4638065A (en) 1987-01-20
GB2156805B (en) 1987-10-07
FR2562538B1 (fr) 1987-04-30
FR2562538A1 (fr) 1985-10-11
YU42385A (en) 1988-10-31
RO93878A (ro) 1988-02-29
ES8608325A1 (es) 1986-07-16
GB8506432D0 (en) 1985-04-17
AU4080685A (en) 1985-10-10
JPH0471039B2 (de) 1992-11-12
SE8401857L (sv) 1985-10-05
DE3510761A1 (de) 1985-10-17
ES541846A0 (es) 1986-07-16
IN163711B (de) 1988-10-29
NO851270L (no) 1985-10-07
CA1243672A (en) 1988-10-25
SE451718B (sv) 1987-10-26
AR240789A2 (es) 1991-02-28
JPS60226500A (ja) 1985-11-11
AR240789A1 (es) 1991-02-28
NO160775B (no) 1989-02-20
SE8401857D0 (sv) 1984-04-04
BR8501575A (pt) 1985-12-03
IT8547908A0 (it) 1985-04-02
GB2156805A (en) 1985-10-16
RO93878B (ro) 1988-03-01
DE3510761C2 (de) 1997-03-06
IT1181872B (it) 1987-09-30

Similar Documents

Publication Publication Date Title
YU45244B (en) Process for recrystallisation of octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine and hexahydro-1,3,5-trinitro-1,3,5-triazinedd
GB2246620B (en) Methods and apparatus for disarming and arming explosive detonators
ZA856047B (en) Non-primary explosive detonator
HUT37548A (en) Herbicides containing - as reagent - derivatives of pirosole
AR240641A1 (es) Procedimiento para prparar compuestos de 4-amino-6-carbamoil-1,3,4,5-tetrahidrobenz(c,d)indol y compuestos intermediarios
EP0273328A3 (en) Triazine derivatives and herbicides containing said derivatives
GB8432803D0 (en) Detonation chamber
ZA829417B (en) Process and intermediates for octahydrobenzofuro-(3,2-e)isoquinolines
GB8524131D0 (en) Carrying strap for weapon
EG17719A (en) Heterocyclic herbicides
IL86233A0 (en) Substituted tetrahydrophthalimides,processes for their preparation and herbicides containing them
DE3565537D1 (en) Triazine derivatives and herbicides
IL74141A0 (en) Process and intermediates for the preparation of aryl substituted pyrido(1,4)benzodiazepines
OA09789A (en) "Processes and compounds useful for resolving 1-methyl-3-phenylpropylamine".
GB2186062B (en) Method of adjusting firearm sights
RO84285B (ro) Detector de radiatii y si neutroni cu alimentare proprie
YU142785A (en) Process for obtaining aromatic 1,4-oxazepinone and thione
ZA826491B (en) Azomethines of 4-amino-6-halogeno-tert.-butyl-1,2,4-triazin-5-ones,a process for their preparation and their use as herbicides
EP0295119A3 (en) 14-chlorodaunomycin and process for the preparation of 14-chlorodaunomycin, and process for the preparation of (2"r)-4'-0-tetrahydropyranyladriamycin
YU43671B (en) Device for closing feeding inlet of pressure resistant vessels
SU1184359A1 (ru) Способ определения бризантности взрывчатого вещества
GB2118175B (en) Herbicidal derivatives of nitrogen-containing heterocycles
IL103461A0 (en) Process for the preparation of herbicidal o-carboxyarylimidazolinones,and novel intermediates thereof
IL84873A0 (en) Process and intermediates for the preparation of aryl substituted pyrido(1,4)benzodiazepines
PL257748A1 (en) Thermite ignition matches