WO2009090899A1 - 載置台装置、処理装置および温度制御方法 - Google Patents
載置台装置、処理装置および温度制御方法 Download PDFInfo
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- WO2009090899A1 WO2009090899A1 PCT/JP2009/050058 JP2009050058W WO2009090899A1 WO 2009090899 A1 WO2009090899 A1 WO 2009090899A1 JP 2009050058 W JP2009050058 W JP 2009050058W WO 2009090899 A1 WO2009090899 A1 WO 2009090899A1
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- temperature
- mounting table
- innermost
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- heating
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Images
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/67—Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
- H01L21/67005—Apparatus not specifically provided for elsewhere
- H01L21/67242—Apparatus for monitoring, sorting or marking
- H01L21/67248—Temperature monitoring
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
- C23C16/46—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating characterised by the method used for heating the substrate
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/67—Apparatus specially adapted for handling semiconductor or electric solid state devices during manufacture or treatment thereof; Apparatus specially adapted for handling wafers during manufacture or treatment of semiconductor or electric solid state devices or components ; Apparatus not specifically provided for elsewhere
- H01L21/67005—Apparatus not specifically provided for elsewhere
- H01L21/67011—Apparatus for manufacture or treatment
- H01L21/67098—Apparatus for thermal treatment
- H01L21/67103—Apparatus for thermal treatment mainly by conduction
Definitions
- the present invention relates to a processing apparatus for performing a heat treatment such as a film forming process on an object to be processed such as a semiconductor wafer, a mounting table apparatus used therefor, and a temperature control method.
- various processes such as a film formation process, an etching process, a thermal diffusion process, and a modification process are repeatedly performed on an object to be processed such as a semiconductor wafer.
- a single wafer processing apparatus that performs heat treatment on a semiconductor wafer one by one will be described as an example.
- a mounting table including a resistance heater made of, for example, molybdenum wire is installed in a processing container that can be evacuated.
- the semiconductor wafer is mounted on the mounting table by being attached to the upper end of the leg that is erected from the bottom of the container. Then, with the semiconductor wafer mounted on the mounting table as described above, a predetermined processing gas is allowed to flow in the processing container while maintaining a predetermined reduced pressure atmosphere, and at the same time, the resistance heater is driven.
- the semiconductor wafer is heated and maintained at a predetermined temperature, and a predetermined process such as a film forming process is performed.
- aluminum alloy has been mainly used for the mounting table and the leg portion for supporting the mounting table.
- the aluminum alloy is used.
- a ceramic material such as AlN, which has less metal contamination and excellent heat resistance, for example, as a mounting table or a leg (for example, Japanese Utility Model Publication No. 3-128668). (Kaihei 6-252055).
- a single hollow leg is connected to the center of the back surface of the mounting table, and necessary wiring such as a power supply line for the resistance heater is accommodated in the hollow leg. ing.
- the resistance heater of the mounting base is divided into a plurality of, for example, two concentric shapes that can be controlled independently of each other.
- a heating zone is provided, and the temperature of each heating zone is individually controlled based on the measured value of the thermocouple provided at the center of the mounting table.
- the temperature distribution at which the in-plane uniformity of the film thickness is the best depends on the process temperature for heating the semiconductor wafer, so before processing the product wafer,
- the current ratio or voltage ratio between the heaters so as to obtain an optimum temperature distribution depending on the process temperature is obtained in advance, and when processing an actual product wafer, the temperature of the innermost heating zone is as follows: Feedback control is performed based on the measured value of the thermocouple, and the temperature of the other outer heating zone is the current ratio or voltage to the heater in the innermost heating zone determined in advance corresponding to the process temperature. By supplying power based on the ratio, so-called open loop control is performed.
- the mounting table and the legs supporting the mounting table are made of a ceramic material such as AlN (aluminum nitride), for example.
- This ceramic material is a brittle material, and the temperature distribution between the inner and outer periphery of the mounting table.
- the mounting table may be easily damaged by thermal stress generated due to the above.
- the method of controlling the temperature of the heating zone (heater) on the inner and outer peripheries of the mounting table with a current ratio or voltage ratio depending on the process temperature has a problem that the ceramic mounting table is likely to be damaged. .
- An object of the present invention is to provide a mounting table device that is less likely to be damaged by thermal stress when a workpiece is mounted on the mounting table and heated, and a processing apparatus equipped with such a mounting table device.
- Another object of the present invention is to provide a temperature control method in which when a workpiece is placed on a mounting table and heated, the mounting table is not easily damaged by thermal stress.
- Still another object of the present invention is to provide a storage medium storing a program for executing such a temperature control method.
- a mounting table for mounting the object to be processed, and a plurality of heater portions provided for each of a plurality of heating zones concentrically divided on the mounting table described above.
- a heating mechanism a leg connected to the center of the mounting table and supporting the mounting table horizontally, and a temperature provided corresponding to the innermost heating zone of the plurality of heating zones Based on the measurement values of the measurement unit and the temperature measurement unit, feedback control is performed on the temperature of the innermost heater unit, and the temperature difference between the heating zones is determined to be within a range in which the mounting table is not damaged.
- a mounting table device including a power supply control unit that controls the power supplied to the other heater heater at a ratio of the safe power supply to the innermost heater heater.
- the temperature of the innermost heater unit is feedback-controlled based on the measurement value of the temperature measuring unit, and each heating of the mounting table is performed. Controls the power supplied to other heaters by the power ratio (safety supply power ratio) to the innermost heater, which is determined so that the temperature difference of the zone (heater) does not damage the mounting table.
- the power ratio safety supply power ratio
- the safety supply power ratio can be set so that the temperature of the innermost heating zone of the mounting table is the lowest, and specifically, the safety supply power ratio is determined by the mounting table.
- the power ratio can be set so that the temperature difference between the innermost and outermost heating zones is within 33 ° C.
- the power control unit is configured so that the temperature of the innermost heating zone is higher than the temperature of the outermost heating zone when the temperature of the mounting table is raised and lowered. However, it is preferable to control so that it does not become lower than a predetermined temperature difference.
- the power supply controller raises the temperature of the mounting table in a state where the temperature of the heating zone on the innermost circumference is higher than that on the outermost circumference, and supplies the heaters when the set temperature is reached. It is preferable to control the power so as to gradually approach the safe supply power ratio.
- a unit having a thermocouple can be typically used as the temperature measuring unit.
- what consists of a ceramic material can be used as at least one of the said mounting base and the said leg part.
- a processing apparatus for performing a predetermined heat treatment on an object to be processed, wherein a processing container in which an internal atmosphere can be evacuated, and a necessary gas is supplied into the processing container.
- the mounting table device includes a mounting table for mounting the object to be processed, and a plurality of concentric compartments on the mounting table.
- a heating mechanism having a plurality of heaters provided for each heating zone, a leg portion connected to the center of the mounting table and supporting the mounting table horizontally, and an outermost of the plurality of heating zones.
- a temperature measurement unit provided corresponding to an inner heating zone, and feedback control of the temperature of the innermost heater unit based on the measured value of the temperature measurement unit, and a temperature difference between the heating zones So that the mounting table is not damaged. Is constant, the safe supply power ratio innermost heater unit, the processing apparatus is provided with a power control unit for controlling the power supplied to the other heater portion.
- the object to be processed is mounted on a mounting table provided in a processing container whose internal atmosphere can be evacuated, and concentrically defined on the mounting table.
- a method for controlling the temperature of the object to be processed by controlling a heating mechanism having a plurality of heater portions provided for each of a plurality of heating zones, the innermost heating zone among the plurality of heating zones The temperature difference between the heating zones is described above, and the temperature difference between the heating zones is controlled as described above by feedback control of the innermost heater unit based on the measured temperature.
- a temperature control method including controlling supply power to the other heater unit at a safe supply power ratio with respect to the innermost heater unit, which is determined so that the pedestal is not damaged. Is done.
- the temperature of the innermost heating zone is maintained in a state in which the temperature of the innermost heating zone does not become lower than the temperature of the outermost heating zone by a predetermined temperature difference or more during the temperature rise of the mounting table. Further, it is preferable to maintain the temperature of the innermost heating zone so that the temperature of the innermost heating zone does not become lower than the temperature of the outermost heating zone by a predetermined temperature or more when the temperature of the mounting table is lowered.
- a plurality of objects to be processed are mounted on a mounting table provided in a processing container in which the internal atmosphere can be evacuated, and concentrically defined on the mounting table.
- the heating mechanism having a plurality of heater portions provided for each heating zone is controlled to control the temperature of the object to be processed and when a predetermined process is performed on the object to be processed, the plurality of heating zones Measuring the temperature of the innermost heating zone, and controlling the innermost heating heater unit based on the measured temperature to have a set temperature by feedback control; and
- the supply power to the other heaters is controlled by the safety supply power ratio with respect to the innermost heater, which is determined so that the temperature difference between the heating zones is within a range in which the mounting table is not damaged.
- a temperature control method including Sea urchin, a storage medium having a program for controlling the processor to the computer is stored is provided.
- FIG. 1 It is a schematic sectional drawing which shows the processing apparatus which concerns on one Embodiment of this invention. It is a top view which shows the heating mechanism provided in the mounting base of the mounting base apparatus with which the processing apparatus of FIG. 1 is provided. It is a figure which shows typically the relationship between the process gas density
- FIG. 1 is a schematic cross-sectional view showing a processing apparatus according to an embodiment of the present invention
- FIG. 2 is a plan view showing a heating mechanism provided on the mounting table of the mounting table device provided in the processing apparatus.
- a film forming process is performed by CVD on a semiconductor wafer which is an object to be processed will be described as an example.
- the processing apparatus 2 includes a processing container 4 formed into a cylindrical shape from, for example, nickel, a nickel alloy, or an aluminum alloy.
- a shower head portion 6 having a large number of gas ejection holes 6A and 6B on the lower surface as a gas supply mechanism is provided on the ceiling portion of the processing vessel 4 so that, for example, a film forming gas is used as the processing gas in the processing vessel 4. It can be introduced into the processing space S.
- the shower head 6 is divided into, for example, two gas spaces 8A and 8B, and the gas ejection holes 6A and 6B communicate with the gas spaces 8A and 8B, respectively. It is a so-called postmix type in which gas can be mixed for the first time.
- the entire shower head portion 6 is made of, for example, nickel, a nickel alloy, an aluminum alloy, or the like.
- the ceiling portion of the processing container 4 having the shower head portion 6 is attached to the upper end of the side wall of the processing container 4 via a seal member 10 made of, for example, an O-ring so as to maintain the airtightness in the processing container 4. It has become.
- a loading / unloading port 12 for loading / unloading a semiconductor wafer W as an object to be processed is formed on the side wall of the processing container 4, and a gate valve 14 is provided in the loading / unloading port 12 to be opened and closed. .
- a load lock chamber or a transfer chamber (not shown) is connected to the gate valve 14.
- a concave portion 17 that is depressed downward is formed on the center side of the bottom portion 16 of the processing container 4, and the inside of the concave portion 17 serves as an exhaust space 18.
- An exhaust port 20 is provided in the lower side wall of the concave portion 17 that defines the exhaust space 18.
- the exhaust port 20 is connected to a vacuum exhaust system 22 in which a pressure control valve and a vacuum pump (not shown) are provided in the middle, and the inside of the processing container 4 is evacuated by the vacuum exhaust system 22 to obtain a predetermined pressure. To be maintained.
- a mounting table device 24 for mounting a semiconductor wafer, which is an object to be processed is provided.
- the mounting table device 24 has a mounting table 26 on which the wafer W is actually mounted on its upper surface, and leg portions 28 that are connected to the center of the lower surface of the mounting table 26 and extend downward to support the mounting table 26 horizontally. And have.
- the lower end of the leg portion 28 is supported by the bottom portion 16 ⁇ / b> A of the concave portion 17 that defines the exhaust space 18.
- the leg portion 28 has a hollow shape, that is, a cylindrical shape, and an open lower end.
- Both the mounting table 26 and the leg portion 28 are made of a ceramic material such as AlN. One of these may be formed of a ceramic material.
- a resistance heater 30 is embedded in the upper part of the mounting table 26 as a heating mechanism for heating the wafer W mounted thereon.
- the resistance heater 30 is made of, for example, molybdenum wire, and as shown in FIG. 2, the resistance heater 30 is divided into an inner zone heater 32A and an outer zone heater 32B in a concentric manner. Two heating zones of the outer heating zone are formed, and the heating temperature can be controlled for each zone.
- the ceramic heater is comprised by the mounting base 26 and the resistance heater 30 which consist of ceramic materials.
- the number of zones is not particularly limited, and may be three or more zones.
- connection terminals of the heaters 32A and 32B in each zone are located at the center of the mounting table 26 (see FIG. 1), and power supply rods 36A and 36B made of, for example, Ni are respectively connected to these connection terminals by, for example, Ni—Au brazing. It is joined.
- power supply rods 36A and 36B extend downward, extend through the hollow leg portion 28 to the outside, and are connected to a power supply unit 37 that supplies electric power.
- feeding rod 36A, 36B Note that only one feeding rod 36A, 36B is shown in FIG. 1, but two feeding rods are actually provided.
- the upper end of the ceramic leg portion 28 is airtightly joined to the lower surface of the central portion of the mounting table 26.
- a mounting flange portion 28A at the lower end of the leg portion 28 is airtightly attached to the bottom portion 16A of the concave portion 17 that defines the exhaust space 18. Note that the leg portion 28, an inert gas such as N 2 gas are supplied.
- the mounting table 26 has a diameter of about 340 mm and the leg portion 28 has a diameter of about 40 to 50 mm.
- a temperature measuring unit 38 is provided at the center of the back surface side (lower surface side) of the mounting table 26 so as to correspond to the innermost heating zone, here, the inner heating zone 34A, and the temperature of the inner heating zone 34A is set. It can be measured.
- a thermocouple can be used, for example, and this thermocouple is attached to the center of the back surface of the mounting table 26 by fusion. In this case, since the temperature measuring unit 38 made of the thermocouple is housed in the leg portion 28, the thermocouple is not exposed to various gases supplied into the processing container 4, and the thermocouple Corrosion is prevented.
- the wiring 40 extending from the temperature measuring unit 38 passes through the bottom 16A side and is drawn to the outside, and is connected to a power supply control unit 42 made of, for example, a microprocessor (computer).
- the power supply control unit 42 can control the heaters 32A and 32B in the heating zone based on the detection value of the temperature measurement unit 38.
- the inner zone heater 32A of the inner heating zone 34A is feedback controlled so as to maintain the process temperature of the film forming process.
- the outer zone heater 32B of the outer heating zone 34B is supplied with power to the inner zone heater 32A regardless of the control mode such as current control, voltage control, and power control. Is set so that power determined by a predetermined safe supply power ratio is supplied, and open loop control is performed.
- control is performed so that 0.8 times the power supplied to the inner zone heater 32A is supplied to the outer zone heater 32B.
- the current control is to output an operation amount corresponding to the difference between the set temperature and the actual temperature as a current form
- the voltage control is to output this difference as a voltage. This difference is output as electric power.
- the safety supply power ratio is determined so that the temperature difference between the heating zones is within a range in which the mounting table 26 is not damaged. Depending on the process temperature, the in-plane uniformity of the film thickness is slightly increased. There is a case where the power ratio is set so as to prevent the mounting table 26 from being damaged even if it is lowered. This point will be described later.
- the power supply control unit 42 In addition to controlling the operation of the mounting table device 24, the power supply control unit 42 also has a function of controlling the entire operation of the processing device 2, and the power supply control unit 42 controls the operation thereof.
- a storage medium 44 storing the program is connected.
- the storage medium 44 for example, a flexible disk, a flash memory, or the like can be used.
- the mounting table 26 is formed with a plurality of pin holes 46 penetrating in the vertical direction, and each pin hole 46 has a lower end commonly connected to a connection ring 48, for example, made of quartz.
- the pin 50 is accommodated in a loosely fitted state.
- the connecting ring 48 is connected to an upper end of a retracting rod 52 that is provided so as to be vertically movable through the bottom of the container.
- the lower end of the retracting rod 52 is connected to an air cylinder 54.
- a bellows 56 that can be expanded and contracted is provided in a through-hole portion of the retractable rod 52 with respect to the bottom of the container so that the retractable rod 52 can be raised and lowered while maintaining the airtightness in the processing container 4. ing.
- a film forming method (including a temperature control method) performed using the processing apparatus 2 configured as described above will be described.
- the vacuum exhaust system 22 The inside of the processing container 4 is maintained at a predetermined process pressure, and a predetermined processing gas (film forming gas) is introduced into the processing container 4 from the shower head unit 6 serving as a gas supply means, and is predetermined on the wafer W by CVD.
- the thin film is formed.
- NH 3 gas is supplied to one gas space 8A of the shower head unit 6, and TiCl 4 + N 2 gas is supplied to the other gas space 8B.
- TiCl 4 + N 2 gas is supplied to the other gas space 8B.
- Each of these gases is mixed in the processing space S to perform a TiN film forming process.
- the power supply control unit 42 controls the power supply unit 37 based on the measurement value from the temperature measurement unit 38 made of a thermocouple provided at the center of the lower surface of the mounting table 26.
- the operation amount to the zone heaters 32A and 32B is controlled via
- the supply voltage to the inner zone heater 32A of the inner heating zone 34A is feedback controlled so as to maintain the process temperature of the film forming process (voltage control).
- the outer zone heater 32B of the outer heating zone 34B has a power determined by a predetermined safe supply power ratio based on the power supplied to the inner zone heater 32A (not the supply voltage). It is set and open loop control is performed. Thereby, it is possible to prevent the temperature difference between the inner and outer circumferences of the mounting table 26 from becoming excessively large, and to prevent the mounting table 26 from being damaged.
- the temperature distribution of the mounting table 26 is such that the temperature at the center of the mounting table 26 is the lowest and gradually increases as it approaches the peripheral part (edge part), that is, the temperature distribution state of the center cool. It has become. The state of this temperature distribution will be described with reference to FIG.
- FIG. 3 is a diagram schematically showing the relationship between the processing gas concentration and the temperature distribution in the diameter direction of the semiconductor wafer.
- the processing gas is generally supplied to the processing space from a shower head unit 6 provided on the ceiling of the processing container, and is diffused substantially uniformly toward the periphery of the mounting table 26 while flowing down into the processing space. Thus, air is exhausted from below the mounting table 26. Therefore, the concentration of the processing gas supplied from the shower head unit 6 to the processing space is high at the wafer center and gradually decreases toward the edge. Accordingly, if the wafer temperature is uniform over the entire surface, the reaction in the portion (center portion) where the gas concentration is high is promoted, and the film thickness of this portion becomes thicker than other portions (edge portions), which is not preferable. .
- the temperature difference ⁇ t between the wafer center and the edge is about 5 ° C., for example.
- the upper limit of the temperature difference ⁇ t is about 33 ° C., and it is desirable to set the temperature difference ⁇ t to 33 ° C. or less to prevent damage. It is.
- the feedback control is performed based on the measured value in the temperature measurement unit composed of the thermocouple for the inner heater, and the process temperature is determined for the temperature of the outer heater.
- the current ratio or voltage ratio that provides the best in-plane film thickness uniformity is determined in advance, and the current and voltage corresponding to the current ratio and voltage ratio are maintained using the inner heater as a reference. In this way, the outer heater was controlled by open loop.
- the outer zone heater 32B is controlled by the power ratio as described above instead of the current ratio or voltage ratio.
- the power ratio is controlled so that the in-plane uniformity of the film thickness is always at the highest level, the temperature difference ⁇ t sometimes increases beyond 33 ° C., in such a case, Even if the in-plane uniformity of the film thickness is slightly reduced, the power ratio is set such that the mounting table 26 is not damaged.
- the supply power ratio (OUT / IN) at which the in-plane uniformity of the film thickness is the best for various process temperatures for example, various process temperatures in the range of about 400 to 900 ° C. Is obtained in advance.
- the supply power ratio is “0.65”
- the supply power ratio is “0.70”.
- the supply power to the outer zone heater 32B is controlled with the supply power ratio as described above according to the process temperature, the optimum center cool state is obtained, and the in-plane uniformity of the film thickness is the best. In this state, a thin film can be obtained. In this case, the mounting table 26 may be damaged depending on conditions.
- a limit is imposed on the supply power ratio. That is, first, at various process temperatures (660 ° C. or less), the power control is performed on the outer zone heater 32B with the above-described power supply ratio to actually perform the film forming process. We examined whether or not. Note that feedback control was performed so as to maintain the set process temperature for the inner zone heater 32A. The result at that time is shown in FIG. In FIG. 5, the horizontal axis indicates the number of heaters for which experiments were performed.
- the supply power ratio is set as the safe supply power ratio.
- the supply power ratio at which the in-plane uniformity of the best film thickness is obtained exceeds 1.00
- “1.00” is set as the safe supply power ratio at the process temperature. That is, here, when the supply power ratio exceeds “1.00”, the in-plane uniformity of the film thickness is slightly sacrificed to make the mounting table 26 safe.
- the same examination as described above was performed when the process temperature was higher than 660 ° C. As a result, it was found that in the case of a process temperature higher than 660 ° C., if the supply power ratio is “0.82” or less, the mounting table 26 is not damaged.
- the safe supply power ratio for each process temperature obtained as described above is stored in the power supply control unit 42 in advance. Therefore, if the temperature control according to this supply power ratio is performed, the temperature difference ⁇ t between the inner and outer circumferences of the mounting table 26 can be controlled within 33 ° C. in the temperature distribution state of the center cool. Can be prevented.
- FIG. 6 is a graph showing the range of the supply power ratio that is allowed depending on the process temperature.
- the control range in the case of control by the conventional supply voltage ratio is also shown.
- the center cool state becomes larger as it goes to the right side
- the center hot state becomes as it goes to the left side.
- the supply power ratio is allowed in the range of 0.38 to 1.00.
- the supply power ratio is 0. It is allowed in the range of 38 to 0.82.
- the mounting table crack may occur in the area A1 shown on the right side, which is not preferable.
- FIG. 7A shows the case of the conventional voltage ratio control
- FIG. 7B shows the case of the power ratio control of the present invention.
- the left vertical axis represents the heater temperature (inner zone heater)
- the right vertical axis represents the operation amount.
- the operation amount 100% indicates 200 volts
- the operation amount 100% indicates 4000 watts.
- the set process temperature at this time is 700 ° C.
- the set supply voltage ratio (in the case of FIG. 7A) and supply power ratio (in the case of FIG. 7B) are “0.95” and “0.82”, respectively.
- the change in the operation amount of each heater and the change in the heater temperature from the wafer loading are shown.
- the temperature until the temperature stabilizes after the wafer loading is a very large value.
- Such a large temperature fluctuation amount H1 causes a large temperature difference between the inner and outer periphery of the mounting table 26, and as a result, the mounting table 26 is damaged.
- the temperature fluctuation amount H2 until the temperature becomes stable after the wafer is loaded is considerably small, which is about half that in the case of FIG. 7A. It has become.
- the temperature difference generated between the inner and outer periphery of the mounting table 26 does not become so large, and it is possible to prevent the mounting table 26 from being damaged, and it can be seen that good results are shown.
- the temperature control of the mounting table 26 when the process is actually performed has been described.
- the mounting table 26 is not cracked even when the mounting table 26 is heated and lowered.
- Temperature control is required.
- the temperature of the inner heating zone 34A is maintained at a predetermined temperature difference, for example, 33 ° C. or less, lower than the temperature of the outer heating zone 34B.
- the temperature is raised or lowered in the center hot state, or the temperature difference is lowered to 33 ° C. or less in the center cool state.
- the temperature difference is set to about 70 ° C. or more, for example, the mounting table 26 is damaged as described above.
- the heater temperature is maintained at 300 ° C., and the supply power ratio at this time is maintained at “0.58”. In this case, control is performed so that the inner peripheral temperature of the mounting table becomes a center hot state higher than the outer peripheral temperature. Then, the heater is heated at a rate of temperature increase of about 5 ° C./min, for example, by increasing the power supplied to both heaters while maintaining the above supply power ratio, that is, maintaining the center hot state. .
- the heater temperature reaches 700 ° C., which is the process temperature (set temperature)
- the supply power ratio gradually becomes the safe supply power ratio.
- the temperature distribution of the mounting table is gradually shifted from the center hot state to the center cool state.
- the heater temperature may be controlled so as to reverse the above process.
- the temperature difference between the inner and outer circumferences of the mounting table can be set to a temperature difference that does not break even when the heater is raised or lowered, it is possible to prevent the mounting table from being damaged.
- the present invention is not limited to the above embodiment and can be variously modified.
- each numerical example used in the above description is merely an example, and it goes without saying that the numerical value also changes depending on the design of the mounting table 26, the resistance heater 30, and the like.
- the present invention is not limited to this, and the present invention is applied to various heat treatments such as an etching process, an oxidation diffusion process, an annealing process, and a modification process.
- the present invention can be applied to a plasma processing apparatus.
- the present invention is not limited to this, and the present invention is also applied to a case where three or more heating zones are provided concentrically. can do.
- the temperature difference between the innermost heating zone and the outermost heating zone is a temperature range in which the mounting table is not broken, for example, within 33 ° C.
- the safety supply power ratio is set in the temperature range.
- the object to be processed is not limited to a semiconductor wafer, and an LCD substrate, a glass substrate, a ceramic substrate, or the like can also be used.
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Abstract
Description
本発明の他の目的は、被処理体を載置台上に載置して加熱する際に、載置台が熱応力によって破損し難い温度制御方法を提供することにある。
本発明のさらに他の目的は、そのような温度制御方法を実行するためのプログラムを記憶した記憶媒体を提供することにある。
また、前記温度測定部としては、典型的には熱電対を有するものを用いることができる。
また、前記載置台および前記脚部の少なくとも一方として、セラミック材よりなるものを用いることができる。
図1は本発明の一実施形態に係る処理装置を示す概略断面図、図2は処理装置が備える載置台装置の載置台に設けられた加熱機構を示す平面図である。なお、ここでは、被処理体である半導体ウエハに対してCVDによって成膜処理を行う場合を例にとって説明する。
まず、押し上げピン50を上下動させて、未処理の半導体ウエハWを、プロセス温度に維持されている載置台26上に載置して処理容器4内を密閉したならば、真空排気系22により、この処理容器4内を所定のプロセス圧力に維持するとともに、ガス供給手段であるシャワーヘッド部6より所定の処理ガス(成膜ガス)を処理容器4内へ導入し、CVDによりウエハWに所定の薄膜を形成する。例えば一例としてサーマルCVDによりTiN膜を成膜する場合には、シャワーヘッド部6の一方のガス空間8Aに、NH3ガスを供給し、他方のガス空間8BにTiCl4+N2ガスを供給し、これらの各ガスを処理空間S内で混合させてTiN膜の成膜処理を行う。
図7Aは従来の電圧比制御の場合を示し、図7Bは本発明の電力比制御の場合を示す。各グラフとも、左側縦軸はヒータ温度(内側ゾーンヒータ)を示し、右側縦軸は操作量を示す。ここで、図7Aの場合は操作量100%が200ボルトを示し、図7Bの場合は操作量100%が4000ワットを示す。この時の設定プロセス温度は700℃であり、設定された供給電圧比(図7Aの場合)および供給電力比(図7Bの場合)はそれぞれ“0.95”と“0.82”である。
0.82”に順次近付けるように変化させて行く。これによって、載置台の 温度分布はセンターホットの状態からセンタークールの状態へ順次移行して行くことになる。
Claims (12)
- 被処理体を載置するための載置台と、
前記載置台に同心状に区画された複数の加熱ゾーン毎に設けられた複数の加熱ヒータ部を有する加熱機構と、
前記載置台の中心部に接続され、前記載置台を水平に支持する脚部と、
前記複数の加熱ゾーンの内の最内周の加熱ゾーンに対応させて設けられた温度測定部と、
前記温度測定部の測定値に基づいて前記最内周の加熱ヒータ部の温度をフィードバック制御するとともに、前記加熱ゾーン間の温度差が前記載置台が破損しない範囲となるように決定された、前記最内周の加熱ヒータ部に対する安全供給電力比で、前記他の加熱ヒータ部への供給電力を制御する電源制御部と
を備えた載置台装置。 - 前記安全供給電力比は、前記載置台の最内周の加熱ゾーンの温度が最も低くなるように設定されている請求項1記載の載置台装置。
- 前記安全供給電力比は、前記載置台が、直径300mmの被処理体に対応するものである時には、前記最内周と最外周の加熱ゾーン間の温度差が33℃以内となるような電力比に設定されている請求項2記載の載置台装置。
- 前記電源制御部は、前記載置台の昇温時および降温時において、最内周の加熱ゾーンの温度が最外周の加熱ゾーンの温度よりも所定の温度差以上低くならないように制御する請求項1に記載の載置台装置。
- 前記電源制御部は、前記載置台の昇温時には最外周よりも最内周の加熱ゾーンの温度が高い状態で昇温し、設定温度に到達したならば前記各加熱ヒータ部への供給電力を前記安全供給電力比に順次近づけるように制御する請求項1に記載の載置台装置。
- 前記温度測定部は、熱電対を有する請求項1に記載の載置台装置。
- 前記載置台および前記脚部の少なくとも一方はセラミック材よりなることを特徴とする請求項1に記載の載置台装置。
- 被処理体に対して所定の熱処理を施す処理装置であって、
内部雰囲気が排気可能になされた処理容器と、
前記処理容器内へ必要なガスを供給するガス供給機構と、
被処理体を載置する載置台装置とを備え、
前記載置台装置は、
被処理体を載置するための載置台と、
前記載置台に同心状に区画された複数の加熱ゾーン毎に設けられた複数の加熱ヒータ部を有する加熱機構と、
前記載置台の中心部に接続され、前記載置台を水平に支持する脚部と、
前記複数の加熱ゾーンの内の最内周の加熱ゾーンに対応させて設けられた温度測定部と、
前記温度測定部の測定値に基づいて前記最内周の加熱ヒータ部の温度をフィードバック制御するとともに、前記加熱ゾーン間の温度差が前記載置台が破損しない範囲となるように決定された、前記最内周の加熱ヒータ部に対する安全供給電力比で、前記他の加熱ヒータ部への供給電力を制御する電源制御部とを有する処理装置。 - 内部雰囲気が排気可能になされた処理容器内に設けられた載置台上に被処理体を載置し、前記載置台に、同心状に区画形成された複数の加熱ゾーン毎に設けられた複数の加熱ヒータ部を有する加熱機構を制御して前記被処理体の温度制御を行う方法であって、
前記複数の加熱ゾーンの内の最内周の加熱ゾーンの温度を測定することと、
前記測定された温度に基づいて前記最内周の加熱ヒータ部をフィードバック制御して設定温度になるように制御することと、
前記加熱ゾーン間の温度差が前記載置台が破損しない範囲となるように決定された、前記最内周の加熱ヒータ部に対する安全供給電力比で、前記他の加熱ヒータ部への供給電力を制御することと
を含む温度制御方法。 - 前記載置台の昇温時において、最内周の加熱ゾーンの温度が最外周の加熱ゾーンの温度よりも所定の温度差以上低くならないような状態に維持する請求項9に記載の温度制御方法。
- 前記載置台の降温時において、最内周の加熱ゾーンの温度が最外周の加熱ゾーンの温度よりも所定の温度差以上低くならないような状態に維持する請求項9に記載の温度制御方法。
- 内部雰囲気が排気可能になされた処理容器内に設けた載置台上に被処理体を載置し、前記載置台に、同心状に区画形成された複数の加熱ゾーン毎に設けられた複数の加熱ヒータ部を有する加熱機構を制御して、前記被処理体の温度制御を行い、被処理体に対して所定の処理を施すに際して、
前記複数の加熱ゾーンの内の最内周の加熱ゾーンの温度を測定することと、
前記測定された温度に基づいて前記最内周の加熱ヒータ部をフィードバック制御して設定温度になるように制御することと、
前記加熱ゾーン間の温度差が前記載置台が破損しない範囲となるように決定された、前記最内周の加熱ヒータ部に対する安全供給電力比で、前記他の加熱ヒータ部への供給電力を制御することと
を含む温度制御方法を行うように、コンピュータに処理装置を制御させるプログラムが記憶された記憶媒体。
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JP5026549B2 (ja) | 2010-04-08 | 2012-09-12 | シャープ株式会社 | 加熱制御システム、それを備えた成膜装置、および温度制御方法 |
CN103628046B (zh) * | 2012-08-24 | 2015-11-11 | 中微半导体设备(上海)有限公司 | 一种调节基片表面温度的控温系统和控温方法 |
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DE102013109155A1 (de) * | 2013-08-23 | 2015-02-26 | Aixtron Se | Substratbehandlungsvorrichtung |
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JP6507953B2 (ja) | 2015-09-08 | 2019-05-08 | 東京エレクトロン株式会社 | 基板処理装置及び基板処理方法 |
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