WO2009011225A1 - ４－フルオロ－１，３－ジオキソラン－２－オンの製造方法 - Google Patents

４－フルオロ－１，３－ジオキソラン－２－オンの製造方法 Download PDF

Info

Publication number
WO2009011225A1
WO2009011225A1 PCT/JP2008/061971 JP2008061971W WO2009011225A1 WO 2009011225 A1 WO2009011225 A1 WO 2009011225A1 JP 2008061971 W JP2008061971 W JP 2008061971W WO 2009011225 A1 WO2009011225 A1 WO 2009011225A1
Authority
WO
WIPO (PCT)
Prior art keywords
dioxolan
fluoro
chloro
chlorine radicals
produced
Prior art date
Application number
PCT/JP2008/061971
Other languages
English (en)
French (fr)
Inventor
Akiyoshi Yamauchi
Michiru Tanaka
Meiten Koh
Original Assignee
Daikin Industries, Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daikin Industries, Ltd. filed Critical Daikin Industries, Ltd.
Priority to CN200880024559.0A priority Critical patent/CN101743236B/zh
Publication of WO2009011225A1 publication Critical patent/WO2009011225A1/ja

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
    • C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
    • C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D317/42—Halogen atoms or nitro radicals

Abstract

　４－クロロ－１，３－ジオキソラン－２－オンを出発物質とし、これをフッ素化剤でフッ素化する製造方法において、高収率を維持しながら短時間で高純度の４－フルオロ－１，３－ジオキソラン－２－オンを製造できる製造方法を提供する。有機溶媒中にて、４－クロロ－１，３－ジオキソラン－２－オン１モルに対して、１．４モル以上のフッ素化剤を添加して反応させて塩素根を含む４－フルオロ－１，３－ジオキソラン－２－オンを得た後、必要に応じて中間処理工程を施し、さらに、得られた塩素根を含む４－フルオロ－１，３－ジオキソラン－２－オンを蒸留により精製することで、塩素根含有量が低減化された４－フルオロ－１，３－ジオキソラン－２－オンを製造する。
PCT/JP2008/061971 2007-07-13 2008-07-02 ４－フルオロ－１，３－ジオキソラン－２－オンの製造方法 WO2009011225A1 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN200880024559.0A CN101743236B (zh) 2007-07-13 2008-07-02 4-氟-1,3-二氧戊环-2-酮的制造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007184442A JP5135926B2 (ja) 2007-07-13 2007-07-13 ４−フルオロ−１，３−ジオキソラン−２−オンの製造方法
JP2007-184442 2007-07-13

Publications (1)

Publication Number Publication Date
WO2009011225A1 true WO2009011225A1 (ja) 2009-01-22

Family

ID=40259563

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/061971 WO2009011225A1 (ja) 2007-07-13 2008-07-02 ４－フルオロ－１，３－ジオキソラン－２－オンの製造方法

Country Status (4)

Country Link
JP (1) JP5135926B2 (ja)
KR (1) KR20100031552A (ja)
CN (1) CN101743236B (ja)
WO (1) WO2009011225A1 (ja)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102993160A (zh) * 2012-09-26 2013-03-27 中国海洋石油总公司 一种氟代碳酸乙烯酯的合成方法

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5358974B2 (ja) * 2008-02-28 2013-12-04 ダイキン工業株式会社 フッ素化１，３−ジオキソラン−２−オンの製造方法
TW201121938A (en) * 2009-09-28 2011-07-01 Solvay Fluor Gmbh Manufacture of difluoroethylene carbonate, trifluoroethylene carbonate and tetrafluoroethylene carbonate
CN102060838A (zh) * 2010-12-31 2011-05-18 浙江华晶氟化学科技有限公司 一种氟代碳酸乙烯酯的制备方法
CN106916136B (zh) * 2017-03-01 2019-06-14 山东永浩新材料科技有限公司 一种氟代碳酸乙烯酯的合成方法
CN110637001B (zh) * 2017-06-22 2022-05-27 日本瑞翁株式会社 八氟环戊烯的制造方法
CN110156743A (zh) * 2019-05-24 2019-08-23 泰兴华盛精细化工有限公司 一种氟代碳酸乙烯酯的合成方法
CN113402496B (zh) * 2021-07-07 2022-03-25 山东海科创新研究院有限公司 二甲基乙酰胺在制备氟代碳酸乙烯酯中的应用
CN114621177B (zh) * 2022-02-24 2023-04-07 浙江诺亚氟化工有限公司 一种氟代碳酸乙烯酯的制备方法
CN117624110B (zh) * 2023-12-06 2024-05-03 珠海百川石化工程设计有限公司 一种氟代碳酸乙烯酯的合成方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007008825A (ja) * 2005-06-28 2007-01-18 Central Glass Co Ltd 高純度の４−フルオロ−１，３−ジオキソラン−２−オンの製造方法
JP2007008826A (ja) * 2005-06-28 2007-01-18 Central Glass Co Ltd 高純度の４−フルオロ−１，３−ジオキソラン−２−オンの製造方法
CN101066965A (zh) * 2007-06-01 2007-11-07 张家港市华盛化学有限公司 氟代环状碳酸酯的制备方法

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE69702618D1 (de) * 1996-10-03 2000-08-24 Ca Nat Research Council Elektrolyt mit fluoro-ethylen- und propylenkarbonaten für alkalische metallionensekundärbatterien

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007008825A (ja) * 2005-06-28 2007-01-18 Central Glass Co Ltd 高純度の４−フルオロ−１，３−ジオキソラン−２−オンの製造方法
JP2007008826A (ja) * 2005-06-28 2007-01-18 Central Glass Co Ltd 高純度の４−フルオロ−１，３−ジオキソラン−２−オンの製造方法
CN101066965A (zh) * 2007-06-01 2007-11-07 张家港市华盛化学有限公司 氟代环状碳酸酯的制备方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102993160A (zh) * 2012-09-26 2013-03-27 中国海洋石油总公司 一种氟代碳酸乙烯酯的合成方法

Also Published As

Publication number Publication date
JP2009019019A (ja) 2009-01-29
KR20100031552A (ko) 2010-03-22
JP5135926B2 (ja) 2013-02-06
CN101743236B (zh) 2013-04-10
CN101743236A (zh) 2010-06-16

Similar Documents

Publication Publication Date Title
WO2009011225A1 (ja) ４－フルオロ－１，３－ジオキソラン－２－オンの製造方法
ATE542807T1 (de) Verfahren zur herstellung von propylenoxid
JP2008540615A5 (ja)
MY150754A (en) Method of producing xylitol using hydrolysate containing xylose and arabinose prepared from byproduct of tropical fruit biomass
TW200700360A (en) Process for converting polyhydroxylated aliphatic hydrocarbons into chlorohydrins
WO2008111557A1 (ja) 光学活性エポキシ化合物の製造方法
EA200800129A1 (ru) Псевдоазеотропная композиция, содержащая дихлорпропанол, и способ ее получения
BRPI0813576A2 (pt) Método para a produção de óxido de propileno
WO2009063487A3 (en) An improved process for manufacture of epoxides, particularly epichlorohydrin
WO2009022676A1 (ja) 五フッ化リン及び六フッ化リン酸塩の製造方法
ATE530537T1 (de) VERFAHREN ZUR HERSTELLUNG VON MONOCHLORETHYLENCARBONAT UND ZU DESSEN ANSCHLIEßENDER UMWANDLUNG IN VINYLENCARBONAT
GB2539158A (en) Bis(1, 1-dichloro-3,3,3-trifluoropropyl)ether and method for producing same
WO2008087657A3 (en) A process for preparing epichlorohydrin
WO2008090755A1 (ja) 光学活性α－フルオロカルボン酸エステルの製造方法
WO2008099882A1 (ja) ２－メチル－３－（３，４－メチレンジオキシフェニル）プロパナール及びその製造方法
MX2013013386A (es) Metodo para mitigar la formacion de subproductos durante la produccion de compuestos haloalcano.
EP2357168B1 (en) Method for producing fluorosulfuric acid ester
IN2014DN02166A (ja)
WO2010030132A3 (ko) 아데포비어 디피복실의 정제방법
EP1726588A4 (en) HIGHLY EXCLUSIVE ALICYCLIC EPOXY COMPOUND, PROCESS FOR THE PRODUCTION THEREOF, HARDENABLE EPOXY RESIN COMPOSITION, CURED PRODUCTS THEREOF PRODUCED, AND APPLICATION
EP1352892A4 (en) METHODS FOR PRODUCING FLUORINATED ESTER, FLUORINATED ACYL FLUORIDE AND FLUORINATED VINYL ETHER
ATE374760T1 (de) Verfahren zur herstellung von 4-fluor-1,3- dioxolan-2-on
WO2010013576A8 (en) Process for producing fluorine-containing propene compound
TW200504003A (en) Method for producing ditrimethylolpropane
AR044296A1 (es) Metodo para la racemizacion de la (s) - (+) y de la (r) - (-) -10, 11-dihidro-10-hidroxi-5h-dibenz [b,f] azepin-5- carboxamida, y mezclas opticamente enriquecidas de las mismas

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 200880024559.0

Country of ref document: CN

121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 08777774

Country of ref document: EP

Kind code of ref document: A1

NENP Non-entry into the national phase

Ref country code: DE

ENP Entry into the national phase

Ref document number: 20107003225

Country of ref document: KR

Kind code of ref document: A

122 Ep: pct application non-entry in european phase

Ref document number: 08777774

Country of ref document: EP

Kind code of ref document: A1