WO2002041710A1 - Una salsa mayonesa y su procedimiento de fabricacion - Google Patents
Una salsa mayonesa y su procedimiento de fabricacion Download PDFInfo
- Publication number
- WO2002041710A1 WO2002041710A1 PCT/ES2001/000451 ES0100451W WO0241710A1 WO 2002041710 A1 WO2002041710 A1 WO 2002041710A1 ES 0100451 W ES0100451 W ES 0100451W WO 0241710 A1 WO0241710 A1 WO 0241710A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- mayonnaise
- weight
- olive oil
- emulsion
- egg yolk
- Prior art date
Links
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/60—Salad dressings; Mayonnaise; Ketchup
Definitions
- the present invention relates to a new mayonnaise sauce, produced on an industrial scale, which as a distinctive and new character has the following characteristics .- oily ingredient constituted by extra virgin olive oil in its highest percentage, taste and texture as those of the best homemade mayonnaise, stability for prolonged periods of time, absence of additives, and presented packaged in Tetra Brik.
- the invention also relates to a process for the manufacture and packaging of said new mayonnaise.
- the mayonnaise sauce is a very old culinary product, on which historians do not agree either as to the etymology of its name or its origin. According to some, the name would be an alteration of "mayonnaise", which refers to the Menorcan city of Mahon that was taken by the French on June 28, 1756. The Duke of Richelieu was commanded by the French troops to whom his cook offered a sauce called “mayonnaise”, which pleased him so much that he took it to France where he changed his name and became famous.
- Mayonnaise sauce according to a well-known text "is an emulsion of egg yolks and oil that is flavored with vinegar, lemon juice, mustard, salt, pepper... If you want to make it at home, you have to move in the same sense and constantly the yolks, while the oil is incorporated, first drop by drop and then to fine thread to prevent the mixture from being cut.Once well bound, the sauce is seasoned with the rest of the ingredients.
- electric mixers and kitchen robots allow it to be done quickly and without failures.
- the proportion is one glass of oil for each egg yolk, 2 or 3 tablespoons of vinegar, mustard and salt to taste "(" The Book of the Techniques of
- Spanish Patent No. 534830 filed on August 2, 1984 and granted on October 14, 1985 refers to a "Procedure for preparing light food products of the Mayonnaise type", in which together with the three essential ingredients, others are used, in particular stabilizers, and it also has the peculiarity that the producer is in the form of foam that is a consequence of the dispersion of air that forms microbubbles.
- neither extra virgin olive oil is used, and contrary to the product of the present invention employs stabilizers, and in addition the product is presented in the form of foam.
- SUBSTITUTE SHEET (RULE 26) What constitutes this mayonnaise are: edible oil in a proportion less than 10% by weight, water, egg white, microcrystalline cellulose and polydextrose.
- European Patent 0546215 filed on December 12, 1991 and issued on 04-01-1998 refers to: "An emulsion of the oil-in-water type stable against heat and process for its preparation”. Said emulsion consists of 10-85% oil, 1-10% egg yolk, acetic acid, salt, water and 0.1-5 grams of soy lysophosphatidylcholine per 1000 grams of emulsion.
- European Patent Application No. 0758531 filed on August 2, 1996 protects: "Mayonnaise compounds with little or no fat".
- the main characteristic of this product is the use of a methyl ester of galacturonic acid with amides or without amides that replaces part or all of the fat (oil) of the usual mayonnaise.
- European Patent Application No. 0855863 filed on September 18, 1996 refers to a "food sauce” containing 10-60% by weight of oil, and water, and proteins from eggs, milk, vegetables or fruits. It is therefore an emulsion product that in purity cannot be called mayonnaise, while its proteins do not come exclusively from eggs.
- SUBSTITUTE SHEET mayonnaise simply by adding the egg component (either just the yolk, or the whole egg) with the subsequent stirring of the resulting mixture.
- Said premix comprises as essential ingredients: vegetable oil, edible vinegar, an emulsifier (egg yolk expressly excluded), condiments and spices.
- egg yolk expressly excluded
- condiments and spices mayonnaise simply by adding the egg component (either just the yolk, or the whole egg) with the subsequent stirring of the resulting mixture.
- Said premix comprises as essential ingredients: vegetable oil, edible vinegar, an emulsifier (egg yolk expressly excluded), condiments and spices.
- egg yolk expressly excluded
- condiments and spices mayonnaise simply by adding the egg component (either just the yolk, or the whole egg) with the subsequent stirring of the resulting mixture.
- Said premix comprises as essential ingredients: vegetable oil, edible vinegar, an emulsifier (egg yolk expressly excluded), condiments and spices.
- a feature of the product is that it is packaged in oxygen-free
- SUBSTITUTE SHEET (RULE 26) cation of a mayonnaise for immediate consumption, the pH values that are generally obtained are usually in the environment or higher than 4.50; values that, in addition to breaching the Sanitary Technical Regulation (RTS) of Mayonnaise Sauce allow the growth of a whole series of pathogenic microorganisms that would make the product dangerous from a sanitary point of view.
- RTS Sanitary Technical Regulation
- the present invention supposes a surprising technical advance in that it allows for the first time, according to the loyal knowledge and understanding of the inventor and the requesting firm, to obtain an industrial mayonnaise that contains extra virgin olive oil as its main oily ingredient and as a secondary oily ingredient.
- Olive oil a taste and texture like the best homemade mayonnaise, stability for prolonged periods of time, is free of additives, and is marketed and preserved in a Tetra Brik container at a maximum temperature of 12 ° C, under which conditions It lasts for six months. These characteristics make it an exceptional gastronomic product.
- mayonnaise is a food product that is reputed to be dangerous as evidenced by news of events in the media, which have sometimes reported Salmonella poisoning as a result of ingestion in massive mayonnaise banquets in poor conditions . This is due to several factors that if they occur simultaneously multiply the severity of the poisonings:
- SUBSTITUTE SHEET (RULE 26) tion with industrial mayonnaise) but loses all the delicacy of the sauce traditionally made with extra virgin olive oil.
- the selection of an extra virgin olive oil with a maximum determined acidity b) the emulsion temperatures, c) the temperature of incorporation of the egg yolk, d ) the times of incorporation, e) the emulsion speeds and f) the packaging in a system like the Tetra Brik that keeps the product from light and air, avoiding the occurrence of oxidation phenomena and microbial growths that need of these elements that could shorten the life of the product.
- the constituent ingredients of the new mayonnaise object of the invention are: A) Extra virgin olive oil of 40-80% by weight / total weight. B) Olive oil from 20% to 40% by weight / total weight.
- Cider vinegar from 2% to 5% by weight / total weight.
- Extra virgin olive oil is a particular type of virgin olive oil which, according to the definition of the International Olive Oil Council (International Olive Oil Council (International Olive Oil
- SUBSTITUTE SHEET (RULE 26) Council, abbreviated IOOC), the Food Code (of the World Health Organization), and the Regulations of the European Union (EU) is "that obtained from the fruit of the olive tree only by mechanical or other physical means, particularly in conditions thermal conditions that do not lead to tensions in the oil, and that have not undergone any treatment other than washing, decanting, centrifugation and filtration. " This oil has a color that goes from green and yellow-green to golden. Its free acidity expressed as free oleic acid content should not exceed 3.3%.
- Extra virgin olive oil is defined as virgin olive oil whose acidity does not exceed 1% and, among others, has irreproachable organoleptic characteristics, reaching a minimum score of 6.5 in a test panel.
- composition in sterols (% m / m)
- Olive oil is rich in oleic acid (62-83), compared to sunflower or soybean oils whose main component is linoleic acid. Olive oil has, among others, an important cardioprotective activity, specifically, a diet based on this oil helps to: (1) lower harmful cholesterol, that is, the coloesterol associated with low density lipoproteins (LDL-C );
- HDL-C high density lipoproteins
- SUBSTITUTE SHEET (RULE 26) tes) and the resistance of the organism of rats to aging and cell death.
- OLIVE OIL It is the oil obtained by mixing extra virgin olive oil and refined olive oil.
- the characteristics of an ArteOliva oil suitable for use as ingredient B) in the mayonnaise of the present invention are given below.
- PHYSICAL-CHEMICAL CHARACTERISTICS Pale yellow to yellowish-green liquid, transparent with a characteristic odor, practically unstable in alcohol and miscible with petroleum ether.
- composition in sterols (% m / m)
- YEMA DE EGG An ultra-pasteurized liquid industrial egg yolk is used, totally devoid of additives and other ingredients than the egg yolk itself. As an example, the specifications of an egg yolk available on the market for industrial scale use are given. Maker . - Pascual de Aranda S .A. Manufacturer Code - LD- 028
- Organoleptic characteristics . - Presents the color, smell and taste characteristics of freshly beaten egg yolk.
- VINAGRE DE CIDRA (APPLE).
- APPLE VINAGRE DE CIDRA
- the color, appearance, texture, smell and taste are characteristic, without odors or strange or unpleasant flavors
- LEMON JUICE Natural lemon juice is used. It is a yellowish, slightly cloudy liquid that has a strong acid taste and a pleasant smell. It contains 6.7 - 8.6% citric acid, the rest being sugar, gum and trace amounts of potassium carbonate.
- Anti-caking agent 536 10 mg / kg
- An important aspect of the invention is the packaging of the mayonnaise product in a Tetra Brik package.
- the characteristics of a material are given below of this type of stratified structure (manufactured by the Tetra Pak firm), the structure of the layers being arranged in the manner shown in the following scheme:
- the process for manufacturing the mayonnaise object of the present invention comprises the following operations:
- the operation (1) is carried out by mixing the three ingredients with stirring while they are heated to a temperature of 70 to 90 ° C for 1-4 minutes, immediately, they are cooled by a tubular exchanger system, and finally the mixture is brought to a temperature below 23 ° C.
- the egg yolk be removed from the cold room one hour before its use in the manufacture of mayonnaise.
- said yolk is introduced into the container of the emulsion system, preferably KORUMA, where it is brought to a temperature between 18 and 23 ° C.
- the Extra Virgin Olive Oil is introduced at an initial mass flow of 20-25 kg / minute, while the emulsion system agitator is operated at a rotation speed between 2800-3100 rpm and the emulsion temperature being maintained at a value below 23 ° C.
- the emulsion process continues at 2800 - 3100 rpm for a period of 1-3 minutes.
- the batch After verifying that the pH of the product is in the range of 4.00 to 4.10, the batch is ready to be subjected to the packaging operation (3) that is performed in an automatic packaging facility, such as the filler
- SUBSTITUTE SHEET (RULE 26) Tetra Pak, which forms the containers from a coil of flat material and that performs both the functions of packaging formation, sterilization of containers and filling of containers. It should be noted that in this procedure the packaging operation is part of the manufacturing process, as long as the packaging is fully owned the final operation, given that due to the characteristics of the product and the needs of its protection by the specific constituent material of the package, said packaging operation cannot be delayed, after mixing and homogenization of the acid porridge and the egg yolk emulsion + oil phase.
- a high-quality packaging material described in Annex V has been selected.
- the composition of the material is adapted to the requirements of the product, it is protected in an excellent way and maintains its quality until it is consumed.
- Tetra Brik Aseptic system is based on the principle of sealing the containers below the level of the liquid, thus obtaining completely opaque and completely filled containers, therefore free of air. Perhaps this is one of the greatest innovations of our product since it is known the high degree of damage caused by air and light on fatty products (in our case we are talking about 80% of fat in the finished product).
- a PLC (Panel Light Control) system controls the functions of the machine.
- the system works quickly and accurately, and is extremely reliable. Through the signal lamps on the operating panel, the machine operator receives information on the measures to be taken.
- the packaging material is delivered in standard reels or large reels.
- the machine is equipped with an automatic equipment
- SUBSTITUTE SHEET (RULE 26) Tomato splicing, which means that a coil of new packaging material can be automatically spliced to the previous one without the machine operator needing to start this operation.
- the spliced container is automatically separated by the machine.
- the packaging material passes through a 35% hydrogen peroxide bath heated to 72 ° C, which is then removed by rollers.
- the material band then passes through nozzles that project sterile air. In this operation the possible remains of hydrogen peroxide are eliminated.
- the packaging material then acquires the shape of a tube. Sterilization and tube formation take place in a completely closed part of the machine, which prevents recontamination of the material.
- the machine has a very advanced decoration matching system. Photoelectric cells detect the position of the material band and send information to the decoration matching system, which if necessary corrects the material band during the course of production.
- the time for aseptic treatment of the packaging material is, thanks to the deep sterilization bath, long enough, which gives the process high reliability.
- the machines have non-sterile package ejection systems in the event of a stop, they also have mechanisms for the elimination of low Brik
- the packages After packaging, the packages are transferred to a packer and, subsequently, to their palletizing and storage. In order to preserve the stability of the emulsion, the storage and distribution of the product must be carried out at temperatures between 10 and 12 ° C.
- a batch of the industrial mayonnaise object of the invention was manufactured using a KORUMA brand discontinuous emulsion system that processes 600 kg batches of mayonnaise sauce.
- an acid porridge was made consisting of a mixture of cider vinegar, lemon juice and salt. This mixture was heated with stirring to a temperature of 85 ° C for 2 minutes, immediately, it was cooled by a tubular exchanger system, and finally the mixture was brought to a temperature below 23 ° C. The egg yolk was taken out of the cold room, where it was kept, and kept outside before use in time to reach approximately 15 ° C. After this time was introduced into the emulsion system where it was brought to a temperature between 18 and 23 ° C. Then, and under vacuum conditions, which were maintained throughout the process, between -0.4 and -0.5 atmospheres, 150 kg of Extra Virgin Olive Oil were introduced into the emulsion system at a flow rate initial mass of 20-25 kg / minute. The emulsion system agitator was set at a turning speed between 2800-3100 rpm and the
- Emulsion temperature was maintained at a value below 23 ° C, which was achieved by the cooling jacket of said system through which water circulated at a temperature below 15 ° C.
- the rest of the oil phase (the component previously called B) was incorporated using a flow rate of 50-60 kg / minute, and 30-50 seconds later it was added the corresponding amount of acid porridge with an incorporation flow rate of 40-60 kg / minute.
- the emulsion process was continued at 2800-3100 rpm for a time of 1-3 minutes.
- the batch of finished mayonnaise was sent to a Tetra Pak TBA 19 filler which simultaneously performs the functions of packaging formation, sterilization of Packaging and container filling.
- the high quality packaging material was the one described above in which the composition of the material is adapted to the requirements of the product so that it is protected in an excellent way and maintains its quality until it is consumed whenever it is consumed keep at a temperature of 10 to 12 ° C.
- the oil and pH of the four mayonnaises was as follows:
Abstract
Description
Claims
Priority Applications (10)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/415,540 US20040081740A1 (en) | 2000-11-24 | 2001-11-24 | Mayonnaise sauce and preparation method thereof |
ES01997229T ES2236359T3 (es) | 2000-11-24 | 2001-11-24 | Salsa mayonesa y metodo para su preparacion. |
AT01997229T ATE287648T1 (de) | 2000-11-24 | 2001-11-24 | Mayonnaisesauce und zubereitungsverfahren dafür |
JP2002543898A JP4128869B2 (ja) | 2000-11-24 | 2001-11-24 | マヨネーズソースおよびその製造方法 |
DE60108663T DE60108663T2 (de) | 2000-11-24 | 2001-11-24 | Mayonnaisesauce und zubereitungsverfahren dafür |
DK01997229T DK1336340T3 (da) | 2001-11-24 | 2001-11-24 | Mayonnaisesauce og fremgangsmåde til fremstilling deraf |
AU2002221952A AU2002221952A1 (en) | 2000-11-24 | 2001-11-24 | Mayonnaise sauce and preparation method thereof |
BR0115565-2A BR0115565A (pt) | 2000-11-24 | 2001-11-24 | Molho de maionese e seu procedimento de fabricação |
EP01997229A EP1336340B1 (en) | 2000-11-24 | 2001-11-24 | Mayonnaise sauce and preparation method thereof |
MXPA03004594A MXPA03004594A (es) | 2000-11-24 | 2001-11-24 | Una salsa mayonesa y su procedimiento de fabricacion. |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ES200002821A ES2177429B1 (es) | 2000-11-24 | 2000-11-24 | Una salsa mayonesa y su procedimiento de fabricacion. |
ESP200002821 | 2000-11-24 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2002041710A1 true WO2002041710A1 (es) | 2002-05-30 |
Family
ID=8495756
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/ES2001/000451 WO2002041710A1 (es) | 2000-11-24 | 2001-11-24 | Una salsa mayonesa y su procedimiento de fabricacion |
Country Status (11)
Country | Link |
---|---|
US (1) | US20040081740A1 (es) |
EP (1) | EP1336340B1 (es) |
JP (1) | JP4128869B2 (es) |
AT (1) | ATE287648T1 (es) |
AU (1) | AU2002221952A1 (es) |
BR (1) | BR0115565A (es) |
DE (1) | DE60108663T2 (es) |
ES (2) | ES2177429B1 (es) |
MX (1) | MXPA03004594A (es) |
PT (1) | PT1336340E (es) |
WO (1) | WO2002041710A1 (es) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2005052081A (ja) * | 2003-08-05 | 2005-03-03 | Kao Corp | 麺サラダ用ソース |
CN105614398A (zh) * | 2015-06-25 | 2016-06-01 | 开平市水口镇卡摩商行 | 一种陈皮柠檬酱的制备方法 |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES2317816B1 (es) * | 2008-12-29 | 2010-03-15 | Gourmed Diet,S.L. | Producto emulsionado untable a base de aceite de oliva y/u otros aceites vegetales y su procedimiento de preparacion. |
EP2484218A1 (en) * | 2011-02-03 | 2012-08-08 | Bunge ZRt. | New process for preparing stable oil in water emulsion without additives |
WO2019057407A1 (en) | 2017-09-22 | 2019-03-28 | Unilever N.V. | COMPOSITION COMPRISING A PLANT OIL, A SOURCE OF ORGANIC ACIDS, PHENOLIC COMPOUNDS AND AMINO ACIDS |
EP3459365A1 (en) | 2017-09-22 | 2019-03-27 | Unilever N.V. | Composition comprising vegetable oil and apple cider vinegar |
WO2019066645A1 (en) | 2017-09-28 | 2019-04-04 | JPN Business Development B.V. | NUTRIENT BEVERAGE COMPRISING VIRGIN OLIVE OIL |
WO2019165002A2 (en) * | 2018-02-20 | 2019-08-29 | Isoage Technologies Llc | Compositions for retarding rancidity in oil-based food sauces and dressings |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES8603748A1 (es) * | 1983-08-02 | 1986-01-01 | Battelle Memorial Institute | Procedimiento para preparar productos alimenticios ligeros del tipo mayonesa |
EP0377312A1 (en) * | 1989-01-06 | 1990-07-11 | Kraft, Incorporated | Low oil mayonnaise |
WO1999001042A1 (fr) * | 1997-07-03 | 1999-01-14 | Morita Co., Ltd. | Premelange pour mayonnaise et son procede de preparation |
WO2000030473A1 (en) * | 1998-11-25 | 2000-06-02 | Lekic Mirjana | Mayonnaise comprising olive oil and whey |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1820909A (en) * | 1922-04-08 | 1931-09-01 | Samuel B Drucker | Method of making mayonnaise |
US6221420B1 (en) * | 1993-07-30 | 2001-04-24 | National Starch And Chemical Investment Holding Corporation | Foods containing thermally-inhibited starches and flours |
US6113971A (en) * | 1994-07-25 | 2000-09-05 | Elmaleh; David R. | Olive oil butter |
US6132793A (en) * | 1998-06-12 | 2000-10-17 | Olivia Gourmet Ltd. | Method of manufacturing a butterlike composition |
EP1013753B1 (en) * | 1998-12-22 | 2006-03-08 | Unilever N.V. | Refining of vegetable oil |
HUP0104810A3 (en) * | 1998-12-23 | 2005-05-30 | Unilever Nv | Fortification of food products with olive fruit ingredients |
ATE321832T1 (de) * | 2000-05-04 | 2006-04-15 | Unilever Nv | Verfahren zur aufbereitung von oliven |
US6475549B1 (en) * | 2000-11-06 | 2002-11-05 | Jeanne M. Ruhl | Caesar salad dressing |
-
2000
- 2000-11-24 ES ES200002821A patent/ES2177429B1/es not_active Expired - Fee Related
-
2001
- 2001-11-24 US US10/415,540 patent/US20040081740A1/en not_active Abandoned
- 2001-11-24 AU AU2002221952A patent/AU2002221952A1/en not_active Abandoned
- 2001-11-24 WO PCT/ES2001/000451 patent/WO2002041710A1/es active IP Right Grant
- 2001-11-24 PT PT01997229T patent/PT1336340E/pt unknown
- 2001-11-24 EP EP01997229A patent/EP1336340B1/en not_active Expired - Lifetime
- 2001-11-24 BR BR0115565-2A patent/BR0115565A/pt not_active Application Discontinuation
- 2001-11-24 MX MXPA03004594A patent/MXPA03004594A/es active IP Right Grant
- 2001-11-24 JP JP2002543898A patent/JP4128869B2/ja not_active Expired - Fee Related
- 2001-11-24 ES ES01997229T patent/ES2236359T3/es not_active Expired - Lifetime
- 2001-11-24 DE DE60108663T patent/DE60108663T2/de not_active Expired - Lifetime
- 2001-11-24 AT AT01997229T patent/ATE287648T1/de active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ES8603748A1 (es) * | 1983-08-02 | 1986-01-01 | Battelle Memorial Institute | Procedimiento para preparar productos alimenticios ligeros del tipo mayonesa |
EP0377312A1 (en) * | 1989-01-06 | 1990-07-11 | Kraft, Incorporated | Low oil mayonnaise |
WO1999001042A1 (fr) * | 1997-07-03 | 1999-01-14 | Morita Co., Ltd. | Premelange pour mayonnaise et son procede de preparation |
WO2000030473A1 (en) * | 1998-11-25 | 2000-06-02 | Lekic Mirjana | Mayonnaise comprising olive oil and whey |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2005052081A (ja) * | 2003-08-05 | 2005-03-03 | Kao Corp | 麺サラダ用ソース |
JP4495932B2 (ja) * | 2003-08-05 | 2010-07-07 | 花王株式会社 | 麺サラダ用ソース |
CN105614398A (zh) * | 2015-06-25 | 2016-06-01 | 开平市水口镇卡摩商行 | 一种陈皮柠檬酱的制备方法 |
Also Published As
Publication number | Publication date |
---|---|
ATE287648T1 (de) | 2005-02-15 |
MXPA03004594A (es) | 2004-10-14 |
EP1336340A1 (en) | 2003-08-20 |
ES2236359T3 (es) | 2005-07-16 |
EP1336340B1 (en) | 2005-01-26 |
DE60108663D1 (de) | 2005-03-03 |
ES2177429B1 (es) | 2004-08-16 |
US20040081740A1 (en) | 2004-04-29 |
BR0115565A (pt) | 2003-09-23 |
JP4128869B2 (ja) | 2008-07-30 |
DE60108663T2 (de) | 2005-12-22 |
JP2004513659A (ja) | 2004-05-13 |
ES2177429A1 (es) | 2002-12-01 |
AU2002221952A1 (en) | 2002-06-03 |
PT1336340E (pt) | 2005-05-31 |
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