WO1986002286A1 - Procede de dispersion, et machine pour sa mise en oeuvre - Google Patents

Procede de dispersion, et machine pour sa mise en oeuvre Download PDF

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Publication number
WO1986002286A1
WO1986002286A1 PCT/EP1985/000526 EP8500526W WO8602286A1 WO 1986002286 A1 WO1986002286 A1 WO 1986002286A1 EP 8500526 W EP8500526 W EP 8500526W WO 8602286 A1 WO8602286 A1 WO 8602286A1
Authority
WO
WIPO (PCT)
Prior art keywords
grinding
grinding media
agitator mill
agitator
length
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP1985/000526
Other languages
German (de)
English (en)
French (fr)
Inventor
Friedrich Vock
Gerg Kissau
Klaus Warnke
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF Farben und Fasern AG
Original Assignee
BASF Farben und Fasern AG
BASF Lacke und Farben AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF Farben und Fasern AG, BASF Lacke und Farben AG filed Critical BASF Farben und Fasern AG
Priority to AT85904973T priority Critical patent/ATE40056T1/de
Priority to BR8507233A priority patent/BR8507233A/pt
Priority to DE8585904973T priority patent/DE3567584D1/de
Publication of WO1986002286A1 publication Critical patent/WO1986002286A1/de
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/16Mills in which a fixed container houses stirring means tumbling the charge

Definitions

  • the invention relates to a Di spergi erhabilit according to the preamble of claim 1.
  • agitator mills It is known to separate solids in a liquid phase, e.g. To disperse pigments and fillers in a solution of a binder, in agitator mills by adding mechanical energy.
  • the agitator mills contain grinding media, e.g. Sand, and the. Energy is supplied by the movement of rotors arranged in the agitator mill.
  • the grinding chamber of the agitator mill is filled with 70 to 90% by volume of sand.
  • the regrind flows through the grinding chamber in the axial direction.
  • the throughput of the millbase through the milling pot is generally selected such that the prescribed nominal fineness is achieved after one or more passages. This procedure is often referred to as single or multi-pass mode.
  • the production output achievable with this procedure can be increased significantly if the procedure described in DE-PS 22 30 766 or DE-OS 19 02 152 is used.
  • this circular mode of operation high throughputs of millbase are passed through the mill; after leaving the mill, the millbase flows back into a container from which it is pumped back into the mill becomes.
  • the regrind flows in the so-called pendulum drive from a container with high throughputs through the agitator mill * into a second container. This process is repeated until the target fineness is reached.
  • the invention therefore relates to a dispersing process according to claim 1.
  • Grinding body filling forms a rotating hollow cylinder in the agitator mill due to the centrifugal force.
  • the dispersion of temperature-sensitive goods can also be carried out without any problems, since only a slight increase in the temperature of the ground material can be determined per passage through the agitator mill. This heat can easily be extracted from the regrind in an external cooler. With this procedure, a significant reduction in the dispersing energy used is additionally achieved compared to the passage mode.
  • fine grinding media can be used at high throughputs through the mill, the use of which is not possible in machines which correspond to the prior art because they are attached to the separating screen at high throughputs. be washed up.
  • the invention also relates to an agitator mill for carrying out the dispersion process.
  • Fig. 1 shows a vertical longitudinal section through an agitator mill
  • Fig. 2 shows a vertical cross section through a
  • FIG. 4 a section corresponding to FIG. 1, but with a fixed cylindrical separating screen
  • FIG. 5 a section through an agitator mill according to FIG. 1, but with screens arranged on a pitch circle
  • Fig. 6 shows a section according to FIG. 2 through the
  • FIG. 8 an agitator mill with a fixed dip tube and in 9 shows an agitator mill with a rotating sieve in a space free of grinding media.
  • 1 denotes a grinding container in which rotors 2 designed as paddles are arranged.
  • the ground material is fed in at 3 and a sieve is shown at 4. 5 with a storage container is designated.
  • the rotors 2 are driven by a hollow shaft 6, which at the same time serves to discharge the ground material.
  • a turret seal is shown and 8 is the required pump.
  • 9 designates a manometer and 10 designates the grinding media bed within the grinding container 1.
  • a discharge sieve for residual products is shown and the mill outlet is indicated by arrow 12, while the mill inlet is indicated by arrow 13.
  • the cooling water inlet and at 15 the cooling water outlet is 1 t.
  • FIG. 2 an idealized millbase path is shown at 16, while the arrows 17 and 18 indicate the radial speed of the millbase or the circumferential speed of the millbase.
  • Grist consisting of 30.5% by weight of an alkyl resin 60.5% by weight of titanium dioxide
  • Type of grinding media S licium zirconium oxide grinding media (diameter 0.6 - 2.5 mm)
  • FIG. 4 shows, as in FIG. 1, a cross section through an agitator mill according to the invention, but now with a fixed cylindrical separating sieve 4.
  • FIG. 7 shows, in a representation corresponding to FIG. 5, screens 4 arranged on a pitch circle, but this time fixed, i.e. are not designed to rotate.
  • Fig. 8 shows as a grinding body separating device a fixed immersion tube 21 which protrudes into the space free of grinding media. A sieve is not provided.
  • FIG. 9 shows, as the grinding body separating device, a screen 22 rotating in the grinding body-free space, the speed of which is independent of the speed of the rotor drive.

Landscapes

  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Crushing And Grinding (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Disintegrating Or Milling (AREA)
  • Combined Means For Separation Of Solids (AREA)
PCT/EP1985/000526 1984-10-16 1985-10-09 Procede de dispersion, et machine pour sa mise en oeuvre Ceased WO1986002286A1 (fr)

Priority Applications (3)

Application Number Priority Date Filing Date Title
AT85904973T ATE40056T1 (de) 1984-10-16 1985-10-09 Dispergierverfahren und ruehrwerksmuehle zu seiner durchfuehrung.
BR8507233A BR8507233A (pt) 1984-10-16 1985-10-09 Processo de dispersao e moinho misturador para sua concretizacao
DE8585904973T DE3567584D1 (en) 1984-10-16 1985-10-09 Dispersion process, and stirring machine for its implementation

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19843437866 DE3437866A1 (de) 1984-10-16 1984-10-16 Dispergierverfahren und ruehrwerksmuehle zu seiner durchfuehrung
DEP3437866.9 1984-10-16

Publications (1)

Publication Number Publication Date
WO1986002286A1 true WO1986002286A1 (fr) 1986-04-24

Family

ID=6247996

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP1985/000526 Ceased WO1986002286A1 (fr) 1984-10-16 1985-10-09 Procede de dispersion, et machine pour sa mise en oeuvre

Country Status (9)

Country Link
US (1) US5011089A (enExample)
EP (1) EP0214145B1 (enExample)
JP (2) JPS62500503A (enExample)
BR (1) BR8507233A (enExample)
CA (1) CA1272174A (enExample)
DE (2) DE3437866A1 (enExample)
ES (1) ES8703296A1 (enExample)
WO (1) WO1986002286A1 (enExample)
ZA (1) ZA857434B (enExample)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3727863C1 (de) * 1987-08-20 1989-03-02 Netzsch Erich Holding Ruehrwerksmuehle mit Zufuehrrohr fuer Mahlkoerper
EP0446744A1 (de) * 1990-03-12 1991-09-18 BASF Aktiengesellschaft Dispergierverfahren und Rührwerksmühle zu seiner Durchführung
EP0448100A1 (de) * 1990-03-21 1991-09-25 Erich Netzsch GmbH & Co. Holding KG Rührwerksmühle
US6021969A (en) * 1998-05-05 2000-02-08 Draiswerke Gmbh Agitator mill

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NZ226551A (en) * 1987-10-20 1990-03-27 Ici Australia Operations Fine grinding of ceramic particles in attrition mill
JP2579984B2 (ja) * 1988-01-28 1997-02-12 株式会社クボタ 粒状体の製造方法及びその製造装置
JPH04166246A (ja) * 1990-10-31 1992-06-12 Matsushita Electric Ind Co Ltd 媒体撹拌ミル及び粉砕方法
DE4128074C2 (de) * 1991-08-23 1995-06-29 Omya Gmbh Rührwerkskugelmühle
DE4216939C2 (de) * 1992-05-22 1995-01-26 Kneisl Wendelin Dipl Ing Th Rührwerksmühle mit dynamischer Mahlkörperabtrennung
US5269234A (en) * 1992-10-20 1993-12-14 Continental Cement Company Method for processing solid, Hazardous waste material for use as a fuel
US5333804A (en) * 1993-08-20 1994-08-02 Premier Mill Corp. Agitator mill
US5746916A (en) * 1994-01-26 1998-05-05 Mitsubishi Rayon Co., Ltd. Microporous membrane made of non-crystalline polymers and method of producing the same
DE4432154A1 (de) * 1994-09-09 1996-03-14 Evv Vermoegensverwaltungs Gmbh Verfahren und Vorrichtung zum kontinuierlichen Aufschließen von organischen Bestandteilen eines fließfähigen Behandlungsguts
DE4432153A1 (de) * 1994-09-09 1996-03-14 Evv Vermoegensverwaltungs Gmbh Verfahren und Vorrichtung zum kontinuierlichen autogenen Mahlen eines fließfähigen Behandlungsguts
PL192081B1 (pl) 1997-08-29 2006-08-31 Lowan Man Pty Ltd Sposób mielenia rozdrobnionego materiału i młyn do rozdrobnionego materiału
AU732830B2 (en) * 1997-08-29 2001-05-03 Lowan (Management) Pty Limited Grinding mill
US6450428B1 (en) 1999-05-05 2002-09-17 Lowan (Management) Pty Limited Feed arrangement for grinding mill incorporating fluid feed
AU2003902661A0 (en) * 2003-05-29 2003-06-12 Hicom International Pty Ltd Centrifugal grinding mills
JP4785355B2 (ja) * 2004-06-28 2011-10-05 関西ペイント株式会社 アニュラー型ビーズミル、該ビーズミルを備える顔料分散システム、及び該顔料分散システムを用いた顔料分散方法
EP1943022B1 (de) * 2005-10-11 2010-03-31 Bühler AG Rührwerksmühle
CN107309054A (zh) * 2017-06-29 2017-11-03 马鞍山市恒达轻质墙体材料有限公司 一种加气砖中粉料的生产装置
CN107970856B (zh) * 2017-12-13 2024-01-23 北方奥钛纳米技术有限公司 高效分散装置
DE102021101527B4 (de) 2021-01-25 2023-05-17 Wilhelm Niemann Gmbh & Co. Rührwerksmühle

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE707525C (de) * 1936-04-21 1941-06-25 August Schaich Dr Ing Wirbelmuehle
US2592994A (en) * 1942-05-28 1952-04-15 Smidth & Co As F L Method and apparatus for grinding by the use of grinding bodies subjected to centrifugal force
US3251578A (en) * 1961-06-15 1966-05-17 Socony Mobil Oil Co Inc Dispersing and grinding apparatus and method of dispersing and grinding paste
FR1572760A (enExample) * 1967-07-01 1969-06-27
DE1902152A1 (de) * 1969-01-17 1970-07-30 Draiswerke Gmbh Verfahren und Vorrichtung zum diskontinuierlichen Zerkleinern von in Fluessigkeit suspendierten Teilchen
US3550915A (en) * 1968-04-10 1970-12-29 Vyzk Ustav Organ Syntez Agitating apparatus
DE2230766A1 (de) * 1971-07-27 1973-05-10 Union Process International Verfahren und vorrichtung zum zerkleinern von in einer fluessigkeit enthaltenen feststoffen
FR2433981A1 (fr) * 1978-08-24 1980-03-21 Buehler Ag Geb Broyeur-agitateur a billes equipe d'un circuit de regulation

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH477229A (de) * 1967-03-21 1969-08-31 Vyzk Ustav Organ Syntez Vorrichtung zum Dispergieren von Suspensionen fester Teilchen auf kolloidale Feinheit
DE2110336A1 (de) * 1971-03-04 1972-09-07 Draiswerke Gmbh Ruehrwerksmuehle
US3799455A (en) * 1972-06-19 1974-03-26 A Szegvari Method for reacting materials
US4044957A (en) * 1976-02-13 1977-08-30 Schold George R Apparatus for dispersing finely divided solid particles in a liquid vehicle
ES449975A1 (es) * 1976-07-20 1977-07-01 Oliver & Battle Sa Mejoras en los molinos de eje horizontal refrigerados, para productos predispersados de solidos en liquidos.
JPS5892468A (ja) * 1981-11-27 1983-06-01 株式会社三井三池製作所 竪型メデイヤ撹拌乾式粉砕機
DE3345680A1 (de) * 1983-12-16 1985-06-20 Gebrüder Netzsch, Maschinenfabrik GmbH & Co, 8672 Selb Ruehrwerksmuehle
US4742966A (en) * 1985-06-21 1988-05-10 Morehouse Industries, Inc. Media mill screen assembly

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE707525C (de) * 1936-04-21 1941-06-25 August Schaich Dr Ing Wirbelmuehle
US2592994A (en) * 1942-05-28 1952-04-15 Smidth & Co As F L Method and apparatus for grinding by the use of grinding bodies subjected to centrifugal force
US3251578A (en) * 1961-06-15 1966-05-17 Socony Mobil Oil Co Inc Dispersing and grinding apparatus and method of dispersing and grinding paste
FR1572760A (enExample) * 1967-07-01 1969-06-27
US3550915A (en) * 1968-04-10 1970-12-29 Vyzk Ustav Organ Syntez Agitating apparatus
DE1902152A1 (de) * 1969-01-17 1970-07-30 Draiswerke Gmbh Verfahren und Vorrichtung zum diskontinuierlichen Zerkleinern von in Fluessigkeit suspendierten Teilchen
DE2230766A1 (de) * 1971-07-27 1973-05-10 Union Process International Verfahren und vorrichtung zum zerkleinern von in einer fluessigkeit enthaltenen feststoffen
FR2433981A1 (fr) * 1978-08-24 1980-03-21 Buehler Ag Geb Broyeur-agitateur a billes equipe d'un circuit de regulation

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3727863C1 (de) * 1987-08-20 1989-03-02 Netzsch Erich Holding Ruehrwerksmuehle mit Zufuehrrohr fuer Mahlkoerper
EP0304062A3 (de) * 1987-08-20 1990-01-10 Erich Netzsch GmbH & Co. Holding KG Rührwerksmühle mit Zuführrohr für Mahlkörper
EP0446744A1 (de) * 1990-03-12 1991-09-18 BASF Aktiengesellschaft Dispergierverfahren und Rührwerksmühle zu seiner Durchführung
EP0448100A1 (de) * 1990-03-21 1991-09-25 Erich Netzsch GmbH & Co. Holding KG Rührwerksmühle
US6021969A (en) * 1998-05-05 2000-02-08 Draiswerke Gmbh Agitator mill
DE19819967B4 (de) * 1998-05-05 2007-04-26 BüHLER GMBH Rührwerksmühle

Also Published As

Publication number Publication date
JPH089017B2 (ja) 1996-01-31
JPS62500503A (ja) 1987-03-05
ES547946A0 (es) 1987-02-16
DE3567584D1 (en) 1989-02-23
ES8703296A1 (es) 1987-02-16
EP0214145B1 (de) 1989-01-18
ZA857434B (en) 1986-05-28
EP0214145A1 (de) 1987-03-18
US5011089A (en) 1991-04-30
DE3437866A1 (de) 1986-04-17
BR8507233A (pt) 1987-10-27
JPH0342052A (ja) 1991-02-22
CA1272174A (en) 1990-07-31
JPH0261298B2 (enExample) 1990-12-19

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