WO2004112138A1 - 半導体デバイスおよびその製造方法 - Google Patents
半導体デバイスおよびその製造方法 Download PDFInfo
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- WO2004112138A1 WO2004112138A1 PCT/JP2004/008450 JP2004008450W WO2004112138A1 WO 2004112138 A1 WO2004112138 A1 WO 2004112138A1 JP 2004008450 W JP2004008450 W JP 2004008450W WO 2004112138 A1 WO2004112138 A1 WO 2004112138A1
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- insulating film
- semiconductor device
- interlayer insulating
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Classifications
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- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L28/00—Passive two-terminal components without a potential-jump or surface barrier for integrated circuits; Details thereof; Multistep manufacturing processes therefor
- H01L28/10—Inductors
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/70—Manufacture or treatment of devices consisting of a plurality of solid state components formed in or on a common substrate or of parts thereof; Manufacture of integrated circuit devices or of parts thereof
- H01L21/77—Manufacture or treatment of devices consisting of a plurality of solid state components or integrated circuits formed in, or on, a common substrate
- H01L21/78—Manufacture or treatment of devices consisting of a plurality of solid state components or integrated circuits formed in, or on, a common substrate with subsequent division of the substrate into plural individual devices
- H01L21/82—Manufacture or treatment of devices consisting of a plurality of solid state components or integrated circuits formed in, or on, a common substrate with subsequent division of the substrate into plural individual devices to produce devices, e.g. integrated circuits, each consisting of a plurality of components
- H01L21/822—Manufacture or treatment of devices consisting of a plurality of solid state components or integrated circuits formed in, or on, a common substrate with subsequent division of the substrate into plural individual devices to produce devices, e.g. integrated circuits, each consisting of a plurality of components the substrate being a semiconductor, using silicon technology
- H01L21/8221—Three dimensional integrated circuits stacked in different levels
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L23/00—Details of semiconductor or other solid state devices
- H01L23/52—Arrangements for conducting electric current within the device in operation from one component to another, i.e. interconnections, e.g. wires, lead frames
- H01L23/522—Arrangements for conducting electric current within the device in operation from one component to another, i.e. interconnections, e.g. wires, lead frames including external interconnections consisting of a multilayer structure of conductive and insulating layers inseparably formed on the semiconductor body
- H01L23/5227—Inductive arrangements or effects of, or between, wiring layers
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L23/00—Details of semiconductor or other solid state devices
- H01L23/552—Protection against radiation, e.g. light or electromagnetic waves
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L27/00—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate
- H01L27/02—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier
- H01L27/04—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier the substrate being a semiconductor body
- H01L27/06—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier the substrate being a semiconductor body including a plurality of individual components in a non-repetitive configuration
- H01L27/0611—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier the substrate being a semiconductor body including a plurality of individual components in a non-repetitive configuration integrated circuits having a two-dimensional layout of components without a common active region
- H01L27/0617—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier the substrate being a semiconductor body including a plurality of individual components in a non-repetitive configuration integrated circuits having a two-dimensional layout of components without a common active region comprising components of the field-effect type
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L27/00—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate
- H01L27/02—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier
- H01L27/04—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier the substrate being a semiconductor body
- H01L27/06—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier the substrate being a semiconductor body including a plurality of individual components in a non-repetitive configuration
- H01L27/0688—Integrated circuits having a three-dimensional layout
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L27/00—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate
- H01L27/02—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier
- H01L27/04—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier the substrate being a semiconductor body
- H01L27/08—Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components specially adapted for rectifying, oscillating, amplifying or switching and having at least one potential-jump barrier or surface barrier; including integrated passive circuit elements with at least one potential-jump barrier or surface barrier the substrate being a semiconductor body including only semiconductor components of a single kind
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L29/00—Semiconductor devices adapted for rectifying, amplifying, oscillating or switching, or capacitors or resistors with at least one potential-jump barrier or surface barrier, e.g. PN junction depletion layer or carrier concentration layer; Details of semiconductor bodies or of electrodes thereof ; Multistep manufacturing processes therefor
- H01L29/02—Semiconductor bodies ; Multistep manufacturing processes therefor
- H01L29/06—Semiconductor bodies ; Multistep manufacturing processes therefor characterised by their shape; characterised by the shapes, relative sizes, or dispositions of the semiconductor regions ; characterised by the concentration or distribution of impurities within semiconductor regions
- H01L29/0657—Semiconductor bodies ; Multistep manufacturing processes therefor characterised by their shape; characterised by the shapes, relative sizes, or dispositions of the semiconductor regions ; characterised by the concentration or distribution of impurities within semiconductor regions characterised by the shape of the body
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L2924/00—Indexing scheme for arrangements or methods for connecting or disconnecting semiconductor or solid-state bodies as covered by H01L24/00
- H01L2924/0001—Technical content checked by a classifier
- H01L2924/00011—Not relevant to the scope of the group, the symbol of which is combined with the symbol of this group
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L2924/00—Indexing scheme for arrangements or methods for connecting or disconnecting semiconductor or solid-state bodies as covered by H01L24/00
- H01L2924/0001—Technical content checked by a classifier
- H01L2924/0002—Not covered by any one of groups H01L24/00, H01L24/00 and H01L2224/00
Definitions
- the present invention relates to a semiconductor device capable of performing high-frequency signal processing and a method for manufacturing the same, and more particularly, to a semiconductor device including at least a high-frequency signal processing circuit region on a semiconductor substrate and a method for manufacturing the same.
- CMOS gates including CMOS transistors were formed, and only signal processing by digital logic consisting of these CMOS gates was performed.
- the RF communication function is directed to analog signal processing.
- the function of amplifying received waves using passive elements such as inductors, pulse generators and pulse delay circuits It has a transmission function to use such as.
- the communication terminal device includes an LNA (Low noise amplifier) 61a, a transmission signal generation circuit 61b, and a switch circuit 61c in a silicon semiconductor chip to transmit and receive radio signals.
- BB digital baseband
- FIG. 27 shows a schematic top view of an inductor formed on a silicon semiconductor chip and an equivalent circuit thereof. Inductors use multilayer wiring formed on silicon semiconductor chips. Formed.
- ⁇ magnetic permeability of the inductor forming region
- ⁇ number of windings
- r maximum radius of the windings.
- Equation (1) focuses on the inductance (L) of the inductor.
- the inductor has a power loss factor and hinders the high frequency characteristics of the circuit.
- the resistance (Rs) of an inductor line formed from multilayer wiring causes a considerable power consumption because the line length increases when the inductor becomes large.
- the loss due to charge and discharge due to the coupling capacitance (Cp) between the inductor lines, the loss due to the coupling capacitance (Cox / 2) between the inductor and the silicon semiconductor substrate, and the loss due to the pn junction capacitance in the silicon substrate However, it also causes considerable power consumption.
- Factors other than the above loss include noise propagation and loss through the silicon substrate due to an induced current (eddy current) due to high-frequency magnetic field fluctuation from the inductor.
- This noise propagation phenomenon is a technical problem common to RF circuits on silicon semiconductor substrates as well as inductors.
- it is important to increase the substrate resistance (R1) and reduce the substrate capacitance (C1).
- the substrate resistance R1 is determined by the specific resistance p of the substrate and the thickness t of the substrate.
- a high-performance inductor is formed on a silicon semiconductor substrate.
- Technology is being developed.
- a technique has been proposed in which a groove (trench) is formed in a silicon substrate in an inductor formation region and the groove is filled with a silicon oxide film or the like (for example, Japanese Patent Application Laid-Open Nos. 2000-77610 and 2002-2002).
- 28 is a cross-sectional view of the on-chip inductor proposed in Japanese Patent Application Laid-Open No. 2000-77610, where grooves are formed in a lattice pattern on a silicon substrate 71 as shown in FIG.
- a silicon oxide film 72 is buried in the groove, and an inductor 73 is formed on the groove forming region.By burying the silicon oxide film 72 in the silicon substrate 71, the capacitance (C1) of the inductor forming region and the inductor By reducing the coupling capacitance (Cox / 2) between the line and the substrate, the leakage current of the inductor and the induced current can be reduced.
- Japanese Patent Application Laid-Open No. 2002-93622 discloses that a spiral trench is formed in a silicon substrate between and around spiral wires constituting an inductor, and the inside thereof is formed of an insulating material (silicon oxide). The element filled in ()) is described.
- Japanese Patent Application Laid-Open No. 2000-40789 discloses that an inductor is formed on a silicon substrate using multilayer wiring, and an insulator (silicon dioxide, silicon nitride) and intrinsic polysilicon are formed in an opening dug out from the silicon substrate surface.
- insulator silicon dioxide, silicon nitride
- a technique is described in which, by embedding, a plate-shaped insulating film and a shallow trench-shaped insulating film are formed in the inductor formation region from the surface of the silicon substrate as a starting point inside the substrate.
- a substrate is dug starting from the surface of a silicon substrate and the inside thereof is filled with an insulator.
- a technique has been proposed in which a ferromagnetic or soft magnetic material is embedded in an inductor formation region to increase the magnetic permeability around the winding and increase the inductance (eg, And JP-A-2001-284533. That is, as shown in FIG. 29, the winding of the inductor 83 is formed in the insulating film 82 on the silicon substrate 81, and the insulating film at the center (and the periphery) of the winding is formed.
- a magnetic core 84 made of a ferromagnetic metal such as an iron-cobalt alloy is disposed therein.
- Japanese Patent Application Laid-Open No. 2001-284533 discloses that a plurality of wiring layers are used, and a first wiring layer and a second wiring layer are electrically connected in parallel to reduce the resistance of the inductor wiring. Technology It is listed.
- both conventional techniques have been proposed for the purpose of improving the performance of an inductor formed on a silicon substrate, but have the following problems.
- the trench or trench is dug from the surface of the silicon substrate.
- a material having a relatively high relative dielectric constant such as silicon oxide / silicon nitride is assumed. It is effective to embed a low dielectric constant insulating film to reduce stray capacitance, but in the prior art, a transistor formation process is planned after filling the insulating film. The insulation film cannot be buried.
- the low dielectric constant insulating film for example, an organic siloxane film in which oxygen in a silicon oxide film is partially substituted by an organic group such as a methyl group, or a porous material in which minute pores of 5 nm or less are dispersed in the organic siloxane film.
- the heat resistance of low dielectric constant insulating films is generally about 500 ° C or less.
- forming a transistor requires a high heat treatment process at 700 ° C or higher, such as formation of a gate insulating film and activation annealing after impurity injection, so bury the insulating film in the inductor formation region before forming the transistor.
- the buried insulating film is necessarily limited to a silicon oxide film having high heat resistance. Therefore, in the first prior art, the parasitic capacitance of the substrate could not be sufficiently reduced.
- one of the objects is to reduce the substrate current, but the relationship between the trench depth and the silicon substrate thickness, that is, how much the trench depth is dug into the silicon substrate thickness No consideration is given to this point. Since the silicon substrate is doped with an impurity and has low resistance, the substrate current cannot be sufficiently reduced when the substrate thickness is large. That is, noise and loss cannot be sufficiently reduced.
- an opening having a large area with respect to the depth is provided, and the opening is filled with a ferromagnetic material.
- the cross-sectional area diameter is larger than the buried depth of the buried ferromagnetic material, the loss due to the eddy current due to the fluctuation of the magnetic field passing through the ferromagnetic region increases.
- the cross-sectional area must be reduced.
- simply reducing the cross-sectional area reduces the area covered by the magnetic core region, and cannot improve the magnetic flux density.
- JP-A-2001-284533 also describes an embodiment in which the magnetic core is formed by solidifying soft magnetic particles with polyimide, but does not pay any attention to the reduction of Cp. Only an organic adhesive (polyimide) with a relative dielectric constant of 3 or more is used to fix the magnetic material.
- Japanese Patent Application Laid-Open No. 2001-284533 states that the resistance loss of the inductor wiring can be reduced by electrically connecting two wiring layers in parallel, but the lower wiring layer is connected to the inductor layer. There is a problem that the use of the wiring increases the parasitic capacitance. In other words, by using the lower wiring layer closer to the substrate, the distance from the substrate becomes shorter, and the parasitic capacitance Cox between the wiring and the substrate in the equivalent circuit shown in FIG. There is a problem that the performance of the device is deteriorated.
- An object of the present invention is to solve the above-mentioned problems of the related art, and to provide a semiconductor device including at least a high-frequency signal processing circuit region on a semiconductor substrate, thereby enabling loss and noise reduction in a high-frequency band. And, in particular, to provide a semiconductor device capable of reducing the size and loss of an inductor, which is a passive element.
- a semiconductor substrate having a low-capacity substrate region, a transistor formed in a surface region of the semiconductor substrate, and a And a multi-layer wiring structure having a plurality of interlayer insulating films and a plurality of wiring layers provided in the low-capacity substrate region, wherein at least the lowermost interlayer insulating film passes through the inside of the semiconductor substrate.
- a semiconductor device having a plurality of substrate openings formed therein.
- a low dielectric constant insulator is provided in the substrate opening. More preferably, the length of the substrate opening is at least half the thickness of the semiconductor substrate, or the substrate opening penetrates the semiconductor substrate.
- the present invention provides, in a second aspect thereof, a semiconductor substrate, A transistor formed in a surface region of the semiconductor substrate; and a multilayer wiring structure provided on the transistor and having a plurality of interlayer insulating films and a plurality of wiring layers, wherein a high magnetic permeability is provided in the interlayer insulating film.
- the high magnetic permeability region has an aspect ratio (depth Z diameter or length of one side) penetrating at least one interlayer insulating film and reaching another interlayer insulating film.
- a semiconductor device characterized in that one or more openings have a plurality of high-permeability magnetic rods formed by being filled with a high-permeability material having conductivity.
- the oxide-based high permeability region penetrates at least one interlayer insulating film to reach another interlayer insulating film.
- a semiconductor device characterized by having a plurality of insulating high-permeability magnetic rods formed by filling an opening to be reached with an insulating high-permeability material.
- the high-permeability material having insulating properties is a composite material including a low-permittivity insulating material and a high-permeability material having conductivity or a high-permeability material having insulating properties.
- the high magnetic permeability material having an insulating property is, for example, an oxide-based high magnetic permeability material.
- the conductive high magnetic permeability material include a NiFe binary alloy and a multi-component alloy obtained by adding elements such as Mo, Cr, Cu, and Co, that is, a material generally called a permalloy material.
- Fe-Co alloys Ni-Co alloys, Fe-Al alloys, or Fe-A-Si alloys called Sendust, and those with a small amount of other elements added to them, and also amorphous FeP-based alloys, FeB-based alloys, and other elements added to them, and those using SiB as an amorphizing element include FeSiB, NiSiB, CoSiB, CoFeSiB, CoFeNiSiB, CoFeMoSiB, CoFeMNbSiB, and CoFeMnSiB.
- Co- (Zr, Hf, Nb, Ta, Ti), or metal-metal alloys with several percents of Fe, Mn, and Ni added as amorphous materials for Co-based sputtered thin films For example, CoFePbAl, CoMnB, CoMoZr, CoTaZr, CoNbZr, CoNbTi, CoFeNb, CoMnNb, etc.
- a granular film-like substance such as FeTaN or FeTaC may be used.
- Oxide-based high permeability materials include, for example, the chemical formula MFe 0 (M is, for example, Mn 2+ , Ni 2+ , Cu
- a bivalent metal ion such as 2+ a material which is generally called ferrite, or a mixture of the ferrite material and a non-magnetic oxide such as ZnFeO.
- ferrite examples include Mn-Zn ferrite, Mg-Fe ferrite, Cu- ⁇ ⁇ ferrite, Cu-Zn-Mg ferrite, and M-Cu-Zn ferrite. Furthermore, trace amounts of Mn-Mg ferrite, Mn-Mg-Al ferrite, Ni ferrite, M_Zn ferrite, YIG (YFeO), or YIG that can be used at relatively high frequencies such as the MHz band to GHz band
- Garnet-type ferrites such as A1-based YIG, Gd-based YIG, Ca-based YIG, and Nb YIG to which elements are added, hexagonal-type Ba ferrite, and substances obtained by adding a small amount of other elements to Ba-ferrite, and Ni- Co ferrite, M_Cu_Co_Fe ferrite and the like are also preferable examples.
- These examples of the high-permeability material are examples for implementing the present invention in a preferred embodiment, and the present invention is not limited by the above-described example of the high-permeability material. In the listed substances, their composition ratios and the like are not taken into consideration, and the present invention is not limited by these.
- a semiconductor substrate having a low-capacity substrate region, a transistor formed in a surface region of the semiconductor substrate, and a And a multi-layer wiring structure having a plurality of interlayer insulating films and a plurality of wiring layers, wherein the low-capacity substrate region penetrates at least the lowermost interlayer insulating film to reach the inside of the semiconductor substrate.
- a semiconductor device is provided, wherein a plurality of substrate openings are formed, and a wiring layer covering at least two or more layers is formed on the low-capacity substrate region.
- a semiconductor substrate a transistor formed in a surface region of the semiconductor substrate, and a plurality of interlayers provided on the transistor.
- a multilayer wiring structure having an insulating film and a plurality of wiring layers, wherein a high magnetic permeability region is provided in the interlayer insulating film;
- a low-dielectric-constant insulating rod having a low-dielectric-constant film is arranged in a semiconductor substrate below an inductor formation region, and the substrate thickness is further reduced.
- the RF circuit including the inductor can be reduced in size and reduced in loss, and a semiconductor chip incorporating a digital signal processing function and a high-performance RF circuit can be realized.
- the semiconductor substrate is not particularly limited. However, for a silicon semiconductor substrate on which a CMOS device is formed, a region in which a low-dielectric-constant insulating film rod is buried is formed so that a low-resistance material is essentially formed. A low RF noise propagation region with high resistance and low dielectric constant can be formed in any part of the silicon substrate.
- the multilayer wiring structure includes a wiring structure having two or more wiring layers.
- FIG. 1 is a cross-sectional view illustrating a semiconductor device according to a first embodiment of the present invention.
- FIG. 2 is a sectional view showing a semiconductor device according to a second embodiment of the present invention.
- FIG. 3 is a plan view showing a first example of an arrangement state of openings in which a low dielectric constant material is buried.
- FIG. 4 is a plan view showing a second example of an arrangement state of openings in which a low dielectric constant material is buried.
- FIG. 5 is a sectional view showing a semiconductor device according to a third embodiment of the present invention.
- FIG. 6 is a sectional view showing a semiconductor device according to a fourth embodiment of the present invention.
- FIG. 7 is a block diagram illustrating a use state of an apparatus equipped with a plurality of semiconductor devices according to the present invention.
- FIG. 8 is a plan view and a cross-sectional view of the semiconductor device according to the first embodiment of the present invention.
- FIG. 9 is a plan view and a cross-sectional view for explaining one process step of the method for manufacturing a semiconductor device according to the first embodiment of the present invention.
- FIG. 10 is a plan view and a cross-sectional view for explaining one process step of the method for manufacturing a semiconductor device according to the first embodiment of the present invention.
- FIG. 11 is a plan view and a cross-sectional view for explaining one process step of the method for manufacturing a semiconductor device according to the first embodiment of the present invention.
- FIG. 12 is a plan view and a cross-sectional view for explaining one process step of the method for manufacturing a semiconductor device according to the first embodiment of the present invention.
- FIG. 13 is a plan view and a cross-sectional view for explaining one process step of the method for manufacturing a semiconductor device according to the first embodiment of the present invention.
- FIG. 14 is a plan view and a cross-sectional view for explaining one process step of the method for manufacturing a semiconductor device according to the first embodiment of the present invention.
- FIG. 15 is a plan view and a cross-sectional view for explaining one process step of the method for manufacturing a semiconductor device according to the first embodiment of the present invention.
- FIG. 16 is a plan view and a cross-sectional view for explaining one process step of the method for manufacturing a semiconductor device according to the first embodiment of the present invention.
- FIG. 17 is a plan view and a cross-sectional view for explaining one process step of the method for manufacturing a semiconductor device according to the first embodiment of the present invention.
- FIG. 18 is a plan view and a cross-sectional view for explaining one process step of the method for manufacturing a semiconductor device according to the first embodiment of the present invention.
- FIG. 19 is a plan view and a sectional view of a semiconductor device according to a second embodiment of the present invention.
- FIG. 20 is a sectional view of a semiconductor device according to a third embodiment of the present invention.
- FIG. 21 is a sectional view of a semiconductor device according to a fourth embodiment of the present invention.
- FIG. 22 is a sectional view of a semiconductor device according to a fifth embodiment of the present invention.
- FIG. 23 is a sectional view of a semiconductor device according to a sixth embodiment of the present invention.
- FIG. 24 is a sectional view of a semiconductor device according to a seventh embodiment of the present invention.
- FIG. 25 is a sectional view of a semiconductor device according to an eighth embodiment of the present invention.
- FIG. 27 is a plan view of an inductor formed on a semiconductor substrate and an equivalent circuit diagram thereof.
- FIG. 28 is a cross-sectional view of a first conventional technique 1 ;
- FIG. 30 is a cross-sectional view showing a fifth embodiment of the present invention.
- FIG. 31 is a top view showing that a plurality of wiring layers are electrically connected in parallel via vias.
- FIG. 32 is a cross-sectional view showing a sixth embodiment of the present invention.
- FIG. 33 is a top view showing that ends of a plurality of wiring layers are electrically connected in series via vias.
- FIG. 34 is a top view showing that ends of a plurality of wiring layers are electrically connected in series via vias.
- FIG. 35 is a top view and a cross-sectional view showing that ends of a plurality of wiring layers are electrically connected in series via vias.
- FIG. 36 is a top view and a cross-sectional view showing that ends of a plurality of wiring layers are electrically connected in series via vias.
- FIG. 37 is a top view and a cross-sectional view showing that ends of a plurality of wiring layers are electrically connected in series via vias.
- FIG. 38 is a top view and a cross-sectional view showing that ends of a plurality of wiring layers are electrically connected in series via vias.
- FIG. 39 is a cross-sectional view showing a seventh embodiment of the present invention.
- FIG. 40 is a cross-sectional view showing an eighth embodiment of the present invention.
- FIG. 41 is a sectional view showing a ninth embodiment of the present invention.
- FIG. 42 is a process cross-sectional view for manufacturing the seventh embodiment of the present invention.
- FIG. 43 is a process cross-sectional view for manufacturing the seventh embodiment of the present invention.
- FIG. 44 is a process sectional view for manufacturing the seventh embodiment of the present invention.
- FIG. 45 is a process cross-sectional view for manufacturing the seventh embodiment of the present invention.
- FIG. 46 is a process sectional view for manufacturing the eighth embodiment of the present invention.
- FIG. 47 is a process cross-sectional view for manufacturing the eighth embodiment of the present invention.
- FIG. 48 is a process sectional view for manufacturing the eighth embodiment of the present invention.
- FIG. 49 is a process cross-sectional view for manufacturing the ninth embodiment of the present invention.
- FIG. 50 is a process sectional view for manufacturing the ninth embodiment of the present invention.
- FIG. 51 is a process cross-sectional view for manufacturing the ninth embodiment of the present invention.
- FIG. 52 is a plan view showing a third example of an arrangement state of openings in which a low dielectric constant material is buried.
- FIG. 53 is an explanatory diagram for explaining the dependence of the Q value of the inductor on the burying depth of the low dielectric constant filling member in the first embodiment of the present invention.
- FIG. 54 is an explanatory diagram for explaining the dependence of the Q value of the inductor on the burying depth of the low dielectric constant filling member in the first embodiment of the present invention.
- the semiconductor chip according to the first embodiment of the present invention has an RF circuit area 100 for processing a high-frequency analog signal and a digital circuit area 200 for processing a digital signal.
- a laminated insulating structure 52 including a plurality of interlayer insulating films is formed on a semiconductor substrate 51.
- an inductor 53 having a spiral structure is provided using multilayer wiring.
- the RF circuit region 100 is provided with an opening penetrating at least one interlayer insulating film and reaching the inside of the semiconductor substrate 51. Inside the opening, a low dielectric constant having a relative dielectric constant lower than that of the silicon oxide film is provided.
- the rate filling member 54 is embedded.
- the opening may be a circle or a polygon such as a square when viewed in a direction perpendicular to the substrate.
- a so-called honeycomb (honeycomb) structure in which hexagonal openings are arranged so as to increase the filling ratio is also good.
- the shape of the hexagon at this time is not limited to a regular hexagon, but may be a shape as shown in FIG. 52, that is, a hexagon in which a pair of opposed corners are each 90 degrees. good.
- the hexagonal shape shown in Figure 52 is a limitation in the design of currently used semiconductor devices, that is, the allowable lines in the design are 0, 45, and 90 degrees with respect to a certain reference plane. Is limited.
- the shape of the opening actually formed is affected by manufacturing variations such as exposure and etching.
- the angle formed by the shape of the opening actually formed is not always exactly 90 degrees, but is, for example, about 80 to 100 degrees.
- the structure in which the hexagonal openings are arranged in a honeycomb shape is preferable because the filling rate of the openings with respect to the plane of the substrate can be increased and the mechanical strength of the substrate can be maintained.
- the opening may be a groove-shaped opening. In the case of a groove-shaped opening, the groove may be formed so as to intersect.
- the low dielectric constant filling member 54 carried in the opening is an organic siloxane (MSQ) film in which oxygen in silicon oxide is partially substituted by an organic group such as a methyl group, or 5 ⁇ or less in the organic siloxane film. , Formed of a porous insulating film or the like in which minute holes are dispersed.
- the desired dielectric constant of the low dielectric constant filling member 54 is 3 or less.
- the depth of the low-dielectric-constant member 54 embedded in the semiconductor substrate 51 is 2 / im or more. And more preferably 5 ⁇ 5 ⁇ or more.
- FIG. 53 shows that, from the surface of the semiconductor substrate 51, the filling depth of the low dielectric constant filling member 54 is (a) 2.5 ⁇ , (b) 5 im, (c) 10 ⁇ m, and ( ⁇ ) 20 A schematic diagram with ⁇ ⁇ , is shown.
- FIG. 53 (a) shows a laminated insulating film 52 and an inductor 53.
- the laminated insulating film 52 and the inductor 53 are also formed in FIGS. 53 (b), (c) and (d) in the same manner as in FIG. 53 (a), and are not particularly shown.
- the height of the low dielectric constant filling member 54 from the substrate surface in the upward direction in the drawing, the position of the uppermost surface inside the laminated insulating film, and the like are described in the seventh, eighth, and ninth embodiments of the present invention. Since it is described in detail in the form, it is not particularly described in FIG. That is, in the explanatory diagram of FIG. 53, the depth of the low dielectric constant filling member 54 embedded in the substrate depth direction is to be described.
- Figure 53 (e) shows the frequency dependence of the Q value of the on-chip inductor 53 placed in the uppermost wiring layer for each of the above structures (a), (b), (c), and (d). is there.
- the Q value is improved in each of the structures (a), (b), (c), and (d).
- the semiconductor substrate 51 is disclosed, for example, in the Proceedings of IEEE Radio and Wireless Conference, 1998, RAWCON 98 p.
- the low dielectric constant member 54 extends from the surface of the semiconductor substrate to an intermediate depth of the low-resistance epitaxial layer. . Furthermore, it is more preferable that the lowermost layer of the low-resistance epitaxy layer is reached. More preferably, the lower end of the low dielectric member 54 preferably penetrates the low-resistance epitaxy layer and reaches the lowermost support substrate. Referring to FIG.
- a low dielectric constant is applied to a semiconductor substrate 107 including a plurality of layers having different resistivities, each of which includes a high-resistance epitaxial layer 104, a low-resistance epitaxial layer 105, and a high-resistance support substrate 106.
- Schematic diagrams are shown in which the filling depth of the filling member 54 is (a) 2.5 xm, (b) 5 zm, (c) 10 xm, and (d) 20 zm, respectively, from the semiconductor substrate surface.
- FIG. 54 (a) shows the laminated insulating film 52 and the inductor 53. The laminated insulating film 52 and the inductor 53 are also formed in the same manner as in FIG.
- the height of the low dielectric constant filling member 54 from the substrate surface in the upward direction in the drawing, the position of the uppermost surface inside the laminated insulating film, and the like are determined according to the seventh, eighth, and ninth embodiments of the present invention. Since it is described in detail in FIG. 54, it is not particularly described in FIG. That is, in the explanatory diagram of FIG. 54, the embedding depth of the low dielectric constant filling member 54 in the substrate depth direction is to be described. Fig.
- the low dielectric constant filling member when the filling depth of the low dielectric constant filling member is set to 10 ⁇ , the low dielectric constant filling member has a structure penetrating the low resistance epitaxy layer, and thus occurs in the low resistance epitaxy layer. It is considered that the eddy current can be further reduced. Therefore, a semiconductor substrate composed of a plurality of layers having different resistivity is used as the semiconductor substrate. In this case, it is more preferable that the buried depth of the low dielectric constant filling member 54 is deeper than the depth penetrating the low-resistance epitaxy layer.
- the substrate capacity can be reduced according to the present invention. Since the resistance can be effectively increased and the distance between the semiconductor substrate and the metal wiring, which is a main path of the eddy current generated in the semiconductor substrate, can be physically increased, the invention of the present application can be realized. The desired effect can be obtained.
- the low-dielectric-constant filling member 54 may be embedded particularly along the peripheral portion of the semiconductor chip, and the on-chip antenna wiring may be formed thereon.
- the on-chip antenna wiring is formed, for example, in the shape of a letter, a letter “1”, a letter “U”, or a multiple loop.
- the semiconductor substrate has the bottom surface of the opening for accommodating the low dielectric constant filling member 54 exposed.
- the semiconductor device is the same as the semiconductor device according to the first embodiment, except that the semiconductor device is polished to the extent that the semiconductor device is polished. In the present embodiment, the resistance of the semiconductor substrate is further increased.
- the planar arrangement of the low dielectric constant filling member 54 is a square lattice point arrangement and a diagonal arrangement [Fig.
- the low dielectric constant filling members 54 may be arranged at random, the probability that a linear current path is formed in a planar view in the RF circuit area can be reduced, and the substrate resistance R1 can be effectively increased. it can.
- the low-permittivity filling members 54 may be arranged regularly to prevent the formation of a linear current path over the entire width or the entire length in the RF circuit region.
- the hexagonal openings are arranged to increase the filling rate, so that it can be used as a so-called honeycomb structure.
- the low-permittivity filling member 54 is buried in the grooves formed in a lattice shape, thereby forming the RF circuit area. It is also possible to completely suppress the formation of a current path in the region. However, such a structure that divides the substrate weakens the mechanical strength of the substrate.
- a high magnetic permeability region 300 is provided on RF circuit region 100.
- the high-permeability region 300 in the laminated insulating structure 52 having a plurality of interlayer insulating films, one interlayer insulating film penetrates the center of the winding of the inductor 53 and the periphery thereof through another interlayer insulating film. Is formed, and a high-permeability member 55 is formed by filling the opening with a high-permeability magnetic material.
- the loaded high magnetic permeability magnetic material is in the form of a conductive Balta
- the opening has an aspect ratio (depth / diameter or length of one side) to reduce induced current. Is set to the condition that is 1 or more.
- the high magnetic permeability magnetic material to be carried is an insulating material, or when the soft magnetic material particles are mixed with an insulating material (preferably a low dielectric constant insulating material) as described below, No special conditions are required.
- the opening may be filled with a low-permittivity insulating material together with a high-permeability magnetic material.
- the high magnetic permeability member 55 is assumed to be a material in which a high magnetic permeability magnetic material fine powder is dispersed in a low dielectric constant insulating material and is carried in the opening.
- Desirable insulating materials include the above-mentioned organic siloxane film and a porous insulating film in which micropores are dispersed in the organic siloxane film.
- the high-permeability member 55 may be formed by a method of embedding a low-permittivity insulating material in which fine particles of a high-permeability magnetic material are dispersed in the opening. Alternatively, it may be covered with a high-permeability material film and the remaining space in the opening may be filled with a low-permittivity material.
- the high magnetic permeability member 55 When the high magnetic permeability member 55 is made of a conductive barrier material, an opening having a large diameter is formed in a region where the high magnetic permeability member 55 is formed, and the inside of the opening is filled with a low dielectric constant insulating material. May be included. In this case, an opening for filling a high magnetic permeability material may be formed in the low dielectric constant insulating material layer, and a soft magnetic material may be embedded in this opening by a sputtering method or an electrolytic plating method.
- the high permeability member 55 should be provided in an area other than the inductor formation area. You can. In this case, the high magnetic permeability member 55 functions as a magnetic shield.
- a high permeability member 55 is used in addition to the rod member 55a of the high permeability member 55 perpendicular to the substrate surface.
- the third embodiment is the same as the third embodiment except that a plain member 55b that covers the member 55a and connects the rod member 55a is provided.
- the provision of the plain member 55b on the high magnetic permeability member 55 increases the magnetic permeability around the winding of the inductor 53, thereby enabling a further increase in inductance or a further miniaturization of the inductor 53, and other wiring. This can reduce the induced current.
- the plain member 55b of the high magnetic permeability member 55 may be provided below the force rod member 55a provided above the rod member 55a.
- a plane member may be provided on both the upper and lower parts of the rod member 55a.
- the semiconductor device having the first to fourth embodiments it is possible to reduce the size and performance of the inductor, and to reduce the size and performance of passive elements and CMOS circuits. Active elements can be mixed on one chip. Therefore, in the semiconductor device according to the present invention, it is possible to realize a mixed chip of an RF circuit and a digital circuit (including a memory unit such as an SRAM) in which loss and noise propagation are suppressed.
- a plurality of such chips 60 are prepared, and signal transmission between these chips can be performed wirelessly.
- printed wiring boards can be specialized for low-noise power supply, and the number of design steps can be significantly reduced.
- restrictions on chip placement are greatly relaxed.
- FIG. 30 is a structural diagram showing a fifth embodiment of the present invention.
- Fifth embodiment of the present invention According to the embodiment, at least two or more wiring layers 85 are formed on the low-capacity substrate, a plurality of via plugs 86 are formed over the entire area of the wiring layers, and the plurality of wiring layers are electrically connected. Are formed in parallel with each other.
- Reference numeral 19 denotes a high permeability separation region formed in a region including the magnetic core of the inductor and its periphery.
- FIG. 31 shows a top view and a cross section of the inductor wiring portion.
- the via plugs 86a and 86b interconnecting the multiple wiring layers 87-89 are shown.
- a well-known circular or octagonal shape may be used as the shape of the force inductor 85 described using a spiral shape as the planar shape of the inductor 85.
- the number of via plugs is limited in shape, size, system IJ, or the number that can be arranged, etc. due to the semiconductor device formation process or design constraints.
- FIG. 32 is a structural diagram showing a sixth embodiment of the present invention.
- at least two or more wiring layers are electrically connected in series by the plurality of vias 86 on the low-capacity substrate.
- An inductor 91 is formed.
- FIG. 33 shows a top view of the inductor wiring portion. In the illustration of Figure 33, the inductor 91
- the force S described using the spiral type as the plane shape of the inductor may be used, and a known circular or octagonal shape may be used as the inductor shape.
- Connecting a plurality of wiring layers 87 and 88 in series corresponds to increasing the wiring length of the inductor wiring, which is compared with a case where an inductor is formed using only one wiring layer.
- An inductor element having the same value of inductance can be formed with a smaller occupied area.
- the distance between the wiring layer and the substrate becomes shorter and the capacitance between the wiring layer and the substrate increases as compared with the case where only the uppermost wiring layer is used.
- the effect of the increase in capacitance can be suppressed. Therefore, it is possible to obtain an inductor element in which the area occupied in the chip is reduced and an increase in capacitance is suppressed.
- the parasitic capacitance corresponds to the inter-wire capacitance Cp shown in the equivalent circuit of FIG.
- the wiring width of the upper and lower wiring layers 87 and 88 is made different, so that the parasitic capacitance generated between the wirings can be reduced.
- wirings which are in an upper and lower positional relationship with each other are connected to each other in order to prevent a negative mutual inductance from being generated therebetween. It is more preferable than the force S to be arranged so that the directions are not opposed to each other.
- FIG. 33 to FIG. 38 show examples of the arrangement of the multilayer wiring to achieve such an object.
- the number of via plugs 86 is limited by the shape, size, arrangement, or number of via plugs 86 that can be formed due to semiconductor device formation processes or design constraints. In order to reduce the resistance value of the connection part by the via plug, it is preferable to interconnect the wiring layers with as many via plugs as the design allows. Although the number of via plugs shown in the explanatory diagrams 33 to 38 is clearly smaller than the number of vias allowed by the process of forming a commonly used semiconductor device and the design constraints, this is the principle of the present invention. The present invention is not limited at all by the layout 1J, shape, and number of vias in the explanatory diagrams 33 to 38.
- a seventh embodiment of the present invention shown in FIG. 39 is a semiconductor substrate including a low-capacity substrate region. It is applied to semiconductor devices in which metal wiring mainly composed of copper is formed on a board by the damascene method.
- a first stopper insulating film 92 and a second stopper insulating film containing at least silicon on the first interlayer insulating film 4 and containing at least one or more different elements compared to the first interlayer insulating film 4 93 are formed.
- the bottom surface of the first metal wiring 10 formed in the second interlayer insulating film 9, the first stopper insulating film 92, and the second stopper insulating film 93 located above the low-capacitance substrate region is flat. is there.
- the effect can be obtained when copper and an alloy containing copper as a main component are used as a main forming material of the multilayer wiring. Copper and a wiring structure containing copper as a main component are mainly formed by a method called a damascene method.
- the damascene method is used as a method of forming a multilayer wiring. In this case, the effects of the present embodiment can be obtained. Note that the present embodiment is different from the above-described embodiments up to the sixth in that only the structure of a portion of a low-capacity substrate region formed in a semiconductor substrate is different. I do.
- a wiring material mainly composed of copper and a method of forming the same it is assumed that a material and a process which are currently mainstream are used, but in this embodiment, a wiring mainly composed of copper is used. Since the material, structure, and manufacturing process do not affect the present invention, details of a method of forming a wiring containing copper as a main component will not be particularly described.
- the seventh embodiment of the present invention will be described in detail with reference to the drawings.
- a first stopper insulating film 92 containing at least silicon and containing at least one or more different elements compared to the first interlayer insulating film 4 is formed on the first interlayer insulating film 4.
- a second stopper insulating film 93 is formed.
- the stopper insulating film contains at least silicon and is sufficient when performing CMP of the low dielectric constant film 7 which is a constituent material of the low dielectric constant insulator rod 8 and when performing plasma etching of the second interlayer insulating film 9. It is preferable that the material be able to secure a high selectivity.
- the second interlayer insulating film 9 SiO, a material in which SiO is doped with an element such as boron or phosphorus, or a material in which part of oxygen in a silicon oxide film is replaced with hydrogen or a methyl group, If a material having a lower dielectric constant than the silicon oxide film, such as carbon-added silica (SiC) or SiOCH, is used, at least silicon and nitrogen should be used as the stopper insulating films 92 and 93. As an example where the contained material is more preferred Examples include SiN, SiON, and SiCN.
- the low dielectric constant insulating film 7 a silicon oxide film in which a part of oxygen of a silicon oxide film is replaced with hydrogen or a methyl group, or a silicon oxide film such as carbonized silica (SiOC) or SiOCH is used.
- a material having a very low relative dielectric constant is used, a material containing at least silicon and nitrogen is more preferable as the stove insulating films 92 and 93, such as SiN, SiON, or SiCN.
- the stopper insulating films 92 and 93 may have the same constituent elements and the same ratio, that is, the same insulating film material.
- the first stopper insulating film 92 and the second stopper The interface with the insulating film 93 may not be clearly observed even by using a scanning electron microscope or a transmission electron microscope.
- the first metal wiring 10 formed in the first Stoba insulating film 92, the second Stoba insulating film 93, and the second interlayer insulating film 9 located above the low-capacitance substrate region is formed.
- the bottom surface is flat, and the uppermost surfaces of the low dielectric constant insulator rod located immediately below the metal wiring layer 10 and the low dielectric constant rod not located immediately below the metal wiring layer 10 are mutually separated. Not located on the same plane.
- the seventh embodiment can be applied simultaneously to the case where copper and an alloy mainly containing copper are used as the multilayer wiring material in the first to sixth embodiments of the present invention. is there.
- the eighth embodiment of the present invention is applied to a semiconductor device in which a metal wiring containing copper as a main component is formed on a semiconductor substrate including the low-capacity substrate region by a damascene method.
- First stopper insulating film 92 and second stopper insulating film 93 containing at least silicon on first interlayer insulating film 4 and containing at least one or more different elements compared to first interlayer insulating film 4 Is formed, and the bottom surface of the first metal wiring 10 formed in the second interlayer insulating film 9, the first stopper insulating film 92, and the second stopper insulating film 93 located above the low-capacity substrate region is formed.
- a cap insulating film 94 having a higher relative dielectric constant and mechanical strength than the low-dielectric-constant film rod 8 has a low dielectric constant. It is formed on the upper end of the insulator rod.
- the present embodiment when copper and an alloy containing copper as a main component are used as the main forming material of the multilayer wiring, the effect can be obtained. Copper and a wiring structure containing copper as a main component are mainly formed by a method called a damascene method. According to the embodiment, when the damascene method is used as a method of forming a multilayer wiring, the effects of the present embodiment can be obtained. Note that the present embodiment is different from the above-described embodiments up to the sixth in that only the structure of a portion of a low-capacity substrate region formed in a semiconductor substrate is different. I do.
- FIG. 40 is a structural diagram showing the eighth embodiment of the present invention.
- first stopper insulating film 92 containing at least silicon on first interlayer insulating film 4 and containing at least one or more different elements compared to first interlayer insulating film 4
- a second stopper insulating film 93 is formed.
- the stopper insulating film contains at least silicon and has a sufficient selectivity when performing plasma etching of the low dielectric constant film 7 and the second interlayer insulating film 9 which are constituent materials of the low dielectric constant insulator rod 8. It is preferable that the material can be secured.
- the second interlayer insulating film 9 SiO, a material in which SiO is doped with an element such as boron or phosphorus, a material in which part of oxygen in a silicon oxide film is replaced with hydrogen or a methyl group
- the stopper insulating films 92 and 93 are made of a material containing at least silicon and nitrogen. Examples of more preferred are SiN, SiON, and SiCN.
- the low dielectric constant insulating film 7 a silicon oxide film in which part of oxygen is replaced with hydrogen or a methyl group, a carbon-doped silica (Si ⁇ C),
- the top insulating films 92 and 93 When a material having a lower dielectric constant than the silicon oxide film, such as Si ⁇ CH, is used, a material containing at least silicon and nitrogen is more preferable for the top insulating films 92 and 93. Is SiN, SiON, or SiCN. If the stopper insulating films 92 and 93 have the same constituent element and the same ratio, that is, even if the same insulating film material is acceptable, the first stopper insulating film 92 and the second stopper insulating film shown in FIG. 40 can be used. The interface with 93 may not be clearly observed even when using a scanning electron microscope or a transmission electron microscope.
- a cap insulating material having a higher dielectric constant and mechanical strength than the low dielectric constant film rod 8 is provided above the opening of the low dielectric constant film rod 8 located in the low capacitance substrate region.
- a film 94 is formed on the upper end of the low dielectric constant insulator rod.
- the bottom surface of the first metal wiring 10 formed in the first Stoba insulating film 92, the second Stoba insulating film 93, and the second interlayer insulating film 9 located above the low-capacitance substrate region Are flat, and the uppermost surface of a cap insulating film formed on the low dielectric constant insulator rod located immediately below the metal wiring layer 10 and located immediately below the metal wiring layer 10.
- the uppermost surface of the cap insulating film above the low dielectric constant rod that is not located is not coplanar with each other.
- the eighth embodiment can be applied simultaneously to the case where copper and an alloy containing copper as a main component are used as the multilayer wiring material in the first to sixth embodiments of the present invention. It is.
- the main forming material of the multilayer wiring aluminum currently used in the mainstream, or aluminum containing a small amount of silicon or a small amount of copper is used.
- the effects of the present invention can be obtained.
- the present embodiment is different from the above-described sixth to sixth embodiments in that only the structure of the low-capacity substrate region formed in the semiconductor substrate and the main wiring material are different. Only the excerpt is explained.
- the aluminum wiring material and the method of forming the same the current mainstream material and the force that assumes the process are used.
- the material, structure and manufacturing process of the aluminum wiring are No details are given, as it has no effect.
- FIGS. 41 (a) and 41 (b) are structural views showing a ninth embodiment of the present invention.
- the present embodiment is characterized in that the uppermost surface of the low dielectric constant insulator rod 8 is located at a position lower than the uppermost surface of the W contact plug 5, and the low capacitance substrate region is formed.
- a cap insulating film 94 having a higher relative dielectric constant and a higher mechanical strength than the low dielectric constant insulator rod 8 is formed at the upper part of the opening of the low dielectric constant insulator rod 8 to be formed. ing.
- a metal compound containing titanium or the like and at least a After a main wiring material containing aluminum is deposited by a sputtering method or the like, patterning is performed with a photoresist, and a desired wiring shape is formed by plasma etching.
- a desired wiring shape is formed by plasma etching.
- metal is sputtered on the surface where the upper part of the low dielectric constant rod 8 is exposed or exposed to the etching plasma, the sputtered metal diffuses into the low dielectric constant rod or becomes low due to the etching plasma. Degradation may occur, such as an increase in the relative dielectric constant of the low dielectric constant material due to the dissociation of some elements of the low dielectric constant material forming the dielectric constant rod.
- the cap insulating film 94 protects the upper surface of the low dielectric constant rod 8 from sputtering or etching plasma, so that deterioration of the low dielectric constant material can be suppressed.
- the ninth embodiment is different from the first to sixth embodiments of the present invention in that aluminum or a metal compound mainly containing aluminum is used as a multilayer wiring material. Applicable. Example
- FIG. 8 (a) is a plan view showing the first embodiment of the present invention
- FIG. 8 (b) is a cross-sectional view taken along line A- ⁇ ′ of FIG. 8 (a).
- An RF circuit area (high-frequency signal processing circuit area) 100 and a digital circuit area 200 are provided on a silicon semiconductor substrate.
- a MOSFET 3 is formed in a region on the silicon substrate 1 separated by the shallow trench element isolation film 2 to form a CMOS circuit.
- CMOS circuit complementary metal oxide semiconductor oxide
- a plurality of low dielectric constant insulator rods 8 having a low dielectric constant insulator provided thereon are arranged.
- the low dielectric constant insulator rod 8 reaches the inside of the silicon substrate through the first inter-layer insulating film for insulating and separating the CMOS transistor and the multilayer wiring. That is, the low dielectric constant insulator rod is formed after completing all the CMOS transistor forming steps, or, in other words, after completing all the high temperature heat treatment steps required for forming the CMOS transistor. For this reason, it is possible to bury an insulating film having a lower dielectric constant than a silicon oxide film.
- the silicon substrate 1 is ground after all the device forming steps are completed, and is polished until the bottom surface of the low dielectric constant insulator rod 8 appears in the present embodiment, so that the silicon substrate 1 is thinned. Thin substrate structure As a result, the effective resistance of the silicon substrate is increased, and a low-capacitance substrate region is formed by disposing the low dielectric constant insulator rods, thereby reducing noise propagating through the substrate and reducing loss.
- the source and drain regions of the MOSFET 3 are connected to the first-layer copper wiring buried in the second interlayer insulating film 9 through a tantalum (W) contact plug 5 provided in the first interlayer insulating film 4.
- W tantalum
- a third interlayer insulating film 11 buried with the second-layer copper wiring 12 and a fourth interlayer insulating film 13 buried with the third-layer copper wiring 14 are formed thereon.
- An inductor 40 is formed using the third-layer copper wiring 14 and the second-layer copper wiring 12 in the low-capacity substrate region in which the low dielectric constant insulator rod 8 is disposed.
- a fifth interlayer insulating film 15 is formed on fourth interlayer insulating film 13, a recess is provided in fifth interlayer insulating film 15 in RF circuit region 100, and a fifth interlayer insulating film 15 is formed.
- An opening penetrating through the insulating film 15 and the fourth interlayer insulating film 13 is provided, and a soft magnetic material mainly composed of a NiFe alloy is filled in these concave portions and the opening to form a high magnetic permeability separation region 19.
- the high-permeability separating region 19 is formed in a region including the magnetic core of the inductor 40 and its periphery. As a result, the size of the inductor can be reduced.
- This high magnetic permeability separation region can be formed in a region other than the inductor formation region, and in that case, functions as a magnetic field shield of the RF circuit element.
- the upper surface of the fifth interlayer insulating film 15 is covered with the cover film 20.
- FIGS. 9 and 18 are plan views, and (b) is a cross-sectional view taken along the line A-A '.
- a shallow opening with a depth of 300 nm to 500 nm excluding the element formation region 1A is formed on the surface of the silicon substrate 1, and a silicon oxide film is buried in this opening to form a shallow trench element isolation.
- Film 2 is formed.
- Form p and n-wells (not shown) on 1A grow gate insulating film, form gate electrode, form diffused layer and silicide it, and create CMOS circuits for digital circuits and RF circuits. Forming MOSFET3 to configure.
- a silicon oxide film is deposited, planarized by CMP to form a first interlayer insulating film 4, a via hole is formed to a gate electrode and a diffusion layer, and tungsten is buried to form a W contact plug 5.
- Multi-oxide may be used for the gate insulating film of CMOS for digital circuits and CMOS for RF circuits.
- a High_k gate insulating film such as HfSi ⁇ may be used. It is important that all high-temperature heat treatment at 700 ° C or higher be completed in this transistor formation process.
- a silicon oxide film (not shown) having a thickness of about 50 nm is formed as required, and as shown in FIG. 11, the silicon oxide film penetrates through the first interlayer insulating film 4 and the element isolation film 2 in the RF circuit region 100. Then, an opening 6 reaching the inside of the silicon substrate 1 is formed.
- the shape and depth of the opening 6 but for example, the opening diameter is 13 ⁇ and the depth is 5-30 / im.
- the arrangement of the openings are arranged obliquely.
- the opening may include a groove shape.
- honeycomb honeycomb
- a low dielectric constant insulating film 7 is formed so as to cover the opening 6.
- the material of the low dielectric constant insulating film is not particularly limited, but it is necessary that at least the relative dielectric constant is lower than that of the silicon oxide film.
- a ladder oxide in which a part of oxygen in a silicon oxide film is replaced with hydrogen or a coating insulating film such as MSQ in which methyl is replaced with methyl can be used.
- it may be a plasma CVD film made of carbon-added silica (SiOC) or SiOCH.
- a porous film in which pores of 10 nm or less are dispersed in an insulating film may be used.
- a thin silicon oxide film or silicon nitride film is first grown on the wall surfaces of the openings by thermal CVD, ozone oxidation CVD, or plasma CVD. After that, a low dielectric constant insulating film may be filled.
- the low dielectric constant insulating film on the interlayer insulating film is removed by the CMP method, so that the low dielectric constant insulating rod 8 in which the low dielectric constant insulating film is buried inside the opening is made of silicon. Formed in the substrate.
- all the low dielectric constants on the first interlayer insulating film 4 are used.
- the insulating film 7 is removed by CMP is shown, a part of the insulating film 7 can be used as a separating insulating film between multi-layer wirings.
- a second interlayer insulating film 9 is grown, and a wiring groove for exposing the top of the W contact plug 5 is formed.
- a barrier metal of about 25 nm thickness such as TaZTaN or TiW and a seed copper film of about 100 nm thickness are grown in this wiring groove, and the copper film is grown by electrolytic plating using the seed copper film as an electrode.
- a first layer copper wiring 10 having a damascene structure is formed in the second interlayer insulating film 9 by selectively removing the copper film and the nor metal film by CMP.
- the material of the second interlayer insulating film 9 is not particularly limited, and may be a silicon oxide film, ladder oxide, MSQ, SiOCH, or even a porous film.
- a cap film (not shown) such as SiCN or SiC is formed on the surface of the copper damascene wiring to prevent copper diffusion.
- a multilayer wiring having a fourth interlayer insulating film 13 provided with the provided third interlayer insulating film 11 and the third-layer copper wiring 14 is formed.
- the inductor 40 is formed using the third-layer copper wiring 14 and the second-layer copper wiring 12.
- the number of wiring layers forming the inductor it is necessary that it be located at least on the low-k substrate region where the low-k insulator rods 8 carried on the silicon substrate are arranged. is there.
- a fifth interlayer insulating film 15 is grown on the wiring layer on which the inductor is formed. Then, a concave portion 16 is formed on the surface of the fifth interlayer insulating film 15 on the RF circuit region 100, and an opening 17 that penetrates the fifth interlayer insulating film 15, the fourth interlayer insulating film 13 and reaches the third interlayer insulating film 11 is formed. Form. Note that the surface of the fifth interlayer insulating film 15 may be covered with a silicon oxynitride film.
- a soft magnetic material film 18 covering the recess 16 and the opening 17 is formed so as to cover the fifth interlayer insulating film 15.
- the soft magnetic material film 18 Ta / TiW (TiW is a lower layer) deposited by a sputtering method is used as a barrier metal, and a FeNi film is grown thereon by an electrolytic plating method. Lnm-about 10nm Ru between barrier metal and FeNi, etc. Buffer metal may be interposed.
- the soft magnetic material film is made of soft magnetic metal such as NiFe or fine particles of soft magnetic ferrite such as (Ni, Zn) FeO by ladder oxide or MS.
- the particle diameter of the soft magnetic fine particles is desirably about 500 ⁇ or less.
- a high permeability separation region 19 having a flat plane member and a rod member perpendicular to the substrate surface is formed ( ( Figure 18).
- the inductance (L) can be increased even in a small-sized inductor.
- the relative magnetic permeability is 10 to 100, and a small inductor having an area ratio of about 1Z5 can be formed with the same inductance.
- a cover film 20 is formed to cover the fifth interlayer insulating film 15 on which the high magnetic permeability separation region 19 is formed, and the bottom surface of the low dielectric constant insulator rod 8 is exposed by grinding the back surface of the silicon substrate. Then, the semiconductor device of the present embodiment shown in FIG. 8 can be obtained.
- a high-permeability separating rod 21 having no plain member is used in place of the high-permeability separating region (19) having a plain member and a rod portion.
- the first embodiment shown in FIG. 8 of the present embodiment except that the core is formed around and around the inductor core and the bottom surface of the low dielectric constant insulator rod 8 is not exposed from the back surface of the substrate. Is the same as
- the manufacturing method of this embodiment is the same as that of the first embodiment up to the step shown in FIG. Thereafter, a fifth interlayer insulating film 15 is grown on the wiring layer on which the inductor 40 is formed, and a third interlayer insulating film is penetrated through the fifth interlayer insulating film 15 and the fourth interlayer insulating film 13 around and around the core of the inductor 40.
- An opening to the film 11 is formed.
- the diameter of the opening is generally 1 ⁇ force and 2 ⁇ m ⁇ , but there is no particular limitation. What is important here is that the depth of the opening is larger than the diameter of the opening, that is, the aspect ratio is 1 or more.
- the surface of the fifth interlayer insulating film may be covered with a silicon oxynitride film.
- a barrier metal and a NiFe soft magnetic metal are grown, and the metal film on the fifth interlayer insulating film 15 is removed by CMP, so that the fifth interlayer insulating film 1 is formed on and around the inductor core. 5.
- a high permeability separating rod 21 penetrating through the fourth interlayer insulating film 13 and reaching the third interlayer insulating film is formed.
- soft magnetic particles such as (Ni, Zn) Fe O are insulated with low dielectric constant.
- a coating material dispersed in the film may be applied, and the coating film on the fifth interlayer insulating film 15 may be removed by CMP to form the high magnetic permeability separating rod 21.
- the cover film 20 is deposited, and the back surface of the silicon substrate 1 is ground to obtain the semiconductor device of this embodiment. In grinding, the silicon substrate should be thinned so that the thickness of the silicon substrate is less than twice the length of the low dielectric constant insulator rod in the silicon substrate.
- the coupling capacitance between the inductor and the substrate can be reduced by 50%.
- a fourth-layer copper wiring 22 is formed in a fifth-layer insulating film 15 on a winding wiring of an inductor 40, and a sixth-layer copper wiring 22 is further formed thereon.
- This is the same as the first embodiment shown in FIG. 8, except that an insulating film 23 is formed and a fifth-layer copper wiring 24 is embedded therein.
- the steps up to the formation of the fifth interlayer insulating film 15 are the same as those of the first embodiment.
- a wiring groove and a via hole are opened in the fifth interlayer insulating film 15, and a fourth-layer copper wiring 22 is formed by forming a copper film and performing CMP.
- the high-permeability isolation region 19 is formed using the same method as in the first embodiment.
- a sixth interlayer insulating film 23 and a fifth layer copper wiring 24 are formed, and a cover film 20 is formed thereon. Then, when the back surface of the silicon substrate is ground, the semiconductor device of this embodiment is obtained.
- a high permeability separation plane 25 connected to a high permeability separation region 19 is provided in a recess formed on the surface of the third interlayer insulating film 11. This is the same as the third embodiment except that it is provided.
- the steps up to the formation of the third interlayer insulating film 11 are the same as those of the first and third embodiments.
- a wiring groove and a via hole are opened in the third interlayer insulating film 11, and a second-layer copper wiring 12 is formed by forming a copper film and CMP. I do.
- a recess is formed in the third interlayer insulating film 11, a barrier metal and a NiFe soft magnetic metal are grown, and the metal film on the third interlayer insulating film 11 is removed by CMP, so that the high magnetic permeability separating plane 25 is formed.
- CMP high magnetic permeability separating plane 25 is formed.
- the fifth embodiment of the present invention comprises a semiconductor device in which CMOS is formed on an SOI (silicon on insulator) substrate.
- An RF circuit area 100 and a digital circuit area (not shown) are provided on the SOI substrate.
- an n-channel or p-channel MOSFET 3 which is a thin film transistor is formed on the silicon substrate 1 with a buried oxide film 27 interposed therebetween.
- the MOSFET 3 is covered with a first interlayer insulating film 4, and a first layer wiring 10 a connected to the source / drain region of the MOSFET 3 via a contact plug 5 a is formed on the first interlayer insulating film 4.
- An opening is formed around the MOSFET 3 to reach the inside of the silicon substrate 1 through the first interlayer insulating film 4 and the filled oxide film 27, and a low dielectric constant insulator is buried in the opening. Thus, a low dielectric constant insulator rod 8 is formed.
- one or more interlayer insulating films are formed on the first layer wiring to form a multilayer wiring.
- An inductor and a high magnetic permeability region are formed in the interlayer insulating film of the RF circuit region 100.
- a sixth embodiment of the present invention applies the present invention to a compound semiconductor device.
- a semi-insulating GaAs substrate 28 in a region surrounded by the H + implanted high resistance region 29 is the separation region, the n + -GaAs layer 30 constituting the collector region n- A GaAs layer 31 is formed, and ap + -GaAs layer 32 constituting a base region is formed thereon.
- an _8 & 83 layer 33 constituting an emitter region and an n_InGaAs layer 34 as a contact layer are formed.
- An AuZNi / AuGe layer 35 serving as a collector electrode is formed on the n + _GaAs layer 30, and an AuZPtZTi layer 36 serving as a base electrode is formed on the p + _GaAs layer 32. Further, on the n-InGaAs layer 34, a WSi layer 37 and an AuZPtZTi layer 38 constituting an emitter electrode are formed.
- the H + -implanted high-resistance region 29 and the transistor are covered with a first interlayer insulating film 4, and a first-layer wiring 10a connected to each electrode of the transistor via a contact plug 5a is formed on the first interlayer insulating film 4. Have been.
- An opening is formed around the transistor to penetrate the first interlayer insulating film 4 and the H + -implanted high-resistance region 29 to reach the inside of the semi-insulating GaAs substrate 28.
- the dielectric constant insulator is buried, whereby the low dielectric constant insulator rod 8 is formed.
- one or more interlayer insulating films are formed on the first layer wiring to form a multilayer wiring. Then, an inductor and a high magnetic permeability region are formed in the interlayer insulating film of the RF circuit region 100.
- FIG. 24 (a) is a plan view showing a seventh embodiment of the present invention
- FIG. 24 (b) is a cross-sectional view taken along line A- ⁇ ′ of FIG. 24 (a).
- the present invention is applied to a semiconductor device having an on-chip antenna.
- parts that are the same as the parts of the first embodiment shown in FIG. 8 are given the same reference numerals, and overlapping descriptions will be omitted as appropriate.
- a peripheral high resistance region 400 is provided in the peripheral portion of the semiconductor chip, and an RF circuit region 100 and a digital circuit region 200 are provided inside the semiconductor chip.
- a low dielectric constant insulator rod 8 penetrating through the first interlayer insulating film 4 and the shallow trench element isolation film 2 and reaching the inside of the silicon substrate 1 is formed.
- the on-chip antenna wiring 41 is formed using the fourth-layer copper wiring in the fifth interlayer insulating film 15.
- the on-chip antenna wiring 41 is connected to a MOSFET formed in the RF circuit area 100 via a multilayer wiring.
- An antenna for transmitting and receiving radio waves is indispensable for a semiconductor chip having a wireless function.
- a chip formed on an insulating film, for example, alumina ceramics is separately manufactured for this antenna, and this chip is externally attached to a semiconductor chip having an RF circuit.
- this method has a technical problem that loss and noise are mixed in a connection portion between chips and a problem that miniaturization is difficult.
- forming an antenna on-chip Although these technical problems can be solved by, for example, conventionally, even if an antenna is formed on a silicon semiconductor chip, radio waves are shielded due to the low resistance of the silicon substrate, and the antenna is formed efficiently. The power I could't do.
- a high-resistance and low-dielectric peripheral high-resistance region 400 in which a low-dielectric-constant insulator rod 8 is buried is formed in the periphery of a chip to form a semiconductor.
- An antenna is formed on the uppermost wiring layer of the chip.
- the reason for installing the antenna in the surrounding area is to increase the antenna length and improve the transmission and reception efficiency.
- the shape of the force antenna in which the loop-shaped antenna is installed around the chip there is no limitation on the shape of the force antenna in which the loop-shaped antenna is installed around the chip.
- the chip may be I-shaped only on one side, L-shaped only on two sides, or U-shaped only on three sides. Further, a multi-loop structure may be used.
- FIG. 25 (a) is a plan view showing an eighth embodiment of the present invention
- FIG. 25 (b) is a cross-sectional view taken along line A- ⁇ ′ of FIG. 25 (a).
- the present embodiment is characterized in that the antenna wiring has a multilayer structure and a grounded shield wiring 42 is provided along the inner periphery of the on-chip antenna wiring 41 of the multilayer structure. Except for this point, it is the same as the seventh embodiment shown in FIG.
- the multilayer antenna wiring has a structure in which antenna wiring buried in a slit-shaped opening penetrating the interlayer insulating film and circling the chip outer peripheral portion is stacked in multiple stages. That is, the antenna wiring wall from the uppermost layer wiring to the lowermost layer wiring is formed around the chip.
- the antenna wiring does not necessarily have to be formed from the uppermost wiring to the lowermost wiring.
- the antenna wiring may be formed in multiple layers such as two layers of the upper wiring.
- the shield wiring 42 is installed inside the antenna wiring.
- This shield wiring also has a structure in which wiring embedded in a slit-shaped opening that surrounds the wiring is multi-layered. That is, the wall of the shield wiring from the uppermost wiring to the lowermost wiring is formed, and this wall has a structure in which electromagnetic noise from the antenna wiring is cut off.
- the multi-layer antenna wiring and the multi-layer shield wiring also have a function of blocking moisture entering the chip outer peripheral force.
- FIG. 42 (a) a first stopper film is formed on the semiconductor substrate on which the shallow trench element isolation layer 2, the MOSFET 3, and the W contact plug 5 are formed so as to function as a stopper in a CMP process performed later. 92, and, if necessary, a sacrifice layer 97 for improving the applicability of the low dielectric constant film.
- the first stopper film 92 is preferably made of a material that can secure a selectivity with respect to the low dielectric constant insulating film 7 and the sacrificial layer 97 in a subsequent CMP process.
- the material include SiN, Si ⁇ N, and SiCN films.
- the sacrificial layer 97 is more preferably an insulating film containing at least silicon and oxygen, such as SiO. More preferably, low dielectric
- the sacrificial layer 97 is preferably made of a hydrophilic material from the viewpoint of improving the applicability when the rate film 7 is formed by a coating method.
- the shape of the pattern Jung may be a square lattice point arrangement, a diagonal arrangement, a random arrangement, or a groove lattice shape. Further, a so-called honeycomb structure in which hexagonal openings are arranged to increase the filling rate may be used.
- the sacrificial layer 97, the first stopper insulating film 92, the first interlayer insulating film 4, and the shallow trench isolation film 2 are plasma-etched.
- the opening 99a is formed by etching.
- the silicon substrate 1 is etched by plasma etching to form an opening 99b.
- the removal of the photoresist 98 shown in FIG. 43 (c) ′ may be performed after etching the silicon substrate.
- a low dielectric constant film 7 to fill the opening is formed.
- the low dielectric constant film 7 the material described in the embodiment of the present specification is used.
- the surplus low dielectric constant film 7 and the sacrifice layer 97 are removed by CMP.
- the first stopper insulating film 92 functions as a CMP stopper, and after the CMP, the structure shown in FIG. 44F is formed.
- a second stopper insulating film 93 is formed (FIG. 44 (g)).
- the second interlayer insulating film 9 is formed thereon as shown in FIG. 45G). Etching is performed by plasma etching.
- the second stopper insulating film 93 functions as an etching stopper, and functions to prevent the low dielectric constant rod 8 from being etched during the etching of the second interlayer insulating film 9.
- a hard mask method using an insulating film formed on the second interlayer insulating film 9 may be used in addition to the resist mask, but this is not illustrated here.
- the second stopper insulating film 93, the first stopper insulating film 92, and the low dielectric constant insulator rod 8 are simultaneously etched by plasma etching.
- the excess metal film is removed by CMP to obtain the structure shown in FIG. 45 (k). Get.
- the metal wiring mainly containing copper is formed by the damascene method on the semiconductor substrate including the low-capacity substrate region by the present manufacturing method
- the second interlayer insulating layer located on the low-capacity substrate region is formed.
- FIG. 46 (e) showing the same structure as FIG. 43 (e).
- the low dielectric constant film 7 is etched by plasma etching to form a low dielectric constant insulator rod 8 (FIG. 46 (f)). It is preferable that the etching be performed under such a condition that the selectivity with the sacrificial layer 97 can be secured.
- the cap insulating film 94 Is deposited to fill the opening above the low dielectric constant insulator rod 8.
- the cap insulating film 94 is removed by CMP at the same time as the sacrificial layer 97, which is preferably an insulator having a higher relative dielectric constant than the low dielectric constant insulator rod 8 and a higher mechanical strength such as elastic modulus and hardness. It is possible that the insulator is preferred.
- the cap insulating film 94 and the sacrificial layer 97 are removed by CMP, and planarization is performed.
- the first stopper insulating film functions as a CMP stopper, the structure shown in FIG. 47H is formed after the CMP.
- the second stopper insulating film 93 functions as an etching stopper, and functions to prevent the cap insulating film 94 from being etched during the etching of the second interlayer insulating film 9.
- a node mask method using an insulating film previously formed on the second interlayer insulating film 9 may be used in addition to the resist mask. ,.
- the second stopper insulating film 93, the first stopper insulating film 92, and the cap insulating film 94 are simultaneously etched by plasma etching (FIG. 48 (1)). Further, after depositing the barrier metal film 102 and the metal wiring film 10 as necessary, the excess metal film is removed by CMP to obtain the structure of FIG. 48 (m).
- the metal wiring mainly containing copper is formed by the damascene method on the semiconductor substrate including the low-capacity substrate region by the present manufacturing method
- the second interlayer insulating layer located on the low-capacity substrate region is formed.
- FIG. 43 (e) the steps up to FIG. 43 (e) follow the same steps, and therefore the description of the steps up to FIG. Description will be made with reference to FIG. 49 (e) showing the same structure as 43 (e).
- the excess low dielectric constant insulating film 7 is removed by plasma etching to form a low dielectric constant insulator rod 8 (FIG. 49 (f)).
- the above-mentioned plasma etching is performed to move the position of the uppermost part of the low dielectric constant insulator pad 8 to a position lower than the uppermost part of the contact plug 5. It is necessary to become.
- an insulator cap 94 is formed on the low dielectric constant insulator rod 8 later.
- the insulator cap 94 is made of, for example, a metal having a higher mechanical strength than the low-dielectric-constant insulator constituting the low-dielectric-constant insulator rod 8 and containing titanium, aluminum, or the like, or an etching plasma of a wiring metal. Materials that are resistant to are preferred.
- the first stopper insulating film 92 functions as a CMP stopper, and after the CMP step, a cross-sectional shape as shown in FIG. 50H is formed.
- the CMP conditions may be set so that the insulating film cap 94 and the sacrificial layer 97 can be removed, and that the selectivity with the first stopper insulating film layer 92 can be ensured.
- the first stopper insulating film layer 92 is removed by plasma etching.
- the plasma etching conditions may be set so that the W contact plug surface is exposed.
- the shape shown in FIG. 50 (i) is more preferable.
- FIG. 51 (j) and FIG. j) Obtain the structure shown in '.
Abstract
Description
Claims
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JP2017017258A (ja) * | 2015-07-03 | 2017-01-19 | 株式会社東芝 | 半導体スイッチ |
Also Published As
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JP4904813B2 (ja) | 2012-03-28 |
US20060157798A1 (en) | 2006-07-20 |
JPWO2004112138A1 (ja) | 2006-09-14 |
US7750413B2 (en) | 2010-07-06 |
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