WO2009063828A1 - ポリイソシアネートの製造方法 - Google Patents

ポリイソシアネートの製造方法 Download PDF

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Publication number
WO2009063828A1
WO2009063828A1 PCT/JP2008/070418 JP2008070418W WO2009063828A1 WO 2009063828 A1 WO2009063828 A1 WO 2009063828A1 JP 2008070418 W JP2008070418 W JP 2008070418W WO 2009063828 A1 WO2009063828 A1 WO 2009063828A1
Authority
WO
WIPO (PCT)
Prior art keywords
polyisocyanate
tar
unpurified
producing polyisocyanate
producing
Prior art date
Application number
PCT/JP2008/070418
Other languages
English (en)
French (fr)
Inventor
Koji Maeba
Haruhiko Noguchi
Tatsuki Kamatsuki
Masaaki Sasaki
Original Assignee
Mitsui Chemicals Polyurethanes, Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Chemicals Polyurethanes, Inc. filed Critical Mitsui Chemicals Polyurethanes, Inc.
Priority to US12/741,792 priority Critical patent/US9035087B2/en
Priority to CN200880112240.3A priority patent/CN101827812B/zh
Priority to EP08850149.9A priority patent/EP2210873B1/en
Publication of WO2009063828A1 publication Critical patent/WO2009063828A1/ja

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/18—Separation; Purification; Stabilisation; Use of additives
    • C07C263/20—Separation; Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

　ポリイソシアネートの製造方法は、未精製ポリイソシアネートを精製する精製工程を含むポリイソシアネートの製造方法において、精製工程は、未精製ポリイソシアネートからタール成分を除去するタール成分除去工程と、タール成分が除去された未精製ポリイソシアネートを、仕切壁蒸留塔により蒸留する蒸留工程とを備えている。
PCT/JP2008/070418 2007-11-14 2008-11-10 ポリイソシアネートの製造方法 WO2009063828A1 (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
US12/741,792 US9035087B2 (en) 2007-11-14 2008-11-10 Process for producing polyisocyanate
CN200880112240.3A CN101827812B (zh) 2007-11-14 2008-11-10 多异氰酸酯的制造方法
EP08850149.9A EP2210873B1 (en) 2007-11-14 2008-11-10 Process for producing polyisocyanate

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-295868 2007-11-14
JP2007295868A JP5479675B2 (ja) 2007-11-14 2007-11-14 トルエンジイソシアネートの製造方法

Publications (1)

Publication Number Publication Date
WO2009063828A1 true WO2009063828A1 (ja) 2009-05-22

Family

ID=40638677

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/070418 WO2009063828A1 (ja) 2007-11-14 2008-11-10 ポリイソシアネートの製造方法

Country Status (7)

Country Link
US (1) US9035087B2 (ja)
EP (1) EP2210873B1 (ja)
JP (1) JP5479675B2 (ja)
KR (1) KR101570549B1 (ja)
CN (1) CN101827812B (ja)
TW (1) TWI458699B (ja)
WO (1) WO2009063828A1 (ja)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101948565A (zh) * 2010-08-18 2011-01-19 广东嘉宝莉化工集团有限公司 一种耐黄变聚氨酯加成物的分离方法
US9421299B2 (en) 2011-03-22 2016-08-23 Sanyo Chemical Industries, Ltd. Medical adhesive

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010039972A2 (en) * 2008-10-02 2010-04-08 Dow Global Technologies Inc. Apparatus, systems, and methods for purification of isocyanate mixtures
CN104093466A (zh) * 2011-09-19 2014-10-08 凯洛格·布朗及鲁特有限公司 用于α-甲基苯乙烯和枯烯蒸馏的分隔壁塔
CN110437108A (zh) 2012-03-19 2019-11-12 科思创德国股份有限公司 制备异氰酸酯的方法
ES2694130T3 (es) * 2013-03-12 2018-12-18 Covestro Deutschland Ag Procedimiento para la preparación de trímeros de TDI con pureza particular
KR102218225B1 (ko) * 2013-03-12 2021-02-22 코베스트로 도이칠란드 아게 담색 tdi-폴리이소시아네이트를 제조하는 방법
HUE049270T2 (hu) 2015-11-02 2020-09-28 Covestro Deutschland Ag Desztillációs oszlop és ennek alkalmazása izocianátok tisztítására
CN109415307B (zh) * 2016-10-26 2021-06-04 三井化学株式会社 五亚甲基二异氰酸酯的制造方法
KR102039089B1 (ko) * 2016-12-15 2019-11-26 한화케미칼 주식회사 톨루엔디이소시아네이트 정제 방법
CN108794350A (zh) * 2017-04-26 2018-11-13 福建省东南电化股份有限公司 一种提高双线tdi生产装置精馏系统的利用率及减少停车次数的方法
CN109704992A (zh) * 2018-12-18 2019-05-03 甘肃银光聚银化工有限公司 一种降低甲苯二异氰酸酯酸度的方法
CN116041219A (zh) * 2022-12-16 2023-05-02 甘肃银光聚银化工有限公司 一种精制五亚甲基二异氰酸酯的方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002128850A (ja) * 2000-10-23 2002-05-09 Nippon Polyurethane Ind Co Ltd 硬質ポリウレタンフォーム用ポリイソシアネート組成物、及びこれを用いた硬質ポリウレタンフォームの製造方法
JP2004143173A (ja) * 2002-10-22 2004-05-20 Bayer Ag トルエンジイソシアネートの精製および製造方法
JP2004155760A (ja) * 2002-06-14 2004-06-03 Bayer Ag 仕切壁蒸留カラムを用いるトルエンジイソシアネートの混合物の精製方法
JP2004155761A (ja) * 2002-06-14 2004-06-03 Bayer Ag トルエンジイソシアネートの混合物を精製するための方法
JP2006510696A (ja) * 2002-12-19 2006-03-30 ビーエーエスエフ　アクチェンゲゼルシャフト イソシアネートを精製するための方法
JP2006281083A (ja) 2005-03-31 2006-10-19 Mitsui Chemicals Polyurethanes Inc 薄膜蒸発装置

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4118286A (en) * 1974-09-25 1978-10-03 Texaco Development Corp. Process for reducing the acidity of organic polymeric isocyanates
JPS61161250A (ja) * 1985-01-11 1986-07-21 Asahi Chem Ind Co Ltd 有機イソシアナ−トの精製法
US5523467A (en) * 1994-03-22 1996-06-04 Mitsui Toatsu Chemicals, Inc. Process for the preparation of aliphatic polyisocyanates
DE10245703A1 (de) * 2002-09-30 2004-04-01 Bayer Ag Verfahren zur Herstellung von Polyisocyanaten der Diphenylmethanreihe durch Phosgenierung von nichtneutralisiertem Polyamin der Diphenylmethanreihe

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002128850A (ja) * 2000-10-23 2002-05-09 Nippon Polyurethane Ind Co Ltd 硬質ポリウレタンフォーム用ポリイソシアネート組成物、及びこれを用いた硬質ポリウレタンフォームの製造方法
JP2004155760A (ja) * 2002-06-14 2004-06-03 Bayer Ag 仕切壁蒸留カラムを用いるトルエンジイソシアネートの混合物の精製方法
JP2004155761A (ja) * 2002-06-14 2004-06-03 Bayer Ag トルエンジイソシアネートの混合物を精製するための方法
JP2004143173A (ja) * 2002-10-22 2004-05-20 Bayer Ag トルエンジイソシアネートの精製および製造方法
JP2006510696A (ja) * 2002-12-19 2006-03-30 ビーエーエスエフ　アクチェンゲゼルシャフト イソシアネートを精製するための方法
JP2006281083A (ja) 2005-03-31 2006-10-19 Mitsui Chemicals Polyurethanes Inc 薄膜蒸発装置

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of EP2210873A4 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101948565A (zh) * 2010-08-18 2011-01-19 广东嘉宝莉化工集团有限公司 一种耐黄变聚氨酯加成物的分离方法
CN101948565B (zh) * 2010-08-18 2012-05-30 嘉宝莉化工集团股份有限公司 一种耐黄变聚氨酯加成物的分离方法
US9421299B2 (en) 2011-03-22 2016-08-23 Sanyo Chemical Industries, Ltd. Medical adhesive
JP6040149B2 (ja) * 2011-03-22 2016-12-07 三洋化成工業株式会社 医療用接着剤

Also Published As

Publication number Publication date
EP2210873B1 (en) 2014-02-12
EP2210873A4 (en) 2011-07-13
KR20100101088A (ko) 2010-09-16
US20100249450A1 (en) 2010-09-30
TWI458699B (zh) 2014-11-01
KR101570549B1 (ko) 2015-11-19
CN101827812A (zh) 2010-09-08
CN101827812B (zh) 2013-06-05
JP2009120528A (ja) 2009-06-04
US9035087B2 (en) 2015-05-19
TW200934753A (en) 2009-08-16
EP2210873A1 (en) 2010-07-28
JP5479675B2 (ja) 2014-04-23

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