WO2005052214A2 - Verfahren und vorrichtung zur herstellung eines oder mehrerer gase - Google Patents
Verfahren und vorrichtung zur herstellung eines oder mehrerer gase Download PDFInfo
- Publication number
- WO2005052214A2 WO2005052214A2 PCT/EP2004/013452 EP2004013452W WO2005052214A2 WO 2005052214 A2 WO2005052214 A2 WO 2005052214A2 EP 2004013452 W EP2004013452 W EP 2004013452W WO 2005052214 A2 WO2005052214 A2 WO 2005052214A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- gas
- ion exchanger
- produced
- substance
- adheres
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/02—Hydrogen or oxygen
- C25B1/04—Hydrogen or oxygen by electrolysis of water
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/36—Hydrogen production from non-carbon containing sources, e.g. by water electrolysis
Definitions
- the invention relates to a method for producing one or more gases and a device for carrying out such a method.
- a liquid containing the gas to be produced is treated electrolytically.
- One or more gases are formed by the electrolysis.
- the method serves to produce hydrogen or hydrogen and oxygen, the latter in particular as a mixture (detonating gas).
- a device for the electrolytic production of hydrogen and oxygen which has an anode chamber and a cathode chamber, in which electrically conductive ultramicroelectrode particles are present, which are in contact with the cathode and the anode and which are used for Improve conductivity and minimize overvoltages.
- DE 100 16 591 C2 discloses a process for the production of hydrogen, in which a first electrolyte is provided in the interior of a micro hollow fiber and a second electrolyte is provided outside the micro hollow fiber.
- the micro hollow fiber carries anode and cathode separately on its wall surfaces.
- US 2001/0050234 A1 discloses an electrolysis cell with a first electrode and a second electrode, between which an electrolyte membrane is arranged.
- An electron exchange resin can be used for the electrolyte membrane.
- the object of the invention is to propose an improved method of the type specified at the outset.
- a substance is present in the liquid, to which the or one of the gases to be produced by the electrolysis adheres. This gas preferably adheres to this substance in an ionic bond.
- the gas to be produced is preferably hydrogen.
- the gases to be produced can be hydrogen and oxygen. It is possible to produce hydrogen and oxygen separately. However, it is also possible to produce hydrogen and oxygen in a mixture (detonating gas).
- the native production of oxyhydrogen is particularly advantageous. According to the method according to the invention, the oxyhydrogen gas can be mixed in the correct be created. It can be used in this form, especially for power generation.
- the liquid containing the gas or a gas to be produced is preferably water.
- a further advantageous development is characterized in that the substance to which the gas or a gas to be produced adheres is an ion exchanger.
- this substance can be an ion exchange resin.
- the ion exchanger is preferably an acidic, in particular a strongly acidic, ion exchanger.
- the substance to which the gas or a gas to be produced adheres or the ion exchanger can be in the form of a gel.
- the ion exchanger has or consists of a matrix, anchor groups and ions to be exchanged.
- the matrix can in particular be a cross-linked plastic, in particular cross-linked polystyrene.
- the anchor groups are preferably sulfonic acid groups (SO 3 ).
- the ions to be exchanged are preferably hydrogen ions (H).
- the ion exchanger can have the general chemical formula R-SO 3 -H.
- a further advantageous development is characterized in that the substance to which the gas or a gas to be produced adheres, or the ion exchanger, in particular the ion exchanger base material, contains catalytically active substances.
- the catalytically active substances can be, in particular, current-conducting substances, in particular current-conducting foils.
- the catalytically active substances can be mixed with the substance or the ion exchanger or the ion exchanger base material.
- the substance to which the gas or a gas to be produced adheres or the ion exchanger or the ion exchanger base material contains enzymes which act catalytically and / or gas. Organic acids, in particular tartaric acid, are preferably used as such enzymes.
- the enzymes can be added to the substance or the ion exchanger or the ion exchange resin or the ion exchanger base material.
- a device according to the invention for carrying out the method according to the invention is characterized by the features of claim 15. It comprises a container with a liquid and a positive electrode and a negative electrode which can be connected or are connected to a power source. A substance is present in the liquid to which the or one of the gases to be produced during electrolysis adheres.
- An electrode is preferably of tubular design.
- a filling material can be present in the liquid which contains the gas to be produced and a substance to which the gas to be produced adheres, in particular within the tubular electrode.
- This material is preferably cotton.
- An acid is preferably present in the filler material. This material is preferably wetted with an acid.
- the acid is preferably hydrochloric acid.
- the invention makes it possible to use a substance to which the gas or a gas to be produced adheres, in particular an ion exchanger, in which the marginal groups adhering to it by ion binding and / or by Van der Waals forces are released during electrolysis ,
- the device shown in the single figure comprises a container 1 which is designed to be rotationally symmetrical about the central axis 2 and which consists of a tubular housing 3 which is closed off by an upper cover 4 and a lower cover 5.
- the entire device is preferably longer than shown.
- An annular outer electrode 6 is provided on the inner wall of the housing 3. Inside the housing 3 there is a tubular inner electrode 7. The container 1 is filled with water 9 up to the water level 8.
- An ion exchanger 10 is present between the electrodes 6 and 7 and is present in gel form up to the height 11.
- the outer electrode 6 is connected via a switch 12 to the positive pole of a current source 13, for example a 12V car battery.
- the negative pole of the current source 13 is connected to the inner electrode 7.
- the polarity can also be reversed.
- the water level 8 lies above the height 11 of the gel-shaped ion exchanger 10 and above the tube of the inner electrode 7, which is open at the top.
- the electrode 7 can also be designed to be closed. Another possibility is that the electrode 7 projects above the water level 8.
- the height 11 of the gel-shaped ion exchanger 10 is just below the upper end of the outer electrode 6.
- the device can also be designed such that this height 11 is above the upper end of the electrode 6.
- the inner electrode 7 can be closed or open at the bottom. It can also be open at its lower end or can be sealingly connected to the lower cover 5.
- the ion exchanger 10 is a strongly acidic, gel-like ion exchanger with sulfonic acid groups as anchor groups.
- the ion exchanger has the general chemical formula R - SO 3 - H, where R denotes a matrix, in particular a crosslinked polystyrene matrix, SO 3 a sulfonic acid anchor group and H hydrogen.
- the ion exchanger 10 is preferably kept in motion. This is preferably done in such a way that the ion exchanger 10 does not sink.
- the ion exchange shear can be kept in motion by a fluidized bed process. If the ion exchanger is kept in motion, gas formation and electron flow are improved.
- the ion exchanger is kept in suspension in the liquid. This is preferably done in that the ion exchanger or the ion exchanger base material is produced in such a way that they remain in suspension in the liquid, that is to say in the water 9.
- the process can be carried out continuously.
- the ion exchanger 10 can be continuously supplied and removed (not shown in the drawing).
- the removed ion exchanger can be regenerated and fed again.
- the process can also be carried out in several stages.
- the gas that forms can be drawn off from the space 14. For this purpose it is possible to create a vacuum in this space 14. In this way it can also be achieved that the gas withdrawing upwards entrains the ion exchanger 10 and in this way brings about a mixing and distribution of the ion exchanger 10.
- the pressure and temperature can be adjusted so that the process works with optimal efficiency.
- Example 1 The following measured values were determined in practical tests: Example 1 :
- Experiment No. 1 is a comparative experiment which was carried out in water without an ion exchanger. A small amount of ion exchanger was used in Experiment No. 2. Experiment No. 3 was carried out with a large amount of ion exchangers. In experiment No. 4, a small amount of hydrochloric acid was also added.
- the addition of the ion exchanger increases the current depending on the amount added, from 3.0 to 7.5 A, while the voltage drops accordingly from 9.2 V to 6.5 V.
- the amount of oxyhydrogen produced increases over 40 ml / min to 100 ml / min.
- the efficiency increases over 0.260 to 0.370.
- the experimental arrangement shown in the single figure was used, but the polarity was reversed.
- the housing 3 forming the minus electrode is designed as a tube with a length of 116 mm, an inner diameter of 26 mm and an outer diameter of 28 mm.
- the inner electrode 7 forming the plus electrode is designed as a tube with a length of 116 mm, an inner diameter of 14 mm and an outer diameter of 16 mm.
- a battery charger is used as the current source 13, which emits direct current with a voltage of 12V.
- Amberlit styrene DVB which is in the form of dark amber balls, was used as the ion exchanger. The functional group of this ion exchanger is formed by sulfonic acid.
- the inside of the inner electrode 7 was filled with cotton wool (without any further additive).
- the electrode arrangement is filled with 50 ml of drinking water, which corresponds to a quantity of 2.75 mol.
- the entire arrangement is completely "submerged" so that a liquid exchange can take place between the interior of the inner electrode 7 and the annular space between the inner electrode 7 and the housing 3, both via the upper end of the inner electrode 7 and over the lower end, ie the space between the lower end of the inner electrode 7 and the lower cover 5.
- the drinking water has a pH of 7.0, an electrical conductivity of 266 ⁇ S / cm (at 25 ° C) and a Water hardness of 5.4 dH °
- the following values for the current, the voltage, the power and the mass of detonating gas (KG) formed per time result, which is given as the standard volume , using the ion exchanger already described:
- Oxygen gas was generated at 5.0 ml / min. This amount is already doubled by adding 1 ml of ion exchanger. The amount of oxyhydrogen produced per minute increases with the increase in the amount of ion exchanger.
- the process according to the invention can be carried out in such a way that a substance to which the gas to be produced adheres, in particular in ionic bonding, for example an acidic cation exchanger, is added as a catalyst and donor in the electrolysis of a liquid, in particular water, so that the decomposition of the decomposing substance, for example water, is accelerated many times over, the added substance being no acid and no base and no ion exchange membrane.
- a substance to which the gas to be produced adheres in particular in ionic bonding, for example an acidic cation exchanger
- an ion exchanger for example in the electrolysis of water for the production of hydrogen and oxygen or oxyhydrogen, is added to the electrolysis process known per se, which serves as a catalyst for increasing the current flow and at the same time as hydrogen - And / or oxygen donor can contribute to the implementation of the method.
- efficiencies of 0.6 to 0.85 can be achieved at a current of 3900 C / min, for example.
- a corresponding device can produce oxyhydrogen in an amount of 14.6 l / h.
- the device for manufacturing position of the oxyhydrogen can be part of an engine and natively generate the oxyhydrogen required for the engine. In this way, liquefaction and storage of the oxyhydrogen gas can be made superfluous, since it can be generated continuously in the required amount.
- a filling material in particular cotton wool, can be present in the interior of the tubular electrode 7.
- This material or the cotton wool can be wetted with acid, preferably hydrochloric acid.
- acid preferably hydrochloric acid.
- the electrolytically treated liquid can be water. However, other liquids are also possible which contain the gas to be produced, e.g. Hydrogen or another substance.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Description
Claims
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/581,009 US8197666B2 (en) | 2003-11-28 | 2004-11-26 | Method and apparatus for the manufacture of one or more gases |
KR1020067009723A KR101218952B1 (ko) | 2003-11-28 | 2004-11-26 | 하나 이상의 가스 생산 방법 및 장치 |
CA2547295A CA2547295C (en) | 2003-11-28 | 2004-11-26 | A method and an apparatus for the manufacture of one or more gases |
AU2004293566A AU2004293566B2 (en) | 2003-11-28 | 2004-11-26 | Method and device for producing one or several gases |
JP2006540400A JP5094122B2 (ja) | 2003-11-28 | 2004-11-26 | 1種以上のガスを生成する方法および装置 |
EP04819229.8A EP1704268B1 (de) | 2003-11-28 | 2004-11-26 | Verfahren und vorrichtung zur herstellung eines gases oder mehrerer gase |
Applications Claiming Priority (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10355592.7 | 2003-11-28 | ||
DE10355592 | 2003-11-28 | ||
DE10359509A DE10359509B4 (de) | 2003-11-28 | 2003-12-18 | Verfahren zur Herstellung eines oder mehrerer Gase |
DE10359509.0 | 2003-12-18 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2005052214A2 true WO2005052214A2 (de) | 2005-06-09 |
WO2005052214A3 WO2005052214A3 (de) | 2005-09-15 |
Family
ID=34635114
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2004/013452 WO2005052214A2 (de) | 2003-11-28 | 2004-11-26 | Verfahren und vorrichtung zur herstellung eines oder mehrerer gase |
Country Status (8)
Country | Link |
---|---|
US (1) | US8197666B2 (de) |
EP (1) | EP1704268B1 (de) |
JP (1) | JP5094122B2 (de) |
KR (1) | KR101218952B1 (de) |
AU (1) | AU2004293566B2 (de) |
CA (1) | CA2547295C (de) |
RU (1) | RU2385363C2 (de) |
WO (1) | WO2005052214A2 (de) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2006128527A2 (de) * | 2005-05-30 | 2006-12-07 | Roiner, Maria | Vorrichtung zur durchführung eines verfahrens zur herstellung eines oder mehrerer gase |
JP2008510691A (ja) * | 2004-08-20 | 2008-04-10 | ベーリンガー インゲルハイム インターナショナル ゲゼルシャフト ミット ベシュレンクテル ハフツング | Plkインヒビターとしてのピリミジン化合物 |
WO2011031763A1 (en) | 2009-09-11 | 2011-03-17 | Geo Firewall Sarl | Regulating a hydrocarbon combustion process using a set of data indicative of hydrocarbon fuel consumed corresponding to a monitored engine operating characteristic |
WO2011031797A1 (en) * | 2009-09-11 | 2011-03-17 | Geo Firewall Sàrl | System for regulating a hydrocarbon combustion process using a substantially stoichiometric mix of hydrogen and oxygen |
DE202012012463U1 (de) | 2012-11-12 | 2013-02-25 | Jakob Propp | Elektrolyseeinrichtung zur Erzeugung mindestens eines Reaktionsprodukts und einer Anlage zum Bereitstellen des erzeugten Reaktionsproduktes für einen Verbraucher |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100925750B1 (ko) * | 2007-09-20 | 2009-11-11 | 삼성전기주식회사 | 수소 발생 장치용 전해질 용액 및 이를 포함하는 수소 발생장치 |
FI121928B (fi) * | 2008-10-08 | 2011-06-15 | Teknillinen Korkeakoulu | Sähköntuottojärjestelmä |
US9040012B2 (en) | 2009-02-17 | 2015-05-26 | Mcalister Technologies, Llc | System and method for renewable resource production, for example, hydrogen production by microbial electrolysis, fermentation, and/or photosynthesis |
MY187664A (en) | 2009-02-17 | 2021-10-08 | Mcalister Tech Llc | Apparatus and method for gas capture during electrolysis |
RU2484182C2 (ru) | 2009-02-17 | 2013-06-10 | МАКЭЛИСТЭР ТЕКНОЛОДЖИЗ, ЭлЭлСи | Электролитическая ячейка и способ ее применения |
US8075750B2 (en) | 2009-02-17 | 2011-12-13 | Mcalister Technologies, Llc | Electrolytic cell and method of use thereof |
WO2010096504A1 (en) | 2009-02-17 | 2010-08-26 | Mcalister Technologies, Llc | Apparatus and method for controlling nucleation during electrolysis |
US20110233069A1 (en) * | 2010-03-24 | 2011-09-29 | Rasirc | Method and system for electrochemical hydrogen generation |
KR20130081578A (ko) * | 2012-01-09 | 2013-07-17 | 삼성전자주식회사 | 전기 재생 연수 장치 및 이의 운전방법 |
US9127244B2 (en) | 2013-03-14 | 2015-09-08 | Mcalister Technologies, Llc | Digester assembly for providing renewable resources and associated systems, apparatuses, and methods |
US10390494B2 (en) * | 2016-01-20 | 2019-08-27 | Nano Evaporative Technologies, Inc. | Hydroponic electroculture system and methods of use |
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WO1990015659A1 (en) * | 1989-06-16 | 1990-12-27 | Olin Corporation | Process for removing ionizable impurities from non-aqueous fluids |
US5348683A (en) * | 1990-02-06 | 1994-09-20 | Olin Corporation | Chloric acid - alkali metal chlorate mixtures and chlorine dioxide generation |
US5401371A (en) * | 1992-07-16 | 1995-03-28 | Aisin Seiki Kabushiki Kaisha | Hydrogen generator |
EP0650929A1 (de) * | 1993-10-27 | 1995-05-03 | Halox Technologies Corporation | Elektrolytisches Verfahren und Vorrichting zur kontrollierten Oxydation oder Reduktion von Stoffen in wässriger Lösung |
JP2000265290A (ja) * | 1999-03-18 | 2000-09-26 | Matsushita Refrig Co Ltd | 水電解装置 |
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DE3062824D1 (en) * | 1979-08-07 | 1983-05-26 | Agfa Gevaert Nv | Rotary cross-cutting apparatus for cutting continuously moving webs |
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FR2595679B1 (fr) * | 1986-03-14 | 1988-05-13 | Atochem | Procede de fabrication conjointe de peroxyde d'hydrogene et d'isobutene |
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JP2002066563A (ja) | 2000-08-31 | 2002-03-05 | Tokyo Yogyo Co Ltd | 活性水素吸蔵浄水器 |
NZ532402A (en) * | 2001-10-31 | 2005-11-25 | Transcutaneous Tech Inc | Iontophoresis device |
US6652719B1 (en) * | 2002-06-03 | 2003-11-25 | Skydon Corp. | Electrolysis system |
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2004
- 2004-11-26 RU RU2006122945/15A patent/RU2385363C2/ru not_active IP Right Cessation
- 2004-11-26 KR KR1020067009723A patent/KR101218952B1/ko not_active IP Right Cessation
- 2004-11-26 EP EP04819229.8A patent/EP1704268B1/de active Active
- 2004-11-26 CA CA2547295A patent/CA2547295C/en not_active Expired - Fee Related
- 2004-11-26 US US10/581,009 patent/US8197666B2/en active Active
- 2004-11-26 WO PCT/EP2004/013452 patent/WO2005052214A2/de active Application Filing
- 2004-11-26 JP JP2006540400A patent/JP5094122B2/ja not_active Expired - Fee Related
- 2004-11-26 AU AU2004293566A patent/AU2004293566B2/en not_active Ceased
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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WO1990015659A1 (en) * | 1989-06-16 | 1990-12-27 | Olin Corporation | Process for removing ionizable impurities from non-aqueous fluids |
US5348683A (en) * | 1990-02-06 | 1994-09-20 | Olin Corporation | Chloric acid - alkali metal chlorate mixtures and chlorine dioxide generation |
US5401371A (en) * | 1992-07-16 | 1995-03-28 | Aisin Seiki Kabushiki Kaisha | Hydrogen generator |
EP0650929A1 (de) * | 1993-10-27 | 1995-05-03 | Halox Technologies Corporation | Elektrolytisches Verfahren und Vorrichting zur kontrollierten Oxydation oder Reduktion von Stoffen in wässriger Lösung |
JP2000265290A (ja) * | 1999-03-18 | 2000-09-26 | Matsushita Refrig Co Ltd | 水電解装置 |
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Title |
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PATENT ABSTRACTS OF JAPAN Bd. 008, Nr. 205 (C-243), 19. September 1984 (1984-09-19) & JP 59 092028 A (NIPPON PAINT KK), 28. Mai 1984 (1984-05-28) * |
PATENT ABSTRACTS OF JAPAN Bd. 2000, Nr. 12, 3. Januar 2001 (2001-01-03) & JP 2000 265290 A (MATSUSHITA REFRIG CO LTD), 26. September 2000 (2000-09-26) * |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2008510691A (ja) * | 2004-08-20 | 2008-04-10 | ベーリンガー インゲルハイム インターナショナル ゲゼルシャフト ミット ベシュレンクテル ハフツング | Plkインヒビターとしてのピリミジン化合物 |
WO2006128527A2 (de) * | 2005-05-30 | 2006-12-07 | Roiner, Maria | Vorrichtung zur durchführung eines verfahrens zur herstellung eines oder mehrerer gase |
WO2006128527A3 (de) * | 2005-05-30 | 2007-03-15 | Roiner Maria | Vorrichtung zur durchführung eines verfahrens zur herstellung eines oder mehrerer gase |
WO2011031763A1 (en) | 2009-09-11 | 2011-03-17 | Geo Firewall Sarl | Regulating a hydrocarbon combustion process using a set of data indicative of hydrocarbon fuel consumed corresponding to a monitored engine operating characteristic |
WO2011031797A1 (en) * | 2009-09-11 | 2011-03-17 | Geo Firewall Sàrl | System for regulating a hydrocarbon combustion process using a substantially stoichiometric mix of hydrogen and oxygen |
DE202012012463U1 (de) | 2012-11-12 | 2013-02-25 | Jakob Propp | Elektrolyseeinrichtung zur Erzeugung mindestens eines Reaktionsprodukts und einer Anlage zum Bereitstellen des erzeugten Reaktionsproduktes für einen Verbraucher |
Also Published As
Publication number | Publication date |
---|---|
AU2004293566A1 (en) | 2005-06-09 |
US20070108065A1 (en) | 2007-05-17 |
US8197666B2 (en) | 2012-06-12 |
RU2006122945A (ru) | 2008-01-10 |
EP1704268B1 (de) | 2018-05-02 |
AU2004293566B2 (en) | 2011-04-21 |
EP1704268A2 (de) | 2006-09-27 |
CA2547295A1 (en) | 2005-06-09 |
CA2547295C (en) | 2013-08-20 |
JP2007512435A (ja) | 2007-05-17 |
RU2385363C2 (ru) | 2010-03-27 |
KR20060114334A (ko) | 2006-11-06 |
KR101218952B1 (ko) | 2013-01-14 |
WO2005052214A3 (de) | 2005-09-15 |
JP5094122B2 (ja) | 2012-12-12 |
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