WO2023221411A1 - 化工生产用高效混合反应釜 - Google Patents

化工生产用高效混合反应釜 Download PDF

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Publication number
WO2023221411A1
WO2023221411A1 PCT/CN2022/129521 CN2022129521W WO2023221411A1 WO 2023221411 A1 WO2023221411 A1 WO 2023221411A1 CN 2022129521 W CN2022129521 W CN 2022129521W WO 2023221411 A1 WO2023221411 A1 WO 2023221411A1
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Prior art keywords
kettle body
grinding
raw materials
liquid
kettle
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PCT/CN2022/129521
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English (en)
French (fr)
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刘振海
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中润华谷(南京)科技有限公司
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Publication of WO2023221411A1 publication Critical patent/WO2023221411A1/zh

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/19Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/191Stirrers with two or more mixing elements mounted in sequence on the same axis with similar elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/85Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with two or more stirrers on separate shafts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/83Mixing plants specially adapted for mixing in combination with disintegrating operations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C2/00Crushing or disintegrating by gyratory or cone crushers
    • B02C2/10Crushing or disintegrating by gyratory or cone crushers concentrically moved; Bell crushers
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/141Feedstock

Definitions

  • the invention relates to the technical field of reaction kettles, and in particular to a high-efficiency mixing reaction kettle for chemical production.
  • the broad understanding of a reactor is a container for physical or chemical reactions. Through the structural design and parameter configuration of the container, the heating, evaporation, cooling and low-speed mixing functions required by the process are realized.
  • the reactor is widely used in petroleum, chemical industry, In the fields of rubber, pesticides, dyes, medicine and food, etc., they are pressure vessels used to complete vulcanization, nitration, hydrogenation, hydrocarbonization, polymerization, condensation and other processes, such as reactors, reaction pots, decomposition pots, polymerization kettles, etc.; material Generally, there are carbon manganese steel, stainless steel, zirconium, nickel-based alloys and other composite materials.
  • the existing technology has the following shortcomings: Most of the reaction kettles used for chemical production in the existing technology directly add solid chemical raw materials into the reaction kettle. Since the solid chemical raw materials are mostly piled up in one area when they enter the reaction kettle, they need to be dissolved layer by layer. Dissolve, and some solid chemical raw materials have large particles and a small total contact area with the liquid, which takes a long time to dissolve, resulting in a greatly reduced mixing rate of the raw materials. Secondly, because most of the chemical raw materials in the reactor are mixed Horizontal stirring and turning effects are poor, and some solid chemical raw materials are easy to precipitate at the bottom of the reactor, resulting in a further reduction in the mixing rate of the raw materials.
  • the present invention provides a high-efficiency mixing reactor for chemical production.
  • a high-efficiency mixing reaction kettle for chemical production including a kettle body.
  • the top of the kettle body is provided with a grinding mechanism and an air supply mechanism.
  • the air supply mechanism is provided at the bottom of the grinding mechanism.
  • the inner cavity of the kettle is equipped with a liquid extraction and atomization mechanism; the air supply mechanism blows the chemical raw materials ground into powder, and the liquid extraction and atomization mechanism extracts and atomizes the liquid at the bottom of the kettle body, and is driven by the atomized liquid Floating powdered chemical raw materials sink.
  • the grinding mechanism includes a grinding funnel connected to the top of the kettle body, a grinding body arranged inside the grinding funnel, a rotating shaft connected to the top of the grinding body, a first motor fixedly mounted on the top of the kettle body, and a first motor connected to the top of the kettle body.
  • a first transmission mechanism between a motor and a rotating shaft, the rotating shaft is rotationally connected to the kettle body through a bearing.
  • the top of the grinding body is arranged in a tapered surface, the gap between the grinding body and the grinding funnel gradually decreases from top to bottom, and the first transmission mechanism includes an active drive connected to the outside of the first motor output shaft. gear, and a driven gear connected to the outside of the rotating shaft, and the driving gear meshes with the driven gear.
  • the air supply mechanism includes a fan connected to one side of the kettle body, a cavity provided in the kettle body, and an exhaust port connected to the end of the cavity, and the outlet end of the fan is connected to the cavity.
  • the exhaust port is set at the bottom of the discharge opening of the grinding funnel.
  • the liquid pumping and atomizing mechanism includes a liquid storage chamber and a submersible pump arranged at the top of the kettle cavity, an annular cavity arranged at the bottom of the kettle cavity, a hollow cover arranged in an annular array outside the annular cavity, and connected to the There are atomizing nozzles distributed in an annular array at the bottom of the liquid storage chamber, a drain pipe connected between the submersible pump and the liquid storage chamber, a suction pipe connected between the submersible pump and the annular chamber, and a filter screen connected at the bottom of the hollow cover. , and a connecting pipe connected between the annular cavity and the hollow cover.
  • a stirring mechanism is provided on both sides of the kettle body.
  • the stirring mechanism includes a second motor connected to one side of the kettle body, a stirring shaft rotatably connected to the kettle body, and a stirring shaft connected to the output shaft of the second motor.
  • the second transmission mechanism between the stirring shafts and the stirring blades evenly distributed from top to bottom are connected to the outside of the stirring shaft.
  • the second transmission mechanism includes a driving bevel gear connected to the end of the output shaft of the second motor and a driven bevel gear connected to the outside of the stirring shaft, and the driving bevel gear meshes with the driven bevel gear.
  • a scraper mechanism is provided at the bottom of the kettle body, and the scraper mechanism includes a third motor connected to the bottom of the kettle body, a rotating block arranged at the bottom of the kettle body cavity, and an annular array distribution connected to the outside of the rotating block.
  • the scraper strip fits the bottom of the filter screen.
  • liquid raw materials are added to the kettle, and then the solid raw materials are ground by a grinding mechanism, so that the solid raw materials are ground into powder and fall. When the solid raw materials fall, they are blown by the air supply mechanism to make the powdery raw materials. The solid raw materials sway with the wind and eventually fall into the liquid raw materials at multiple drop points, which can effectively prevent the accumulation of solid raw materials and accelerate the mixing between raw materials. Grinding the solid raw materials can increase the contact area between the raw materials and the liquid. This can speed up the mixing rate of solid raw materials and liquid again;
  • the liquid at the bottom of the kettle is extracted and atomized through the liquid pumping and atomizing mechanism, and then falls back, which can effectively turn the mixed raw materials and prevent the solid raw materials from accumulating at the bottom of the kettle cavity, which can further speed up the process.
  • the mixing rate of solid raw materials and liquids can cause the floating powdery chemical raw materials to sink through the sprayed atomized liquid. This not only allows the solid raw materials to quickly fall into the liquid raw materials, but also effectively prevents the powdery chemical raw materials from falling.
  • Chemical raw materials flow out of the kettle, effectively avoiding the waste of solid raw materials flowing out, and at the same time effectively preventing the flow of powdered chemical raw materials from having a certain impact on the surrounding environment.
  • Figure 1 is a schematic diagram of the overall structure of the present invention.
  • Figure 2 is an enlarged view of part A of Figure 1 in the present invention
  • Figure 3 is a bottom view of the liquid storage chamber and atomizing nozzle of the present invention.
  • Figure 4 is a top view of the rotating block and scraper according to the present invention.
  • Figure 5 is a usage scenario diagram of the present invention.
  • a high-efficiency mixing reaction kettle for chemical production includes a kettle body 1.
  • a grinding mechanism 2 and an air supply mechanism 3 are provided on the top of the kettle body 1.
  • the air supply mechanism 3 is disposed on the grinding mechanism. 2 at the bottom, the inner cavity of the kettle body 1 is provided with a liquid extraction and atomization mechanism 4; the air supply mechanism 3 blows the chemical raw materials ground into powder, and the liquid extraction and atomization mechanism 4 extracts and atomizes the liquid at the bottom of the kettle body 1.
  • the atomized liquid drives the floating powdery chemical raw materials to sink;
  • liquid raw materials are first added to the kettle 1, and then the solid raw materials are ground through the grinding mechanism 2, so that the solid raw materials are ground into powder and fall.
  • the wind mechanism 3 blows, causing the powdery solid raw materials to sway with the wind, and finally realizes multiple falling points in the liquid raw materials, which can effectively prevent the accumulation of solid raw materials, accelerate the mixing between raw materials, and grind the solid raw materials to The contact area between the raw material and the liquid is increased, thereby speeding up the mixing rate of the solid raw material and the liquid again.
  • the liquid at the bottom of the kettle body 1 is extracted and atomized through the liquid pumping and atomizing mechanism 4, and then falls back.
  • the mixed raw materials can be effectively turned to prevent the solid raw materials from accumulating at the bottom of the inner cavity of the kettle body 1, and the mixing rate of the solid raw materials and the liquid can be further accelerated.
  • the sprayed atomized liquid can drive the floating powdery chemical raw materials. Sinking not only allows the solid raw materials to quickly fall into the liquid raw materials, but also effectively prevents the powdery chemical raw materials from flowing out of the kettle body 1, effectively avoiding the waste of solid raw materials from flowing out, and effectively preventing the powdery chemical raw materials from flowing out.
  • the outflow will have a certain impact on the surrounding environment.
  • the first transmission mechanism 25 here is a driving gear 251 and a slave gear.
  • Driving gear 252 as shown in Figures 1 and 5, the diameter of the driving gear 251 is larger than the diameter of the driven gear 252, so that the driving gear 251 can accelerate the rotation of the driven gear 252, and at the same time, the setting of the first transmission mechanism 25 can Increasing the bending force arm can effectively reduce the driving force of the first motor 24, which can effectively reduce the required performance parameters of the first motor 24 and reduce the cost of use.
  • the solid raw materials are put into the discharge funnel and the solid raw materials pass through the discharge funnel.
  • the solid raw materials entering the grinding funnel 21 will be ground by the high-speed rotating grinding body 22 and the grinding funnel 21. Since the top of the grinding body 22 is arranged in a conical surface, there is a gap between the grinding body 22 and the grinding funnel 21. The gap gradually decreases from top to bottom, so that the solid raw material can be coarsely ground first, then finely ground, and finally ground into powder and dropped from the bottom of the grinding funnel 21.
  • the fan 31 When the raw materials are being ground, the fan 31 is connected to operate, and the fan 31 blows air into the cavity 32, so that the air passes through the exhaust port 33 and is discharged at a high speed. Since the exhaust port 33 is arranged in the grinding At the bottom of the funnel 21, the high-speed airflow discharged through the exhaust port 33 can blow the solid chemical raw materials ground into powder, causing the powdered chemical raw materials to sway with the wind, and realize the drop-point drop value of the liquid raw materials.
  • the submersible pump 42 When the raw materials are being ground, the submersible pump 42 is turned on so that the submersible pump 42 draws liquid from the kettle body 1 and passes the liquid through the liquid storage chamber 41 and the atomizing nozzle 45. Atomized spraying, through the combination of atomized liquid and powdered chemical raw materials, can effectively accelerate the sinking of powdered chemical raw materials, and can effectively prevent the powdered chemical raw materials from flowing out from the discharge funnel, submersible pump 42 When absorbing liquid, it will generate adsorption force for the solid chemical raw materials precipitated in the kettle body 1, which can effectively prevent the solid chemical raw materials from settling at the bottom of the inner cavity of the kettle body 1.
  • the solid raw materials can float in the liquid raw materials, thereby accelerating the solid raw materials.
  • the dissolution of the solid chemical raw materials with larger particles can be blocked by the setting of the filter screen 48, effectively preventing the solid chemical raw materials with larger particles from entering into the atomizing nozzle 45 and causing the atomizing nozzle 45 to be blocked; here, the filter screen 48 is used.
  • the solid chemical raw material particles are extremely small and will not cause clogging of the atomizing nozzle 45.
  • the second motor 51 When the raw materials are being ground, the second motor 51 is turned on and runs. The second motor 51 will drive the stirring shaft 52 and the stirring blade 54 to rotate through the second transmission mechanism 53. The stirring blade 54 can achieve The mixed raw materials are stirred laterally, and the liquid pumping and atomizing mechanism 4 is used to drive the mixed raw materials to turn up and down, and the mixed raw materials are stirred laterally through the stirring blades 54, thereby effectively increasing the probability of the raw materials hitting each other, and thereby effectively increasing the raw materials. Mixing effect between.
  • the third motor 61 When the raw material is being ground, the third motor 61 is turned on. When the third motor 61 is running, it can drive the rotating block 62 and the scraper 63 to rotate synchronously. Since the scraper 63 and the filter The bottom of the screen 48 is in contact with each other, and the rotating scraper 63 can scrape the bottom of the filter screen 48 to effectively prevent solid chemical raw materials with larger particles from clogging the filter screen 48 .

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Food Science & Technology (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

化工生产用高效混合反应釜,包括釜体(1),釜体(1)顶部设置有研磨机构(2)、以及送风机构(3),送风机构(3)设置在研磨机构(2)底部,釜体(1)内腔设置有抽液雾化机构(4)。通过研磨机构(2)将固体原料研磨成粉末状落下,固体原料落下时通过送风机构(3)进行吹拂,使粉末状的固体原料随风飘摇,最终实现多落点式地落在液体原料内。通过抽液雾化机构(4)将釜体(1)底部的液体抽出雾化,再回落,可有效地对混合原料进行翻动,同时可带动漂浮的粉末状的化工原料下沉。

Description

化工生产用高效混合反应釜 技术领域
本发明涉及反应釜技术领域,尤其涉及化工生产用高效混合反应釜。
背景技术
反应釜的广义理解即有物理或化学反应的容器,通过对容器的结构设计与参数配置,实现工艺要求的加热、蒸发、冷却及低高速的混配功能,反应釜广泛应用于石油、化工、橡胶、农药、染料、医药和食品等领域,是用来完成硫化、硝化、氢化、烃化、聚合、缩合等工艺过程的压力容器,例如反应器、反应锅、分解锅、聚合釜等;材质一般有碳锰钢、不锈钢、锆、镍基合金及其它复合材料。
现有技术存在以下不足:现有技术的化工生产用反应釜大多是将固体化工原料直接加入至反应釜内,由于固体化工原料进入至反应釜内时大多堆积在一片区域,溶解时需要逐层溶解,且一些固体化工原料颗粒较大,与液体的接触总面积较小,需要花费较长的时间溶解,从而导致原料的混合速率大大降低,其次,由于反应釜内的化工原料混合时大多是水平搅动,翻动效果较差,且一些固体化工原料容易沉淀在反应釜底部,从而导致原料的混合速率进一步降低。
发明内容
本发明针对现有技术的不足,提供了化工生产用高效混合反应釜。
本发明通过以下技术手段实现解决上述技术问题的:化工生产用高效混合反应釜,包括釜体,所述釜体顶部设置有研磨机构、以及送风机构, 所述送风机构设置在研磨机构底部,所述釜体内腔设置有抽液雾化机构;送风机构对研磨成粉末状的化工原料进行吹拂,抽液雾化机构将釜体底部的液体抽出雾化,通过雾化后的液体带动漂浮的粉末状的化工原料下沉。
优选的,所述研磨机构包括连接在釜体内腔顶部的研磨漏斗、设置在研磨漏斗内侧的研磨体、连接在研磨体顶部的转轴、固定设置在釜体顶部的第一电机、以及连接在第一电机与转轴之间的第一传动机构,所述转轴通过轴承与釜体转动连接。
优选的,所述研磨体顶部呈锥形面设置,所述研磨体与研磨漏斗之间的间隙由上至下逐渐减小,所述第一传动机构包括连接在第一电机输出轴外部的主动齿轮、以及连接在转轴外部的从动齿轮,所述主动齿轮与从动齿轮相啮合。
优选的,所述送风机构包括连接在釜体一侧的风机、设置在釜体内腔的空腔、以及连接在空腔端部的排气口,所述风机出风端与空腔相连接,所述排气口设置在研磨漏斗下料口底部。
优选的,所述抽液雾化机构包括设置在釜体内腔顶部的储液腔与潜水泵、设置在釜体内腔底部的环形腔,设置在环形腔外侧呈环形阵列分布的空心罩、连接在储液腔底部呈环形阵列分布的雾化喷头、连接在潜水泵与储液腔之间的排液管、连接在潜水泵与环形腔之间的吸液管、连接在空心罩底部的滤网、以及连接在环形腔与空心罩之间的连接管。
优选的,所述釜体内腔两侧均设置有搅拌机构,所述搅拌机构包括连接在釜体一侧的第二电机、转动连接在釜体内腔的搅拌轴、连接在第二电机输出轴与搅拌轴之间的第二传动机构、以及连接在搅拌轴外部由上至下 均匀分布的搅拌叶。
优选的,所述第二传动机构包括连接在第二电机输出轴端部的主动伞齿轮、以及连接在搅拌轴外部的从动伞齿轮,所述主动伞齿轮与从动伞齿轮相啮合。
优选的,所述釜体底部设置有刮料机构,所述刮料机构包括连接在釜体底部的第三电机、设置在釜体内腔底部的转动块、以及连接在转动块外部呈环形阵列分布的刮条,所述刮条与滤网底部相贴合。
本发明的有益效果:
1、本发明通过向釜体内加注液体原料,随后通过研磨机构对投放的固体原料进行研磨,使固体原料被研磨成粉末状落下,固体原料落下时通过送风机构进行吹拂,使粉末状的固体原料随风飘摇,最终实现多落点式地落在液体原料内,可有效地防止固体原料堆积,加速原料之间的混合,将固体原料研磨后可增加原料与液体之间的接触面积,从而可再次加快固体原料与液体的混合速率;
2、在固体原料下落过程中,通过抽液雾化机构将釜体底部的液体抽出雾化,再回落,可有效地对混合原料进行翻动,防止固体原料堆积在釜体内腔底部,可进一步加快固体原料与液体的混合速率,通过喷出的雾化后的液体可带动漂浮的粉末状的化工原料下沉,不仅可使固体原料快速地落至液体原料内,同时可有效地防止粉末状的化工原料从釜体内流出,有效地避免固体原料流出浪费,同时有效地防止粉末状的化工原料流出对周围环境造成一定的影响。
附图说明
图1为本发明的整体结构示意图;
图2为本发明中图1的A部放大图;
图3为本发明储液腔与雾化喷头的仰视图;
图4为本发明转动块与刮条的俯视图;
图5为本发明的使用场景图。
图中:1、釜体;2、研磨机构;21、研磨漏斗;22、研磨体;23、转轴;24、第一电机;25、第一传动机构;251、主动齿轮;252、从动齿轮;3、送风机构;31、风机;32、空腔;33、排气口;4、抽液雾化机构;41、储液腔;42、潜水泵;43、环形腔;44、空心罩;45、雾化喷头;46、排液管;47、吸液管;48、滤网;49、连接管;5、搅拌机构;51、第二电机;52、搅拌轴;53、第二传动机构;531、主动伞齿轮;532、从动伞齿轮;54、搅拌叶;6、刮料机构;61、第三电机;62、转动块;63、刮条。
具体实施方式
为使本发明实施例的目的、技术方案和优点更加清楚,下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。
需要说明的是,当元件被称为“固定于”另一个元件,它可以直接在另一个元件上或者也可以存在居中的元件。当一个元件被认为是“连接”另一个元件,它可以是直接连接到另一个元件或者可能同时存在居中元件。
实施例
请参阅图1至图5所示,本实施例化工生产用高效混合反应釜,包括釜体1,釜体1顶部设置有研磨机构2、以及送风机构3,送风机构3设置在研磨机构2底部,釜体1内腔设置有抽液雾化机构4;送风机构3对研磨成粉末状的化工原料进行吹拂,抽液雾化机构4将釜体1底部的液体抽出雾化,通过雾化后的液体带动漂浮的粉末状的化工原料下沉;
请参阅图1至图5所示,先向釜体1内加注液体原料,随后通过研磨机构2对投放的固体原料进行研磨,使固体原料被研磨成粉末状落下,固体原料落下时通过送风机构3进行吹拂,使粉末状的固体原料随风飘摇,最终实现多落点式地落在液体原料内,可有效地防止固体原料堆积,加速原料之间的混合,将固体原料研磨后可增加原料与液体之间的接触面积,从而可再次加快固体原料与液体的混合速率,在固体原料下落过程中,通过抽液雾化机构4将釜体1底部的液体抽出雾化,再回落,可有效地对混合原料进行翻动,防止固体原料堆积在釜体1内腔底部,可进一步加快固体原料与液体的混合速率,通过喷出的雾化后的液体可带动漂浮的粉末状的化工原料下沉,不仅可使固体原料快速地落至液体原料内,同时可有效地防止粉末状的化工原料从釜体1内流出,有效地避免固体原料流出浪费,同时有效地防止粉末状的化工原料流出对周围环境造成一定的影响。
请参阅图1与图5所示,接通第一电机24运行,第一电机24将通过第一传动机构25带动研磨体22高速转动,此处的第一传动机构25为主动齿轮251与从动齿轮252,由图1与图5所示,主动齿轮251的直径大于从动齿轮252齿轮的直径,从而通过主动齿轮251可加速从动齿轮252的转动,同时第一传动机构25的设置可增加屈动力臂,有效地降低第一电机24 的驱动力,可有效地降低第一电机24所需的性能参数,降低使用成本,将固体原料经下料漏斗投放,使固体原料经过下料漏斗进入至研磨漏斗21内,进入至研磨漏斗21内的固体原料会被高速转动的研磨体22与研磨漏斗21研磨,由于研磨体22顶部呈锥形面设置,研磨体22与研磨漏斗21之间的的间隙由上至下逐渐减小,从而可实现对固体原料先粗研磨,在细研磨,最终研磨成粉末状经研磨漏斗21底部落下。
请参阅图1与图5所示,原料在研磨时,接通风机31运行,通过风机31向空腔32内吹风,使空气经过排气口33后高速排出,由于排气口33设置在研磨漏斗21底部,从而通过排气口33排出的高速气流可实现对研磨成粉末状的固体化工原料进行吹拂,使粉末状的化工原料随风飘摇,实现对落点式降落值液体原料内。
请参阅图1至图3、以及图5所示,原料在研磨时,接通潜水泵42,使潜水泵42从釜体1内抽液,将液体经过储液腔41以及雾化喷头45后雾化喷出,通过雾化后的液体与粉末状的化工原料结合,可有效地加快粉末状的化工原料下沉,通过可有效地防止粉末状的化工原料从下料漏斗外流,潜水泵42在吸液时会对釜体1沉淀的固体化工原料产生吸附力,可有效地防止固体化工原料沉淀在釜体1内腔底部,同时可使固体原料在液体原料内浮动,从而可加速固体原料的溶解,滤网48的设置可对颗粒较大的固体化工原料进行阻隔,有效地防止颗粒较大的固体化工原料进入至雾化喷头45内导致雾化喷头45堵塞;此处通过滤网48的固体化工原料颗粒极小,不会对雾化喷头45造成堵塞。
请参阅图1与图5所示,原料在研磨时,接通第二电机51运行,第二 电机51将通过第二传动机构53驱动搅拌轴52以及搅拌叶54转动,通过搅拌叶54可实现对混合原料进行横向搅拌,通过抽液雾化机构4带动混合原料进行上下翻动,通过搅拌叶54对混合原料横向搅拌,从而可有效地增大原料相互撞击的几率,进而可有效地的提高原料之间的混合效果。
请参阅图1、图4、以及图5所示,原料在研磨时,接通第三电机61,第三电机61运行时可带动转动块62与刮条63同步转动,由于刮条63与滤网48底部相贴合,通过转动的刮条63可对滤网48底部进行刮动,有效地防止颗粒较大的固体化工原料对滤网48造成堵塞。
需要说明的是,在本文中,如若存在第一和第二等之类的关系术语仅仅用来将一个实体或者操作与另一个实体或操作区分开来,而不一定要求或者暗示这些实体或操作之间存在任何这种实际的关系或者顺序。而且,术语“包括”、“包含”或者其任何其他变体意在涵盖非排他性的包含,从而使得包括一系列要素的过程、方法、物品或者设备不仅包括那些要素,而且还包括没有明确列出的其他要素,或者是还包括为这种过程、方法、物品或者设备所固有的要素。在没有更多限制的情况下,由语句“包括一个……”限定的要素,并不排除在包括所述要素的过程、方法、物品或者设备中还存在另外的相同要素。
以上实施例仅用以说明本发明的技术方案,而非对其限制;尽管参照前述实施例对本发明进行了详细的说明,本领域的普通技术人员应当理解:其依然可以对前述各实施例所记载的技术方案进行修改,或者对其中部分技术特征进行等同替换;而这些修改或者替换,并不使相应技术方案的本质脱离本发明各实施例技术方案的精神和范围。

Claims (8)

  1. 化工生产用高效混合反应釜,包括釜体(1),其特征在于:所述釜体(1)顶部设置有研磨机构(2)、以及送风机构(3),所述送风机构(3)设置在研磨机构(2)底部,所述釜体(1)内腔设置有抽液雾化机构(4);送风机构(3)对研磨成粉末状的化工原料进行吹拂,抽液雾化机构(4)将釜体(1)底部的液体抽出雾化,通过雾化后的液体带动漂浮的粉末状的化工原料下沉。
  2. 根据权利要求1所述的化工生产用高效混合反应釜,其特征在于:所述研磨机构(2)包括连接在釜体(1)内腔顶部的研磨漏斗(21)、设置在研磨漏斗(21)内侧的研磨体(22)、连接在研磨体(22)顶部的转轴(23)、固定设置在釜体(1)顶部的第一电机(24)、以及连接在第一电机(24)与转轴(23)之间的第一传动机构(25),所述转轴(23)通过轴承与釜体(1)转动连接。
  3. 根据权利要求2所述的化工生产用高效混合反应釜,其特征在于:所述研磨体(22)顶部呈锥形面设置,所述研磨体(22)与研磨漏斗(21)之间的的间隙由上至下逐渐减小,所述第一传动机构(25)包括连接在第一电机(24)输出轴外部的主动齿轮(251)、以及连接在转轴(23)外部的从动齿轮(252),所述主动齿轮(251)与从动齿轮(252)相啮合。
  4. 根据权利要求2所述的化工生产用高效混合反应釜,其特征在于:所述送风机构(3)包括连接在釜体(1)一侧的风机(31)、设置在釜体(1)内腔的空腔(32)、以及连接在空腔(32)端部的排气口(33),所述风机(31)出风端与空腔(32)相连接,所述排气口(33)设置在研磨漏斗(21)下料口底部。
  5. 根据权利要求1所述的化工生产用高效混合反应釜,其特征在于:所述抽液雾化机构(4)包括设置在釜体(1)内腔顶部的储液腔(41)与潜水泵(42)、设置在釜体(1)内腔底部的环形腔(43),设置在环形腔(43)外侧呈环形阵列分布的空心罩(44)、连接在储液腔(41)底部呈环形阵列分布的雾化喷头(45)、连接在潜水泵(42)与储液腔(41)之间的排液管(46)、连接在潜水泵(42)与环形腔(43)之间的吸液管(47)、连接在空心罩(44)底部的滤网(48)、以及连接在环形腔(43)与空心罩(44)之间的连接管(49)。
  6. 根据权利要求1所述的化工生产用高效混合反应釜,其特征在于:所述釜体(1)内腔两侧均设置有搅拌机构(5),所述搅拌机构(5)包括连接在釜体(1)一侧的第二电机(51)、转动连接在釜体(1)内腔的搅拌轴(52)、连接在第二电机(51)输出轴与搅拌轴(52)之间的第二传动机构(53)、以及连接在搅拌轴(52)外部由上至下均匀分布的搅拌叶(54)。
  7. 根据权利要求6所述的化工生产用高效混合反应釜,其特征在于:所述第二传动机构(53)包括连接在第二电机(51)输出轴端部的主动伞齿轮(531)、以及连接在搅拌轴(52)外部的从动伞齿轮(532),所述主动伞齿轮(531)与从动伞齿轮(532)相啮合。
  8. 根据权利要求5所述的化工生产用高效混合反应釜,其特征在于:所述釜体(1)底部设置有刮料机构(6),所述刮料机构(6)包括连接在釜体(1)底部的第三电机(61)、设置在釜体(1)内腔底部的转动块(62)、以及连接在转动块(62)外部呈环形阵列分布的刮条(63),所述刮条(63)与滤网(48)底部相贴合。
PCT/CN2022/129521 2022-05-17 2022-11-03 化工生产用高效混合反应釜 WO2023221411A1 (zh)

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