WO2008146368A1 - 高耐食性希土類永久磁石の製造方法及び使用方法 - Google Patents

高耐食性希土類永久磁石の製造方法及び使用方法 Download PDF

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Publication number
WO2008146368A1
WO2008146368A1 PCT/JP2007/060947 JP2007060947W WO2008146368A1 WO 2008146368 A1 WO2008146368 A1 WO 2008146368A1 JP 2007060947 W JP2007060947 W JP 2007060947W WO 2008146368 A1 WO2008146368 A1 WO 2008146368A1
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WO
WIPO (PCT)
Prior art keywords
rare earth
permanent magnet
earth permanent
same
highly anticorrosive
Prior art date
Application number
PCT/JP2007/060947
Other languages
English (en)
French (fr)
Inventor
Kazuo Tamura
Original Assignee
Shin-Etsu Chemical Co., Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shin-Etsu Chemical Co., Ltd. filed Critical Shin-Etsu Chemical Co., Ltd.
Priority to US12/522,779 priority Critical patent/US8105444B2/en
Priority to CN2007800502379A priority patent/CN101589445B/zh
Priority to KR1020097015556A priority patent/KR101317800B1/ko
Priority to JP2009516106A priority patent/JP4873201B2/ja
Priority to PCT/JP2007/060947 priority patent/WO2008146368A1/ja
Priority to EP07744366.1A priority patent/EP2110823B1/en
Publication of WO2008146368A1 publication Critical patent/WO2008146368A1/ja

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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
    • H01F1/032—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials
    • H01F1/04—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials metals or alloys
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00—Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/06—Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases
    • C23C8/08—Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases only one element being applied
    • C23C8/10—Oxidising
    • C23C8/12—Oxidising using elemental oxygen or ozone
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/73—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals characterised by the process
    • C23C22/74—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals characterised by the process for obtaining burned-in conversion coatings
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
    • C23C28/04—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/48—After-treatment of electroplated surfaces
    • C25D5/50—After-treatment of electroplated surfaces by heat-treatment
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D7/00—Electroplating characterised by the article coated
    • C25D7/001—Magnets
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F41/00—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
    • H01F41/02—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F41/00—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
    • H01F41/02—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets
    • H01F41/0253—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets for manufacturing permanent magnets
    • H01F41/026—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets for manufacturing permanent magnets protecting methods against environmental influences, e.g. oxygen, by surface treatment
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
    • H01F1/032—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials
    • H01F1/04—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials metals or alloys
    • H01F1/047—Alloys characterised by their composition
    • H01F1/053—Alloys characterised by their composition containing rare earth metals
    • H01F1/055—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5
    • H01F1/057—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B
    • H01F1/0571—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes
    • H01F1/0575—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together
    • H01F1/0577—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and IIIa elements, e.g. Nd2Fe14B in the form of particles, e.g. rapid quenched powders or ribbon flakes pressed, sintered or bonded together sintered
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F41/00—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
    • H01F41/14—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for applying magnetic films to substrates
    • H01F41/24—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for applying magnetic films to substrates from liquids
    • H01F41/26—Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for applying magnetic films to substrates from liquids using electric currents, e.g. electroplating

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Power Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Electrochemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • General Chemical & Material Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing Cores, Coils, And Magnets (AREA)
  • Hard Magnetic Materials (AREA)
  • Electroplating Methods And Accessories (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Other Surface Treatments For Metallic Materials (AREA)

Abstract

　Ｒ－Ｆｅ－Ｂ系焼結磁石を切断及び／又は研磨して表面の加工仕上げを行い、メッキ前処理をした後、電気ニッケルメッキにより所定の厚みにメッキ処理を行い、リン酸塩を含む水溶液に浸漬した後、水洗し、次いで酸素分圧が１．３×１０3Ｐａ以上の雰囲気下において、１５０～４００°Cにて１～２４時間熱処理し、表層部に薄いニッケル酸化物層を形成させることを特徴とする高耐食性希土類永久磁石の製造方法。
PCT/JP2007/060947 2007-05-30 2007-05-30 高耐食性希土類永久磁石の製造方法及び使用方法 WO2008146368A1 (ja)

Priority Applications (6)

Application Number Priority Date Filing Date Title
US12/522,779 US8105444B2 (en) 2007-05-30 2007-05-30 Process for producing highly anticorrosive rare earth permanent magnet and method of using the same
CN2007800502379A CN101589445B (zh) 2007-05-30 2007-05-30 高耐蚀性稀土永磁体的制造方法及其使用方法
KR1020097015556A KR101317800B1 (ko) 2007-05-30 2007-05-30 고내식성 희토류 영구자석의 제조방법 및 사용방법
JP2009516106A JP4873201B2 (ja) 2007-05-30 2007-05-30 高耐食性希土類永久磁石の製造方法及び使用方法
PCT/JP2007/060947 WO2008146368A1 (ja) 2007-05-30 2007-05-30 高耐食性希土類永久磁石の製造方法及び使用方法
EP07744366.1A EP2110823B1 (en) 2007-05-30 2007-05-30 Process for producing highly anticorrosive rare earth permanent magnet and method of using the same

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/JP2007/060947 WO2008146368A1 (ja) 2007-05-30 2007-05-30 高耐食性希土類永久磁石の製造方法及び使用方法

Publications (1)

Publication Number Publication Date
WO2008146368A1 true WO2008146368A1 (ja) 2008-12-04

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Country Status (6)

Country Link
US (1) US8105444B2 (ja)
EP (1) EP2110823B1 (ja)
JP (1) JP4873201B2 (ja)
KR (1) KR101317800B1 (ja)
CN (1) CN101589445B (ja)
WO (1) WO2008146368A1 (ja)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010273426A (ja) * 2009-05-20 2010-12-02 Toshiba Corp 永久磁石モータ
JP2017043832A (ja) * 2015-08-25 2017-03-02 住友金属鉱山株式会社 希土類元素を含む鉄系合金微粉末の製造方法、希土類元素を含む鉄系合金微粉末
CN109136897A (zh) * 2018-10-10 2019-01-04 高飞 一种氮化金属锰磷化液配方及其处理方法
WO2023119908A1 (ja) * 2021-12-24 2023-06-29 愛知製鋼株式会社 希土類磁石粉末、その製造方法およびボンド磁石

Families Citing this family (14)

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CN102117692B (zh) * 2009-12-30 2014-12-31 北京中科三环高技术股份有限公司 具有多层复合电镀层的稀土永磁体及在其上进行复合电镀的方法
US9558885B2 (en) * 2010-06-30 2017-01-31 Hitachi Metals, Ltd. Method for producing surface-modified rare earth metal-based sintered magnet
CN102456458B (zh) * 2010-10-15 2017-02-08 中国科学院宁波材料技术与工程研究所 高耐蚀性烧结钕铁硼磁体及其制备方法
CN102586682B (zh) * 2011-01-17 2016-01-20 三环瓦克华（北京）磁性器件有限公司 一种高性能稀土永磁烧结磁体及其制造方法
CN102436891A (zh) * 2011-12-06 2012-05-02 常熟市碧溪新城特种机械厂 稀土磁铁
CN103426578B (zh) * 2012-05-22 2016-04-27 比亚迪股份有限公司 一种稀土永磁材料及其制备方法
DE102013019499A1 (de) * 2013-11-21 2015-05-21 Linde Aktiengesellschaft Kolbenverdichter und Verfahren zum Verdichten eines tiefkalten, gasförmigen Mediums, insbesondere Wasserstoff
CN105161240A (zh) * 2015-10-13 2015-12-16 南通长江电器实业有限公司 一种高性能稀土永磁材料
CN105374490A (zh) * 2015-12-16 2016-03-02 南通长江电器实业有限公司 一种耐腐蚀稀土永磁材料
CN105679482A (zh) * 2016-04-18 2016-06-15 赣州诚博科技服务有限公司 钕铁硼永磁材料及其制备方法
CN106637122A (zh) * 2016-12-20 2017-05-10 薛亚红 钕铁硼铁氧体防腐的处理方法
CN109836176B (zh) * 2018-12-25 2021-11-09 安徽中马磁能科技股份有限公司 一种永磁铁氧体磁瓦的除锈工艺
CN114420439B (zh) * 2022-03-02 2022-12-27 浙江大学 高温氧化处理提高高丰度稀土永磁抗蚀性的方法
CN115862988B (zh) * 2022-12-20 2023-07-25 东莞金坤新材料股份有限公司 一种防锈式钕铁硼永磁材料及制造方法

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010273426A (ja) * 2009-05-20 2010-12-02 Toshiba Corp 永久磁石モータ
JP2017043832A (ja) * 2015-08-25 2017-03-02 住友金属鉱山株式会社 希土類元素を含む鉄系合金微粉末の製造方法、希土類元素を含む鉄系合金微粉末
CN109136897A (zh) * 2018-10-10 2019-01-04 高飞 一种氮化金属锰磷化液配方及其处理方法
WO2023119908A1 (ja) * 2021-12-24 2023-06-29 愛知製鋼株式会社 希土類磁石粉末、その製造方法およびボンド磁石
WO2023119612A1 (ja) * 2021-12-24 2023-06-29 愛知製鋼株式会社 希土類磁石粉末およびその製造方法

Also Published As

Publication number Publication date
KR101317800B1 (ko) 2013-10-15
EP2110823B1 (en) 2017-03-01
EP2110823A4 (en) 2010-05-26
US8105444B2 (en) 2012-01-31
CN101589445A (zh) 2009-11-25
US20100013585A1 (en) 2010-01-21
CN101589445B (zh) 2012-10-24
EP2110823A1 (en) 2009-10-21
JPWO2008146368A1 (ja) 2010-08-12
JP4873201B2 (ja) 2012-02-08
KR20100014335A (ko) 2010-02-10

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