WO2012138108A1 - Natural antiseptic deodorizer - Google Patents

Natural antiseptic deodorizer Download PDF

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Publication number
WO2012138108A1
WO2012138108A1 PCT/KR2012/002510 KR2012002510W WO2012138108A1 WO 2012138108 A1 WO2012138108 A1 WO 2012138108A1 KR 2012002510 W KR2012002510 W KR 2012002510W WO 2012138108 A1 WO2012138108 A1 WO 2012138108A1
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Prior art keywords
extract
weight
mulberry
essence oil
natural
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PCT/KR2012/002510
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French (fr)
Korean (ko)
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김진홍
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Kim Jin-Hong
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Publication of WO2012138108A1 publication Critical patent/WO2012138108A1/en

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9755Gymnosperms [Coniferophyta]
    • A61K8/9767Pinaceae [Pine family], e.g. pine or cedar
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q15/00Anti-perspirants or body deodorants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations

Definitions

  • the present invention includes a natural plant extract as an active ingredient, and relates to a natural bactericidal deodorant which can be usefully used for removing bacteria and fungi, removing odors and combating insects.
  • the deodorant refers to drugs that remove or weaken odors, and are classified into drugs using self-dispersion such as calcium chloride and formalin and drugs using adsorption such as activated carbon.
  • the main raw materials include natural plant materials including herbal medicines such as oak, oleander, zelkova, camellia, oakpigo, elm, plum, donkey, licorice, astragalus, jujube, cheonggung and wormwood.
  • herbal medicines such as oak, oleander, zelkova, camellia, oakpigo, elm, plum, donkey, licorice, astragalus, jujube, cheonggung and wormwood.
  • Liquid deodorants have been disclosed.
  • insecticides are used to exterminate pests such as flies, mosquitoes, cockroaches, ants, etc., which transmit disease to people through food or skin contact.
  • Such insecticides are used in various formulations such as organophosphorus compounds, pyrethroid compounds, carbamate compounds, organochlorine compounds, etc. as emulsions, hydrating agents, aerosols, powders, granules, and the like.
  • organophosphorus compounds such as pyrethroid compounds, carbamate compounds, organochlorine compounds, etc.
  • emulsions such as emulsions, hydrating agents, aerosols, powders, granules, and the like.
  • the principle is that the pesticidal components contained in the insecticide enter the insect body through the skin, breathing or ingestion of the insect, causing neurotoxicity to reach a lethal condition.
  • the pesticide for pest control is a pesticide component, dichlorbose, chloropyriphos, pyridaphenthione, diazinone, rothion, propenophos, etofenprox, cyfemethrin, hycis cyspermeth Organophosphorus, such as lean, cardedin, bifenthrin, alphamethrin, deltamethrin, fenvalinate, alphacyspermethrin, lambdahalosulin, phenpropasrin, beta-cyflurin, flucirinate, etc.
  • One or more selected from among compounds or pyrethroid-based compounds is mixed and used.
  • the present inventors conducted research to develop insecticidal deodorant using natural materials, the composition containing yellow wall extract, mulberry extract, mulberry extract, cedar extract, triticale extract, green tea extract and vegetable ethanol as an active ingredient And it has been found that it can be usefully used for mold removal, odor removal and insect control to complete the present invention.
  • the present invention provides a natural bactericidal deodorant containing oak tree extract, yellow bark extract, mulberry extract, mulberry extract, cedar extract, triticale extract, green tea extract and vegetable ethanol as an active ingredient.
  • Natural bactericidal deodorant according to the present invention does not contain chemicals, fragrances and preservatives, and contains natural plant extracts, etc. as an active ingredient, and therefore has fewer side effects by artificial or synthetic ingredients, and eliminates bacteria, mold, and odors. And because the insect repellent effect is excellent, it can be usefully used as a natural sterilizing deodorant.
  • Figure 1 discloses a process for producing a natural plant extract used as a main component in the natural bactericidal deodorant according to the present invention.
  • the present invention provides a natural bactericidal deodorant containing oak tree extract, yellow bark extract, mulberry extract, mulberry extract, cedar extract, triticale extract, green tea extract, and vegetable ethanol as an active ingredient.
  • the natural bactericidal deodorant is 2 to 8% by weight of the extract of the alpine tree, 5 to 15% by weight of the yellow bark extract, 10 to 20% by weight of the mulberry extract, 15 to 25% by weight of the mulberry extract, 5 to 15% by weight of the cedar extract, triticale extract It is preferable to contain 5 to 15% by weight, green tea extract 10 to 20% by weight and vegetable ethanol 10 to 20% by weight as an active ingredient. It can exhibit the most excellent bactericidal and deodorizing effect in the above content range.
  • the extract may be an extract extracted with a solvent selected from the group consisting of hot water, ethyl acetate, chloroform, hexane, C1-C4 alcohol, and mixtures thereof, and more preferably hot water extract.
  • a solvent selected from the group consisting of hot water, ethyl acetate, chloroform, hexane, C1-C4 alcohol, and mixtures thereof, and more preferably hot water extract.
  • the extract may be an ultrasonic treatment after extraction with a solvent selected from the group consisting of hot water, ethyl acetate, chloroform, hexane, C1-C4 alcohol and mixtures thereof. This sonication can further grind the extract to improve the antimicrobial, sterilization and deodorization efficiency.
  • the extract includes not only the extract by the aforementioned extraction solvent, but also an extract that has undergone a conventional purification process.
  • an active fraction obtained through separation using an ultrafiltration membrane having a constant molecular weight cut-off value, separation by various chromatography, and various purification methods additionally performed may be included in the extract of the present invention.
  • the oak tree extract, yellow wall extract, mulberry extract and mulberry extract is obtained by bark through the cuticle work of yellow wall, mulberry and mulberry, completely dried, aged with mineral water, extracted with a solvent, and prepared by ultrasonic treatment. Can be.
  • the oak tree is a deciduous tree belonging to the Rosaceae, the leaves are shifted, and the edges of the leaves have fine serrates and long egg shapes. Flowers bloom in May with gunshot inflorescences and bloom in white. The fruit of the core fruit ripens in black in June and tastes good. Dried twigs are called Kowloon Mok, which can be used for congestion or by applying fresh juice to the boils on the legs. In July, the leaves are boiled and eaten as herbs, and the fruits are eaten raw. They grow in deep valleys and are distributed more and more toward the north.
  • the yellow wall is also known as the Yellow Tree, which is a deciduous tree belonging to the Rutaceae, its height is about 10m and grows in the area below 1,300m above sea level.
  • the branches are thick and spread in all directions, and the light gray bark has a cork layer that is deeply divided and the inner layer is yellow.
  • Leaves are 5 ⁇ 13 pairs of feather-shaped twigs facing each other with lanceolate.
  • the lanceolate twigs have rounded bottoms, long pointed ends, and have blunt teeth and luster.
  • Fruits are spherical black nucleus about 1cm in diameter. It is distributed in Japan, China, Usuri, and Amur. In Korea, the same Phellodendron, P. molle, with hairs on the back of the leaves, P. insulare with 3 to 5 pairs of leaves, and a broad leaf yellow wall with thin cork layers and light hairs on the leaves ( P. sachalinense) grows. Yellow wall is suitable as a wheat plant, wood is used as veneer, furniture, and wood craft. Bark and fruit are used for typhoid fever, cholera, blood, poisoning, gonorrhea, stamens, diabetes, etc. The name is said because the inner skin is yellow.
  • the mulberry grows up to about 3m in height, its leaves are alternately divided into two or three branches, with fine teeth and thorns on the edges, and thorns on both sides of the leaves.
  • the flowers and the male flowers are grouped separately on a tree.
  • the fruit is round, ripens in June, and has tiny thorns on the outside.
  • the fruit of the mulberry is called the lower room, which is used in the treatment of yang tribe and species. Finely chop roots and decoct before eating to cure Sogal. In addition, it extracts the fiber from the bark and makes window papers. To obtain this window papers, it is planted with paper mulberry. It is distributed all over Korea and grows well on sunny foothills or field banks.
  • the mulberry is called the leaf of the upper leaf, and has the efficacy of breeze, blue heat, nominal, wind-heat, fever, headache, purpose, cures.
  • Mulberry leaves contain flavonoids, rutin, quercetin, isoquercetin, moracetin, and insect transformation hormones inosterone and ecdysterone. It is contained, mulberry leaf extract is known to have a hypoglycemic effect.
  • the cedar extract may be prepared by completely drying the bark through the cuticle work of the cedar, drying it with salt, pulverizing by heating, extracting with a solvent, and sonicating.
  • the cedar tree belongs to the eucommiaceae, and its bark is mainly used as a medicinal herb, which is also called the bark of the soybean.
  • the head of the caterpillar forms a plate, its thickness is about 3-7mm and the size is different.
  • the outer surface is gray or dark gray, the inner surface is smooth, dark purple and the quality is smooth.
  • Crossing the cedar tree produces three white, tough, coarse fibrous fibers.
  • Main components are epithelium, resin and ash.
  • the tofu collected in May-June is poisonous, sweet and spicy. It mainly works in the meridians of the kidneys and liver, and its efficacy is interpolation, iliac bone, and antenatal (to stabilize the fetus).
  • Toothache is mainly used for low back pain, especially for low back pain caused by Xinyangheo. At this time, it is used in combination with fasting, earthenware and breeding. In addition, it is used for lower abdominal pain and genital bleeding during pregnancy due to Xinyangheo, and because the tooth decay has a lactic acid prevention effect, it is used in combination with fasting and the above life, and also used for high blood pressure. At this time, a drug with a coercive effect such as golden, hazel, sanggi, and hyssop should be combined. Since the main function is to control the body by looking at the Yanggi yanggi is not effective for hypertension of the liver condition (pathological phenomenon caused by the lack of control of the liver's positive elements due to lack of liver's positive factors).
  • the triticale extract and green tea extract may be prepared by completely drying the leaves of each of the triticale and green tea and extracting them with a solvent, followed by sonication.
  • the three hundred sec is a perennial herb of the dicotyledonous pepper tree, three hundred perennial, and when the flowers bloom, two to three leaves under the flowers turn white, and the flowers and roots are also white, so they were named three hundred seconds. It is called 'invoice pool' because it has a bitter taste and smells like rotting invoice. I like wet and soft places like mud, and the white rhizome stretches aside. It is a plant with strong vitality and no pests. In early summer, white leaves come out, and at the end of it is a white flower of the shape of Isaac. The stalk is bent at first, but stands straight as the flower blooms. Although it is native to Jeju Island, it is cold and can be overwintered in the central region. Three hundred seconds is excellent anti-cancer action, and strengthens capillaries and is effective in hypertension or arteriosclerosis. Detoxification and diuretic effect is also used as a treatment for nephritis and edema.
  • the green tea is a tea leaf that has not been fermented, and the tea tree is evergreen and relatively warm and grows well in areas with high rainfall. Green tea is known for its powerful anti-cancer effects, inhibition of inflammation, inhibition and alleviation of elevated blood sugar levels, antioxidant activity, dietary effects, heavy metal and nicotine detoxification, fatigue and hangover removal, prevention of acidification of constitution, removal of tooth decay and bad breath, and skin care. have.
  • the vegetable ethanol is preferably a grain fermentation alcohol made by fermenting grains such as rice, barley, sweet potato, sorghum.
  • the natural bactericidal deodorant of the present invention is composed of grapefruit seed extract, sweet seed extract, tea tree essence oil, lemongrass essence oil, citronola essence oil, eucalyptus essence oil, mandarin essence oil, juniper berry essence oil and propolis It may further comprise one or two or more selected from the group.
  • the propolis is also called Russian penicillin, natural penicillin, bees apply propolis in the gaps of the honeycomb to protect themselves from germs and viruses, and prevent invasion of enemies such as wasps and mice.
  • Ingredients are the most organic and minerals (inorganic salts), with 104 kinds of ingredients.
  • Bark of European bird cherry was dried and aged with mineral water, and hot water was extracted at 80-90 °C with purified water. The yellow wall extract was sonicated for 3 minutes and used as a sample.
  • the bark of the Phellodendron amurense and the same plants were dried, aged in mineral water, and extracted with purified water at 80-90 ° C.
  • the yellow wall extract was sonicated for 3 minutes and used as a sample.
  • Bark of the Eucommia ulmoides Oliver was dried, salted, heated, ground and extracted with purified water at 80-90 ° C. The larvae extract was sonicated for 3 minutes and used as a sample.
  • the dried leaves of green tea were extracted with purified water at 80-90 ° C.
  • the green tea extract was sonicated for 3 minutes and used as a sample.
  • mulberry Stems and root bark of mulberry (Morus alba L.), Mulberry (Morus bombycis Koidzumi) or other similar plants (Moraceae) were dried, aged in mineral water and extracted with hot water at 80-90 ° C with purified water. The mulberry extract was sonicated for 3 minutes and used as a sample.
  • Burberry Stems or roots of Burberry (Broussonetia kazinoki) and related plants (Moraceae) were dried and aged with mineral water and extracted with hot water at 80-90 ° C with purified water. The mulberry extract was sonicated for 3 minutes and used as a sample.
  • Dry leaves of three hundred (Saururus chinensis) were extracted with purified water at 80-90 °C.
  • the 300 sec extract was sonicated for 3 minutes and used as a sample.
  • Example 1 Component (weight (g)) efficacy
  • Example 2 Example 3 Rhubarb Extract Antibacterial, sterilization, fungus, deodorization 4 6 8 Yellow Wall Extract Antibacterial, sterilization, fungus, deodorization 10 9 8 Cedar extract Antibacterial 16 15 14 Green tea extract Sterilization, detoxification 20 20 20 Mulberry Extract Antibacterial, anti-inflammatory 9 9 9 9 Paper mulberry extract Antibacterial, anti-inflammatory, detoxification 8 8 8 Three hundred seconds Antiseptic, antibacterial 15 15 15 15 Vegetable Ethanol (Oil) Sterilization, Disinfection 15 15 15 15 Grapefruit Seed Extract Antibacterial, antiseptic 1.1 1.1 1.1 Peony Seed Extract Antibacterial, anti-inflammatory One One One Tea tree essence oil Antiseptic, antibacterial 0.05 0.05 0.05 Lemongrass Essence Oil Sterilization, antiseptic 0.5 0.5 0.5 Citronola Essence Oil Sterilization, insect repellent 0.05 0.05 0.05 Eucalyptus essence oil Antibacterial, antiviral 0.05 0.05 0.05 Mandarin Essence
  • the antifungal test was performed by evaluating the bactericidal effect on the fungi infected in the plywood after the treatment of the natural bactericidal deodorant. That is, the sterilization operation was performed by spraying the natural sterilization deodorant prepared in Examples 1 to 3 on the plywood. Non-sterile plywood was also prepared for the control. The finished plywood was wrapped to prevent other contamination. After 24 hours, bacteria were collected from each plywood with cotton swabs and incubated at 37 ° C. for up to 3 days and at room temperature for 6 days. The above work was performed three, six and nine days later. At this time, a dextrose medium was used as a culture medium.
  • the bactericidal effect was maintained until 3 days after the sterilization treatment of the natural sterilizing deodorant according to the embodiment, but after 6 days the fungal growth occurred. A few fungi grew before the sterilization treatment (see Table 2).

Abstract

The present invention relates to a natural antiseptic deodorizer and said natural antiseptic deodorizer is a composition comprising naturally-derived plant extracts such as Prunus padus L. extract, Phellodendron amurense Rupr. extract, Broussonetia kazinoki Sieb. extract, mulberry extract, Eucommia ulmoides OLIV. extract, Saururus chinensis BAILL. extract, green tea extract and bioethanol as active ingredients. While not containing chemicals, perfumes and preservatives and thus being very safe, the composition has excellent bacteria and fungi removal, odor removal and insect extermination effects, and thus can be useful as a natural antiseptic deodorizer.

Description

천연 살균 탈취제Natural Sterilization Deodorant
본 발명은 천연 식물 추출물을 유효성분으로 포함하며, 세균 및 곰팡이 제거, 냄새 제거, 곤충퇴치에 유용하게 사용될 수 있는 천연 살균 탈취제에 관한 것이다. The present invention includes a natural plant extract as an active ingredient, and relates to a natural bactericidal deodorant which can be usefully used for removing bacteria and fungi, removing odors and combating insects.
일반적으로 탈취제라 함은 악취를 제거하거나 약하게 하는 약제를 말하며, 크게 염화칼슘, 포르말린 등과 같이 자체방산을 이용한 약제와 활성탄 등과 같이 흡착 작용을 이용한 약제로 분류된다.In general, the deodorant refers to drugs that remove or weaken odors, and are classified into drugs using self-dispersion such as calcium chloride and formalin and drugs using adsorption such as activated carbon.
최근에는 탈취제의 원료로서 용도가 한정되는 고상의 활성탄이나 인체에 유독성을 갖는 방향성 화학물질의 사용이 줄어들면서, 천연식물재료를 원료로 하여 인체에 무해하면서 살균효과까지 갖는 탈취제가 개발되고 있다.Recently, as the use of solid activated carbon and aromatic chemicals toxic to humans has been reduced as a raw material for deodorizing agents, deodorants having natural plant materials as raw materials and harmless to the human body have been developed.
대한민국 특허 제337148호에서는 주원료로서 엄나무, 행정피나무, 제피나무, 동백나무, 오갈피나무, 누릅나무, 매실, 당귀, 감초, 황기, 대추나무, 천궁, 약쑥 등과 같은 한약재를 포함하는 천연식물재료를 사용한 액상의 탈취제를 개시한 바 있다.In Korean Patent No. 337148, the main raw materials include natural plant materials including herbal medicines such as oak, oleander, zelkova, camellia, oakpigo, elm, plum, donkey, licorice, astragalus, jujube, cheonggung and wormwood. Liquid deodorants have been disclosed.
한편, 음식이나 피부접촉을 통하여 사람들에게 병을 옮기는 파리, 모기, 바퀴벌레, 개미 등과 같은 방역해충을 박멸하기 위하여 살충제를 사용하게 된다.On the other hand, insecticides are used to exterminate pests such as flies, mosquitoes, cockroaches, ants, etc., which transmit disease to people through food or skin contact.
이러한 살충제는 주요성분으로서 유기인계 화합물, 피레스로이드계 화합물, 카바메이트계 화합물, 유기염소계 화합물 등을 유제, 수화제, 에어로솔제, 분제, 입제 등과 같은 다양한 제제형태로 사용되고 있으며, 이에 따라 사용되는 용도도 각기 다르지만, 그 원리는 살충제에 포함되어 있는 살충성분이 곤충의 피부나 호흡 또는 섭취를 통하여 곤충 체내로 들어가 신경 독성을 야기함으로써 치사상태에 이르도록 하는 것이 일반적인 살충기전이다.Such insecticides are used in various formulations such as organophosphorus compounds, pyrethroid compounds, carbamate compounds, organochlorine compounds, etc. as emulsions, hydrating agents, aerosols, powders, granules, and the like. Although different, the principle is that the pesticidal components contained in the insecticide enter the insect body through the skin, breathing or ingestion of the insect, causing neurotoxicity to reach a lethal condition.
상기한 다양한 살충제에 있어서, 방역용 살충제는 살충성분으로 디클로르보스, 클로로피리포스, 피리다펜치온, 다이아지논, 로치온, 프로페노포스, 에토펜프록스, 싸이페메스린, 하이씨스 싸이퍼메스린, 카데스린, 비펜스린, 알파메스린, 델타메스린, 펜발리네이트, 알파싸이퍼메스린, 람다싸이할로스린, 펜프로파스린, 베타싸이플루스린, 플루싸이스린레이트 등의 유기인계 화합물 또는 피레스로이드계 화합물들 중에서 1종 이상을 선택하여 혼합된 것을 사용한다.In the various pesticides described above, the pesticide for pest control is a pesticide component, dichlorbose, chloropyriphos, pyridaphenthione, diazinone, rothion, propenophos, etofenprox, cyfemethrin, hycis cyspermeth Organophosphorus, such as lean, cardedin, bifenthrin, alphamethrin, deltamethrin, fenvalinate, alphacyspermethrin, lambdahalosulin, phenpropasrin, beta-cyflurin, flucirinate, etc. One or more selected from among compounds or pyrethroid-based compounds is mixed and used.
이러한 방역용 살충제들이 사용되는 장소로는 재래식 또는 간이 화장실, 쓰레기 하차장이나 매립장, 하수구 등과 같이 대부분이 먹이와 악취를 수반하는 곳으로, 이러한 곳에 파리나 모기를 비롯한 방역해충들이 밀집해 있기 때문이다.Where pesticides are used, conventional or simple toilets, garbage dumps, landfills, sewers, etc., most of them are accompanied by food and odors, such as flies, mosquitoes and other pests are concentrated.
그러나 이와 같이 악취가 수반되는 장소에 살충제를 사용하여 해충들을 박멸하기는 하나, 해충들을 유인하는 근본적인 악취는 제거되지 않아 일정 시일이 지나면 다시 해충들이 모여들게 되고, 이러한 해충들이 다시 병균들을 퍼트리는 악순환이 계속된다는 문제점이 있었다.However, while insecticides are used to destroy pests in places where odors are involved, the fundamental odor that attracts pests is not eliminated, and after a certain period of time, pests gather again, and the vicious cycle of spreading germs again There was a problem going on.
또한, 대부분의 살충제 성분들은 역한 냄새를 동반하기 때문에 방역하는 사람들이 다량의 살충제를 흡입하게 되면 메스꺼움을 느낄 수 있고, 따라서 작업성이 좋지 않다는 문제점도 있었다.In addition, since most insecticide components are accompanied by an inverse smell, the pesticides may feel nauseous when they inhale a large amount of insecticide, and thus there is a problem in that workability is not good.
따라서, 방역시 악취를 제거함과 동시에 해충들을 박멸할 수 있는 천연 살충 탈취제 조성물의 개발이 절실한 실정이다.Therefore, there is an urgent need to develop a natural insecticidal deodorant composition capable of removing odors at the same time as pest control and at the same time exterminate pests.
이에, 본 발명자는 천연 소재를 이용하여 살충 탈취제를 개발하고자 연구 노력한 결과, 황벽나무 추출물, 닥나무 추출물, 뽕나무 추출물, 두충나무 추출물, 삼백초 추출물, 녹차 추출물 및 식물성 에탄올을 유효성분으로 함유하는 조성물이 세균 및 곰팡이 제거, 냄새 제거 및 곤충퇴치에 유용하게 사용될 수 있다는 점을 밝혀내어 본 발명을 완성하였다.Therefore, the present inventors conducted research to develop insecticidal deodorant using natural materials, the composition containing yellow wall extract, mulberry extract, mulberry extract, cedar extract, triticale extract, green tea extract and vegetable ethanol as an active ingredient And it has been found that it can be usefully used for mold removal, odor removal and insect control to complete the present invention.
본 발명의 목적은 세균 및 곰팡이 제거, 냄새 제거 및 곤충퇴치에 유용하게 사용될 수 있는 천연 살균 탈취제를 제공하는 데에 있다.It is an object of the present invention to provide a natural bactericidal deodorant which can be usefully used for bacterial and mold removal, odor removal and insect control.
상기 목적을 달성하기 위하여, 본 발명은 귀룽나무 추출물, 황벽나무 추출물, 닥나무 추출물, 뽕나무 추출물, 두충나무 추출물, 삼백초 추출물, 녹차 추출물 및 식물성 에탄올을 유효성분으로 함유하는 천연 살균 탈취제를 제공한다.In order to achieve the above object, the present invention provides a natural bactericidal deodorant containing oak tree extract, yellow bark extract, mulberry extract, mulberry extract, cedar extract, triticale extract, green tea extract and vegetable ethanol as an active ingredient.
본 발명에 따른 천연 살균 탈취제는 화학물질, 향료 및 방부제를 포함하지 않고 천연으로부터 유래한 식물 추출물 등을 유효성분으로 함유하므로 인공 또는 합성 성분들에 의한 부작용이 적으며, 세균 및 곰팡이 제거, 냄새 제거 및 곤충퇴치 효과가 탁월하므로 천연 살균 탈취제로서 유용하게 사용될 수 있다. Natural bactericidal deodorant according to the present invention does not contain chemicals, fragrances and preservatives, and contains natural plant extracts, etc. as an active ingredient, and therefore has fewer side effects by artificial or synthetic ingredients, and eliminates bacteria, mold, and odors. And because the insect repellent effect is excellent, it can be usefully used as a natural sterilizing deodorant.
도 1은 본 발명에 따른 천연 살균 탈취제에 주성분으로 사용되는 천연 식물 추출물을 제조하는 공정을 개시한 것이다.Figure 1 discloses a process for producing a natural plant extract used as a main component in the natural bactericidal deodorant according to the present invention.
본 발명은 귀룽나무 추출물, 황벽나무 추출물, 닥나무 추출물, 뽕나무 추출물, 두충나무 추출물, 삼백초 추출물, 녹차 추출물 및 식물성 에탄올을 유효성분으로 함유하는 천연 살균 탈취제를 제공한다.The present invention provides a natural bactericidal deodorant containing oak tree extract, yellow bark extract, mulberry extract, mulberry extract, cedar extract, triticale extract, green tea extract, and vegetable ethanol as an active ingredient.
상기 천연 살균 탈취제는 귀룽나무 추출물 2 내지 8 중량%, 황벽나무 추출물 5 내지 15 중량%, 닥나무 추출물 10 내지 20 중량%, 뽕나무 추출물 15 내지 25 중량%, 두충나무 추출물 5 내지 15 중량%, 삼백초 추출물 5 내지 15 중량%, 녹차 추출물 10 내지 20 중량% 및 식물성 에탄올 10 내지 20 중량%를 유효성분으로 함유하는 것이 바람직하다. 상기 함량 범위에서 가장 뛰어난 살균 및 탈취 효과를 나타낼 수 있다.The natural bactericidal deodorant is 2 to 8% by weight of the extract of the alpine tree, 5 to 15% by weight of the yellow bark extract, 10 to 20% by weight of the mulberry extract, 15 to 25% by weight of the mulberry extract, 5 to 15% by weight of the cedar extract, triticale extract It is preferable to contain 5 to 15% by weight, green tea extract 10 to 20% by weight and vegetable ethanol 10 to 20% by weight as an active ingredient. It can exhibit the most excellent bactericidal and deodorizing effect in the above content range.
상기 추출물은 열수, 에틸아세테이트, 클로로포름, 헥산, C1-C4 알코올 및 이들의 혼합물로 이루어진 군에서 선택된 용매로 추출한 추출물일 수 있으며, 보다 바람직하게는 열수 추출물일 수 있다.The extract may be an extract extracted with a solvent selected from the group consisting of hot water, ethyl acetate, chloroform, hexane, C1-C4 alcohol, and mixtures thereof, and more preferably hot water extract.
또한, 상기 추출물은 열수, 에틸아세테이트, 클로로포름, 헥산, C1-C4 알코올 및 이들의 혼합물로 이루어진 군에서 선택된 용매로 추출한 후, 초음파 처리한 추출물일 수 있다. 이러한 초음파 처리는 추출물을 보다 잘게 분쇄하여 항균, 살균 및 탈취 효율을 향상시킬 수 있다.In addition, the extract may be an ultrasonic treatment after extraction with a solvent selected from the group consisting of hot water, ethyl acetate, chloroform, hexane, C1-C4 alcohol and mixtures thereof. This sonication can further grind the extract to improve the antimicrobial, sterilization and deodorization efficiency.
또한, 상기 추출물은 상술한 추출 용매에 의한 추출물 뿐만 아니라, 통상적인 정제 과정을 거친 추출물도 포함한다. 예컨대, 일정한 분자량 컷-오프 값을 갖는 한외여과막을 이용한 분리, 다양한 크로마토그래피에 의한 분리, 추가적으로 실시된 다양한 정제 방법을 통해 얻어진 활성 분획도 본 발명의 추출물에 포함될 수 있다.In addition, the extract includes not only the extract by the aforementioned extraction solvent, but also an extract that has undergone a conventional purification process. For example, an active fraction obtained through separation using an ultrafiltration membrane having a constant molecular weight cut-off value, separation by various chromatography, and various purification methods additionally performed may be included in the extract of the present invention.
상기 귀룽나무 추출물, 황벽나무 추출물, 닥나무 추출물 및 뽕나무 추출물은 황벽나무, 닥나무 및 뽕나무 각각의 표피 작업을 통해 수피를 얻은 후 완전 건조시키며, 광천수로 숙성시킨 후 용매로 추출하며, 초음파 처리하여 제조할 수 있다.The oak tree extract, yellow wall extract, mulberry extract and mulberry extract is obtained by bark through the cuticle work of yellow wall, mulberry and mulberry, completely dried, aged with mineral water, extracted with a solvent, and prepared by ultrasonic treatment. Can be.
상기 귀룽나무는 장미과(Rosaceae)에 속하는 낙엽교목으로서, 잎은 어긋나고 잎가장자리에는 잔 톱니가 있으며 긴 달걀 모양으로 생겼다. 꽃은 5월에 총상꽃차례로 무리져서 하얗게 피며 꽃줄기는 밑으로 약간 처진다. 핵과인 열매는 6월에 동그랗게 검은색으로 익으며 맛이 떫다. 작은 가지 말린 것을 구룡목이라고 하는데, 체증에 쓰거나 다리에 나는 부스럼에 생즙을 내서 바르면 효과가 있다. 7월에 잎을 삶아서 나물로 먹으며, 열매는 날것으로 먹기도 하는데, 깊은 산골짜기에서 자라며 북쪽으로 갈수록 많이 분포한다고 한다.The oak tree is a deciduous tree belonging to the Rosaceae, the leaves are shifted, and the edges of the leaves have fine serrates and long egg shapes. Flowers bloom in May with gunshot inflorescences and bloom in white. The fruit of the core fruit ripens in black in June and tastes good. Dried twigs are called Kowloon Mok, which can be used for congestion or by applying fresh juice to the boils on the legs. In July, the leaves are boiled and eaten as herbs, and the fruits are eaten raw. They grow in deep valleys and are distributed more and more toward the north.
상기 황벽나무는 황경나무라고도 하는데, 이는 운향과(Rutaceae)에 속하는 낙엽교목로서, 그 키는 10m 정도이며 해발 1,300m 이하 지역에서 자생한다. 가지는 굵고 사방으로 퍼지며 연한 회색의 수피는 코르크층이 발달하여 깊게 갈라지고 내피는 황색이다. 잎은 깃털 모양의 잔잎 5~13쌍이 겹잎으로 마주나는데 피침형의 잔잎은 밑이 둥글고 끝이 길게 뾰족하며 뭉뚝한 톱니와 광택이 있다. 꽃은 6월경 암꽃과 수꽃이 다른 그루에 원추꽃차례를 이루며 핀다. 꽃잎은 5~8개이고 수꽃에는 5~6개의 수술이 있으며 암꽃에는 1개의 암술이 있다. 열매는 지름이 약 1㎝인 구형의 검은색 핵과이다. 일본·중국·우수리·아무르 지역 등에 분포한다. 한국에는 같은 황벽나무속(Phellodendron)이며 잎 뒷면에 털이 많은 털황벽나무(P. molle), 잔잎이 3~5쌍인 섬황벽(P. insulare), 코르크층이 얇고 잎에 연한 털이 적은 넓은잎황벽(P. sachalinense)이 자란다. 황벽나무는 밀원식물로 적당하며 목재는 무늬목·가구재·목공예재로 쓰이고 수피와 열매는 장티푸스·콜레라·토혈·중독·임질·동상·당뇨의 치료 등으로 쓰이며 내피는 노란색의 염료로 사용되는데 황벽이라는 이름은 내피가 노란색이기 때문에 붙여졌다고 한다.The yellow wall is also known as the Yellow Tree, which is a deciduous tree belonging to the Rutaceae, its height is about 10m and grows in the area below 1,300m above sea level. The branches are thick and spread in all directions, and the light gray bark has a cork layer that is deeply divided and the inner layer is yellow. Leaves are 5 ~ 13 pairs of feather-shaped twigs facing each other with lanceolate. The lanceolate twigs have rounded bottoms, long pointed ends, and have blunt teeth and luster. Flowers bloom in June, with female and male flowers forming a conical inflorescence. Petals are 5-8, male flowers have 5-6 stamens, and female flowers have 1 pistil. Fruits are spherical black nucleus about 1cm in diameter. It is distributed in Japan, China, Usuri, and Amur. In Korea, the same Phellodendron, P. molle, with hairs on the back of the leaves, P. insulare with 3 to 5 pairs of leaves, and a broad leaf yellow wall with thin cork layers and light hairs on the leaves ( P. sachalinense) grows. Yellow wall is suitable as a wheat plant, wood is used as veneer, furniture, and wood craft. Bark and fruit are used for typhoid fever, cholera, blood, poisoning, gonorrhea, stamens, diabetes, etc. The name is said because the inner skin is yellow.
상기 닥나무는 그 키가 3m 정도까지 자라는데, 그 잎은 어긋나고 흔히 2~3갈래로 나누어지며 가장자리에는 잔톱니와 가시가 있고, 잎 양쪽에 가는 가시가 달린다. 꽃은 잎이 나올 때 암꽃과 수꽃이 한 나무에 따로따로 무리 지어핀다. 수꽃은 새로 나온 가지의 아래쪽 잎겨드랑이에서 피며 암꽃은 위쪽 잎겨드랑이에서 핀다. 열매는 둥그렇고 6월에 붉은색으로 익으며 겉에는 아주 작은 가시들이 달려 있다. 닥나무의 열매를 저실이라 하는데 이것을 한방에서는 양기부족·수종의 치료에 쓰고 있다. 뿌리를 잘게 썰어 밥 먹기 전에 달여 먹으면 소갈을 치료할 수 있다. 또한 나무껍질 속의 섬유를 뽑아내 창호지를 만드는데 이 창호지를 얻기 위해 닥나무를 심고 있으며 조선시대에는 닥나무 껍질로 만든 종이로 저화라는 돈을 만들어 쓰기도 했다. 한국 전지역에 분포하며, 양지바른 산기슭이나 밭둑에서 잘 자란다고 한다.The mulberry grows up to about 3m in height, its leaves are alternately divided into two or three branches, with fine teeth and thorns on the edges, and thorns on both sides of the leaves. When the leaves come out, the flowers and the male flowers are grouped separately on a tree. A male flower blooms in the lower leaf axle of a new branch, and a female flower blooms in the upper leaf axle. The fruit is round, ripens in June, and has tiny thorns on the outside. The fruit of the mulberry is called the lower room, which is used in the treatment of yang tribe and species. Finely chop roots and decoct before eating to cure Sogal. In addition, it extracts the fiber from the bark and makes window papers. To obtain this window papers, it is planted with paper mulberry. It is distributed all over Korea and grows well on sunny foothills or field banks.
상기 뽕나무는 그 잎을 상엽이라고 하며, 거풍, 청열, 명목의 효능이 있고, 풍온발열, 두통, 목적, 구갈을 치료한다. 뽕나무잎에는 플라보노이드(flavonoid) 성분인 루틴(rutin), 퀘르세틴(quercetin), 이소퀘르세틴(isoquercetin), 모라세틴(moracetin), 곤충 변태 호르몬인 이노코스테론(inokosterone), 엑디스테론(ecdysterone) 등이 함유되어 있으며, 뽕나무잎 추출액은 혈당강하작용효과가 있음이 알려져 있다.The mulberry is called the leaf of the upper leaf, and has the efficacy of breeze, blue heat, nominal, wind-heat, fever, headache, purpose, cures. Mulberry leaves contain flavonoids, rutin, quercetin, isoquercetin, moracetin, and insect transformation hormones inosterone and ecdysterone. It is contained, mulberry leaf extract is known to have a hypoglycemic effect.
상기 두충나무 추출물은 두충나무의 표피 작업을 통해 수피를 얻은 후 완전 건조시키며, 소금에 절인 후 가열하여 분쇄하고, 용매로 추출하며, 초음파 처리하여 제조할 수 있다.The cedar extract may be prepared by completely drying the bark through the cuticle work of the cedar, drying it with salt, pulverizing by heating, extracting with a solvent, and sonicating.
상기 두충나무는 두충과(Eucommiaceae)에 속하며 그 수피는 주로 한약재로 쓰이는데 이를 두충의 수피라고도 한다. 두충은 판상을 이루는데 그 두께가 3~7㎜ 정도이고 크기는 다르다. 외면은 회색 또는 암회색을 나타내고 내면은 평활한데 암자색을 보이고 질은 깔끄럽다. 두충나무를 횡단하면 세백색의 질긴 잠사상의 섬유질이 나온다. 주성분은 상피질·수지·회분 등이다. 일반적으로 5~6월에 채취되는 두충은 독이 없으며 단맛이 있고 맵다. 주로 신장과 간의 경락에 들어가 작용하며 효능은 보간신·강근골·안태(태아를 안정되게 함)이다. 두충은 주로 요통에 사용하며 특히 신양허로 인한 요통에 반드시 필요하며, 이때 속단·토사자·육종용 등을 배합해 사용한다. 또 신양허로 인한 임신중의 하복통, 성기출혈에 사용하는데 두충에는 유산방지작용이 있으므로 속단과 상기생을 배합해 사용하며, 고혈압에 사용하기도 한다. 이때는 황금·하고초·상기생·우슬 등의 강압작용이 있는 약물을 배합해야 한다. 두충은 양기를 보해서 신체를 조정하는 것이 주된 작용이므로 간양상항(간의 음적인 요소가 부족하여 간의 양적인 요소를 제어하지 못하여 간정이 편왕하여 상항하게 되는 병리현상)의 고혈압에는 효과가 없다. The cedar tree belongs to the eucommiaceae, and its bark is mainly used as a medicinal herb, which is also called the bark of the soybean. The head of the caterpillar forms a plate, its thickness is about 3-7mm and the size is different. The outer surface is gray or dark gray, the inner surface is smooth, dark purple and the quality is smooth. Crossing the cedar tree produces three white, tough, coarse fibrous fibers. Main components are epithelium, resin and ash. In general, the tofu collected in May-June is poisonous, sweet and spicy. It mainly works in the meridians of the kidneys and liver, and its efficacy is interpolation, iliac bone, and antenatal (to stabilize the fetus). Toothache is mainly used for low back pain, especially for low back pain caused by Xinyangheo. At this time, it is used in combination with fasting, earthenware and breeding. In addition, it is used for lower abdominal pain and genital bleeding during pregnancy due to Xinyangheo, and because the tooth decay has a lactic acid prevention effect, it is used in combination with fasting and the above life, and also used for high blood pressure. At this time, a drug with a coercive effect such as golden, hazel, sanggi, and hyssop should be combined. Since the main function is to control the body by looking at the Yanggi yanggi is not effective for hypertension of the liver condition (pathological phenomenon caused by the lack of control of the liver's positive elements due to lack of liver's positive factors).
상기 삼백초 추출물 및 녹차 추출물은 삼백초 및 녹차 각각의 잎을 완전 건조시킨 후 용매로 추출하며, 초음파 처리하여 제조할 수 있다.The triticale extract and green tea extract may be prepared by completely drying the leaves of each of the triticale and green tea and extracting them with a solvent, followed by sonication.
상기 삼백초는 쌍떡잎식물 후추목 삼백초과의 여러해살이풀로서, 꽃이 필 때쯤 꽃 밑에 있는 2~3개의 잎이 하얗게 변하고 꽃과 뿌리 또한 흰빛이어서 세가지 흰색을 가졌다고 해서 삼백초라는 이름이 붙었다. 야릇한 쓴맛이 있고 송장 썩는 냄새가 난다고 하여 '송장풀'이라고도 한다. 진흙 같이 습하고 무른 곳을 좋아하며 흰 뿌리줄기가 길게 옆으로 뻗는다. 생명력이 강하며 병충해가 없이 깨끗한 식물이다. 초여름에 흰색 잎이 나오고 그 끝에 이삭 모양의 흰꽃이 달린다. 꽃대는 처음에는 구부러져 있지만 꽃이 피면서 곧추 선다. 자생지는 제주도이지만 추위에 강해 중부지방에서도 월동이 가능하며, 주로 땅속줄기로 번식한다. 삼백초는 항암작용이 뛰어나며, 모세혈관을 강화하여 고혈압이나 동맥경화에 효과가 있다. 또한 해독 및 이뇨 작용을 하여 신장염과 부종 등의 치료약으로 쓰이기도 한다. The three hundred sec is a perennial herb of the dicotyledonous pepper tree, three hundred perennial, and when the flowers bloom, two to three leaves under the flowers turn white, and the flowers and roots are also white, so they were named three hundred seconds. It is called 'invoice pool' because it has a bitter taste and smells like rotting invoice. I like wet and soft places like mud, and the white rhizome stretches aside. It is a plant with strong vitality and no pests. In early summer, white leaves come out, and at the end of it is a white flower of the shape of Isaac. The stalk is bent at first, but stands straight as the flower blooms. Although it is native to Jeju Island, it is cold and can be overwintered in the central region. Three hundred seconds is excellent anti-cancer action, and strengthens capillaries and is effective in hypertension or arteriosclerosis. Detoxification and diuretic effect is also used as a treatment for nephritis and edema.
상기 녹차는 발효시키지 않은 차잎으로서, 차나무는 상록수로 비교적 따뜻하고 강우량이 많은 지역에서 잘 자란다. 녹차는 강력한 항암 효과, 염증 억제, 혈당 상승치 억제 및 완화, 항산화 작용, 다이어트 효능, 중금속과 니코틴 해독작용, 피로회복과 숙취제거, 체질의 산성화 예방, 충치 및 입냄새 제거, 피부미용에 좋은 것으로 알려져 있다.The green tea is a tea leaf that has not been fermented, and the tea tree is evergreen and relatively warm and grows well in areas with high rainfall. Green tea is known for its powerful anti-cancer effects, inhibition of inflammation, inhibition and alleviation of elevated blood sugar levels, antioxidant activity, dietary effects, heavy metal and nicotine detoxification, fatigue and hangover removal, prevention of acidification of constitution, removal of tooth decay and bad breath, and skin care. have.
상기 식물성 에탄올은 쌀, 보리, 고구마, 수수 등의 곡물을 발효시켜 만들어진 곡물 발효주정인 것이 바람직하다.The vegetable ethanol is preferably a grain fermentation alcohol made by fermenting grains such as rice, barley, sweet potato, sorghum.
또한, 본 발명의 천연 살균 탈취제는 자몽씨 추출물, 목단씨 추출물, 티트리 에센스 오일, 레몬그라스 에센스 오일, 시트로낼라 에센스 오일, 유칼립투스 에센스 오일, 만다린 에센스 오일, 주니퍼베리 에센스 오일 및 프로폴리스로 이루어진 군에서 선택된 1종 또는 2종 이상을 추가로 포함할 수 있다.In addition, the natural bactericidal deodorant of the present invention is composed of grapefruit seed extract, sweet seed extract, tea tree essence oil, lemongrass essence oil, citronola essence oil, eucalyptus essence oil, mandarin essence oil, juniper berry essence oil and propolis It may further comprise one or two or more selected from the group.
특히, 상기 프로폴리스는 러시안 페니실린, 천연페니실린이라고도 하며, 꿀벌은 벌집의 틈이 난 곳에 프로폴리스를 발라 병균이나 바이러스로부터 스스로를 보호하고, 말벌이나 쥐와 같은 적의 침입을 막는다. 성분으로는 유기물과 미네랄(무기염류)이 가장 많으며 이와 함께 104종 정도의 성분이 들어 있다. In particular, the propolis is also called Russian penicillin, natural penicillin, bees apply propolis in the gaps of the honeycomb to protect themselves from germs and viruses, and prevent invasion of enemies such as wasps and mice. Ingredients are the most organic and minerals (inorganic salts), with 104 kinds of ingredients.
이하, 하기 실시예를 통해 본 발명을 보다 상세하게 설명한다. 다만, 이러한 실시예에 의해 본 발명이 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail with reference to the following examples. However, the present invention is not limited by these examples.
<실시예 1 내지 실시예 3> 천연 살균 탈취제 제조<Examples 1 to 3> Preparation of natural bactericidal deodorant
1. 추출물 준비1. Extract Preparation
1) 귀룽나무 추출물(European bird cherry Extract)1) European bird cherry extract
귀룽나무(European bird cherry)의 수피를 건조하고 광천수로 숙성시킨 후 정제수로 80-90℃에서 열수 추출하였다. 상기 황벽나무 추출물을 3분 동안 초음파 처리하여 시료로서 사용하였다. Bark of European bird cherry was dried and aged with mineral water, and hot water was extracted at 80-90 ℃ with purified water. The yellow wall extract was sonicated for 3 minutes and used as a sample.
2) 황벽나무 추출물(Amur cork Extract)2) Amur cork extract
황벽나무 (Phellodendron amurense) 및 동속식물(운향과 rutaceae)의 수피를 건조하고 광천수로 숙성시킨 후 정제수로 80-90℃에서 열수 추출하였다. 상기 황벽나무 추출물을 3분 동안 초음파 처리하여 시료로서 사용하였다. The bark of the Phellodendron amurense and the same plants (Rhyang and rutaceae) were dried, aged in mineral water, and extracted with purified water at 80-90 ° C. The yellow wall extract was sonicated for 3 minutes and used as a sample.
3) 두충 추출물(Eucommia Extract)3) Eucommia Extract
두충나무 (Eucommia ulmoides Oliver)의 수피를 건조하여 소금에 절인 후 가열하여 분쇄하고 정제수로 80-90℃에서 열수 추출하였다. 상기 두충 추출물을 3분 동안 초음파 처리하여 시료로서 사용하였다. Bark of the Eucommia ulmoides Oliver was dried, salted, heated, ground and extracted with purified water at 80-90 ° C. The larvae extract was sonicated for 3 minutes and used as a sample.
4) 녹차 추출물(Green tea Extract)4) Green tea Extract
녹차 (Green tea)의 건조한 잎을 정제수로 80-90℃에서 열수 추출하였다. 상기 녹차 추출물을 3분 동안 초음파 처리하여 시료로서 사용하였다. The dried leaves of green tea were extracted with purified water at 80-90 ° C. The green tea extract was sonicated for 3 minutes and used as a sample.
5) 뽕나무 추출물(Morus Extract)5) Morus Extract
뽕나무 (Morus alba L.), 산뽕나무 (Morus bombycis Koidzumi) 또는 그 밖의 동속식물(Moraceae)의 줄기와 뿌리껍질을 건조하고 광천수로 숙성시킨 후 정제수로 80-90℃에서 열수 추출하였다. 상기 뽕나무 추출물을 3분 동안 초음파 처리하여 시료로서 사용하였다. Stems and root bark of mulberry (Morus alba L.), Mulberry (Morus bombycis Koidzumi) or other similar plants (Moraceae) were dried, aged in mineral water and extracted with hot water at 80-90 ° C with purified water. The mulberry extract was sonicated for 3 minutes and used as a sample.
6) 닥나무 추출물(Broussonetia Extract)6) Broussonetia Extract
닥나무 (Broussonetia kazinoki) 및 동속식물(뽕나무과 Moraceae)의 줄기 또는 뿌리를 건조하고 광천수로 숙성시킨 후 정제수로 80-90℃에서 열수 추출하였다. 상기 닥나무 추출물을 3분 동안 초음파 처리하여 시료로서 사용하였다. Stems or roots of Burberry (Broussonetia kazinoki) and related plants (Moraceae) were dried and aged with mineral water and extracted with hot water at 80-90 ° C with purified water. The mulberry extract was sonicated for 3 minutes and used as a sample.
7) 삼백초 추출물(Saururus Extract)7) Samururus Extract
삼백초 (Saururus chinensis)의 건조한 잎을 정제수로 80-90℃에서 열수 추출하였다. 상기 삼백초 추출물을 3분 동안 초음파 처리하여 시료로서 사용하였다. Dry leaves of three hundred (Saururus chinensis) were extracted with purified water at 80-90 ℃. The 300 sec extract was sonicated for 3 minutes and used as a sample.
2. 천연 살균 탈취제 제조2. Natural Sterilization Deodorant Manufacturer
앞서 준비된 각 추출물들과 하기 표 1에 기재된 다른 성분들을 표 1에 기재된 함량으로 포함시켜 천연 살균 탈취제를 제조하였다. 이때, 식물성 에탄올은 디씨케미칼 제품을 사용하였다.To prepare a natural bactericidal deodorant by including each of the extracts prepared in advance and the other components shown in Table 1 in the content shown in Table 1. At this time, vegetable ethanol was used for DC Chemical.
표 1
성분 (중량(g)) 효능 실시예 1 실시예 2 실시예 3
귀룽나무 추출물 항균, 살균, 진균, 탈취 4 6 8
황벽나무 추출물 항균, 살균, 진균, 탈취 10 9 8
두충나무 추출물 항균 16 15 14
녹차 추출물 살균, 해독 20 20 20
뽕나무 추출물 항균, 항염 9 9 9
닥나무 추출물 항균, 항염, 해독 8 8 8
삼백초 살균, 항균 15 15 15
식물성에탄올 (주정유) 살균, 소독 15 15 15
자몽씨 추출물 항균, 방부 1.1 1.1 1.1
목단씨 추출물 항균, 항염 1 1 1
티트리 에센스 오일 방부, 항균 0.05 0.05 0.05
레몬그라스 에센스 오일 살균, 방부 0.5 0.5 0.5
시트로낼라 에센스 오일 살균, 곤충기피제 0.05 0.05 0.05
유칼립투스 에센스 오일 항박테리아, 항바이러스 0.05 0.05 0.05
만다린 에센스 오일 진정, 살균 0.05 0.05 0.05
주니퍼베리 에센스 오일 해독, 이뇨, 살균 0.05 0.05 0.05
프로폴리스 항균, 면역, 항바이러스 0.15 0.15 0.15
Table 1
Component (weight (g)) efficacy Example 1 Example 2 Example 3
Rhubarb Extract Antibacterial, sterilization, fungus, deodorization 4 6 8
Yellow Wall Extract Antibacterial, sterilization, fungus, deodorization 10 9 8
Cedar extract Antibacterial 16 15 14
Green tea extract Sterilization, detoxification 20 20 20
Mulberry Extract Antibacterial, anti-inflammatory 9 9 9
Paper mulberry extract Antibacterial, anti-inflammatory, detoxification 8 8 8
Three hundred seconds Antiseptic, antibacterial 15 15 15
Vegetable Ethanol (Oil) Sterilization, Disinfection 15 15 15
Grapefruit Seed Extract Antibacterial, antiseptic 1.1 1.1 1.1
Peony Seed Extract Antibacterial, anti-inflammatory One One One
Tea tree essence oil Antiseptic, antibacterial 0.05 0.05 0.05
Lemongrass Essence Oil Sterilization, antiseptic 0.5 0.5 0.5
Citronola Essence Oil Sterilization, insect repellent 0.05 0.05 0.05
Eucalyptus essence oil Antibacterial, antiviral 0.05 0.05 0.05
Mandarin Essence Oil Calm, Sterilize 0.05 0.05 0.05
Juniper Berry Essence Oil Detoxification, diuresis, sterilization 0.05 0.05 0.05
Propolis Antibacterial, immune, antiviral 0.15 0.15 0.15
<실험예 1> 항진균 시험Experimental Example 1 Antifungal Test
앞선 실시예에서 제조된 천연 살균 탈취제의 항진균 활성을 검토하기 위하여, 천연 살균 탈취제 처리 후 합판 중에 감염된 진균에 대한 살균 효과를 평가하여 항진균 시험을 수행하였다. 즉, 실시예 1 내지 3에서 제조된 천연 살균 탈취제를 3개의 합판에 뿌려서 살균작업을 실시하였다. 대조군을 위하여 살균작업이 안 된 합판도 준비하였다. 작업이 끝난 합판에는 랩을 씌워서 다른 오염을 방지하였다. 24시간이 지난 뒤에 각각의 합판에서 면봉으로 균을 채취하여 37℃에서 최대 3일간, 실온에서 6일간 배양하였다. 3일, 6일, 9일 뒤에도 위와 같은 작업을 실시하였다. 이때, 배양을 위한 배지로는 덱스트로즈 배지를 사용하였다.In order to examine the antifungal activity of the natural bactericidal deodorant prepared in the previous example, the antifungal test was performed by evaluating the bactericidal effect on the fungi infected in the plywood after the treatment of the natural bactericidal deodorant. That is, the sterilization operation was performed by spraying the natural sterilization deodorant prepared in Examples 1 to 3 on the plywood. Non-sterile plywood was also prepared for the control. The finished plywood was wrapped to prevent other contamination. After 24 hours, bacteria were collected from each plywood with cotton swabs and incubated at 37 ° C. for up to 3 days and at room temperature for 6 days. The above work was performed three, six and nine days later. At this time, a dextrose medium was used as a culture medium.
실시예에 따른 천연 살균 탈취제를 합판에 살균 처리 후 3일까지는 살균효과가 지속되지만 6일 이후에는 진균의 성장이 일어났다. 살균 처리 전에 비하여서는 소수의 진균이 성장하였다(표 2 참조).The bactericidal effect was maintained until 3 days after the sterilization treatment of the natural sterilizing deodorant according to the embodiment, but after 6 days the fungal growth occurred. A few fungi grew before the sterilization treatment (see Table 2).
표 2
배양조건 경과일 [unit: CFU(colony forming unit)]
살균 전 1일 후 3일 후 6일 후 9일 후
37℃3일간 실시예 1 100↑ 0 0 15 15
실시예 2 100↑ 0 0 8 20
실시예 3 100↑ 0 0 4 10
대조군 100↑ 100↑ 100↑
실온6일간 실시예 1 100↑ 0 0 10 25
실시예 2 100↑ 0 0 20 10
실시예 3 100↑ 0 2 7 5
대조군 100↑ 100↑ 100↑
TABLE 2
Culture condition Elapsed [unit: colony forming unit]
Before sterilization 1 day later 3 days later 6 days later 9 days later
37 ° C for 3 days Example 1 100 ↑ 0 0 15 15
Example 2 100 ↑ 0 0 8 20
Example 3 100 ↑ 0 0 4 10
Control 100 ↑ 100 ↑ 100 ↑
Room temperature for 6 days Example 1 100 ↑ 0 0 10 25
Example 2 100 ↑ 0 0 20 10
Example 3 100 ↑ 0 2 7 5
Control 100 ↑ 100 ↑ 100 ↑

Claims (5)

  1. 귀룽나무 추출물, 황벽나무 추출물, 닥나무 추출물, 뽕나무 추출물, 두충나무 추출물, 삼백초 추출물, 녹차 추출물 및 식물성 에탄올을 유효성분으로 함유하는 천연 살균 탈취제.Natural bactericidal deodorant containing oak extract, yellow bark extract, mulberry extract, mulberry extract, cedar extract, triticale extract, green tea extract and vegetable ethanol as active ingredients.
  2. 청구항 1에 있어서, 상기 천연 살균 탈취제는 귀룽나무 추출물 2 내지 8 중량%, 황벽나무 추출물 5 내지 15 중량%, 닥나무 추출물 10 내지 20 중량%, 뽕나무 추출물 15 내지 25 중량%, 두충나무 추출물 5 내지 15 중량%, 삼백초 추출물 5 내지 15 중량%, 녹차 추출물 10 내지 20 중량% 및 식물성 에탄올 10 내지 20 중량%를 유효성분으로 함유하는 것을 특징으로 하는 천연 살균 탈취제.The method according to claim 1, wherein the natural bactericidal deodorant 2 to 8% by weight of the extract of the alpine tree, 5 to 15% by weight of the yellow bark extract, 10 to 20% by weight of the mulberry extract, 15 to 25% by weight of mulberry extract, 5 to 15 cedar extract Natural bactericidal deodorant, characterized in that containing as an active ingredient by weight, 5 to 15% by weight, 300 to 30% by weight, green tea extract 10 to 20% by weight and vegetable ethanol.
  3. 청구항 1 또는 청구항 2에 있어서, 상기 추출물은 열수, 에틸아세테이트, 클로로포름, 헥산, C1-C4 알코올 및 이들의 혼합물로 이루어진 군에서 선택된 용매로 추출한 추출물인 것을 특징으로 하는 천연 살균 탈취제.The natural bactericidal deodorant of claim 1 or 2, wherein the extract is an extract extracted with a solvent selected from the group consisting of hot water, ethyl acetate, chloroform, hexane, C1-C4 alcohol, and mixtures thereof.
  4. 청구항 3에 있어서, 상기 추출물은 열수, 에틸아세테이트, 클로로포름, 헥산, C1-C4 알코올 및 이들의 혼합물로 이루어진 군에서 선택된 용매로 추출한 후, 초음파 처리한 추출물인 것을 특징으로 하는 천연 살균 탈취제.The method of claim 3, wherein the extract is a natural bactericidal deodorant, characterized in that the extract after sonication after extraction with a solvent selected from the group consisting of hot water, ethyl acetate, chloroform, hexane, C1-C4 alcohol and mixtures thereof.
  5. 청구항 1 또는 청구항 2에 있어서, 상기 천연 살균 탈취제는 자몽씨 추출물, 목단씨 추출물, 티트리 에센스 오일, 레몬그라스 에센스 오일, 시트로낼라 에센스 오일, 유칼립투스 에센스 오일, 만다린 에센스 오일, 주니퍼베리 에센스 오일 및 프로폴리스로 이루어진 군에서 선택된 1종 또는 2종 이상을 추가로 포함하는 것을 특징으로 하는 천연 살균 탈취제.The method according to claim 1 or claim 2, wherein the natural bactericidal deodorant is grapefruit seed extract, Peony seed extract, tea tree essence oil, lemongrass essence oil, citronola essence oil, eucalyptus essence oil, mandarin essence oil, juniper berry essence oil and Natural bactericidal deodorant further comprising one or two or more selected from the group consisting of propolis.
PCT/KR2012/002510 2011-04-05 2012-04-04 Natural antiseptic deodorizer WO2012138108A1 (en)

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