TWI789013B - 鈦材及鈦材之製造方法 - Google Patents
鈦材及鈦材之製造方法 Download PDFInfo
- Publication number
- TWI789013B TWI789013B TW110134275A TW110134275A TWI789013B TW I789013 B TWI789013 B TW I789013B TW 110134275 A TW110134275 A TW 110134275A TW 110134275 A TW110134275 A TW 110134275A TW I789013 B TWI789013 B TW I789013B
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- TW
- Taiwan
- Prior art keywords
- titanium material
- titanium
- atomic
- mass
- less
- Prior art date
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- 239000010936 titanium Substances 0.000 title claims abstract description 175
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title claims abstract description 171
- 229910052719 titanium Inorganic materials 0.000 title claims abstract description 170
- 239000000463 material Substances 0.000 title claims abstract description 145
- 238000004519 manufacturing process Methods 0.000 title claims description 30
- 239000000203 mixture Substances 0.000 claims abstract description 23
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 claims abstract description 20
- 239000000126 substance Substances 0.000 claims abstract description 8
- 239000011701 zinc Substances 0.000 claims description 38
- 239000011575 calcium Substances 0.000 claims description 36
- 238000004140 cleaning Methods 0.000 claims description 32
- 239000007864 aqueous solution Substances 0.000 claims description 26
- 238000010438 heat treatment Methods 0.000 claims description 25
- 159000000007 calcium salts Chemical class 0.000 claims description 22
- 238000007654 immersion Methods 0.000 claims description 21
- 150000003751 zinc Chemical class 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 18
- 238000005406 washing Methods 0.000 claims description 18
- 238000006243 chemical reaction Methods 0.000 claims description 13
- 239000011261 inert gas Substances 0.000 claims description 12
- 230000000694 effects Effects 0.000 description 15
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 14
- 229910052760 oxygen Inorganic materials 0.000 description 13
- 229910001069 Ti alloy Inorganic materials 0.000 description 12
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 12
- 239000001301 oxygen Substances 0.000 description 12
- 238000004544 sputter deposition Methods 0.000 description 11
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 10
- 238000005554 pickling Methods 0.000 description 10
- 238000004458 analytical method Methods 0.000 description 9
- 238000007598 dipping method Methods 0.000 description 9
- 238000002845 discoloration Methods 0.000 description 9
- 239000007789 gas Substances 0.000 description 9
- 238000005259 measurement Methods 0.000 description 9
- 229910004298 SiO 2 Inorganic materials 0.000 description 8
- 230000002378 acidificating effect Effects 0.000 description 7
- 238000005097 cold rolling Methods 0.000 description 7
- 230000007797 corrosion Effects 0.000 description 7
- 238000005260 corrosion Methods 0.000 description 7
- 238000011156 evaluation Methods 0.000 description 7
- 239000011787 zinc oxide Substances 0.000 description 7
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 6
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 6
- 239000004566 building material Substances 0.000 description 6
- 239000000292 calcium oxide Substances 0.000 description 6
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 6
- 229910052799 carbon Inorganic materials 0.000 description 6
- 229910017604 nitric acid Inorganic materials 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 238000000137 annealing Methods 0.000 description 5
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 5
- 238000013461 design Methods 0.000 description 5
- 238000004090 dissolution Methods 0.000 description 5
- 229910052731 fluorine Inorganic materials 0.000 description 5
- 238000002844 melting Methods 0.000 description 5
- 230000008018 melting Effects 0.000 description 5
- 238000004445 quantitative analysis Methods 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 4
- 206010021143 Hypoxia Diseases 0.000 description 4
- 229910052791 calcium Inorganic materials 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 239000011737 fluorine Substances 0.000 description 4
- 238000005098 hot rolling Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 238000005096 rolling process Methods 0.000 description 4
- 235000002639 sodium chloride Nutrition 0.000 description 4
- 229910052786 argon Inorganic materials 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 239000001307 helium Substances 0.000 description 3
- 229910052734 helium Inorganic materials 0.000 description 3
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 238000010301 surface-oxidation reaction Methods 0.000 description 3
- 229910052725 zinc Inorganic materials 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 229910010413 TiO 2 Inorganic materials 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000003916 acid precipitation Methods 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000013590 bulk material Substances 0.000 description 2
- 238000004364 calculation method Methods 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000003112 inhibitor Substances 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000012528 membrane Substances 0.000 description 2
- 239000005416 organic matter Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000004451 qualitative analysis Methods 0.000 description 2
- 230000008439 repair process Effects 0.000 description 2
- 238000005211 surface analysis Methods 0.000 description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- 229910000883 Ti6Al4V Inorganic materials 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000005275 alloying Methods 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000010894 electron beam technology Methods 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 238000012552 review Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
- 238000004506 ultrasonic cleaning Methods 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/10—Alloys containing non-metals
- C22C1/1026—Alloys containing non-metals starting from a solution or a suspension of (a) compound(s) of at least one of the alloy constituents
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C14/00—Alloys based on titanium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21B—ROLLING OF METAL
- B21B3/00—Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/16—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
- C22F1/18—High-melting or refractory metals or alloys based thereon
- C22F1/183—High-melting or refractory metals or alloys based thereon of titanium or alloys based thereon
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
- C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
- C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/82—After-treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Thermal Sciences (AREA)
- Physics & Mathematics (AREA)
- Chemical Treatment Of Metals (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
- Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2020155144 | 2020-09-16 | ||
| JP2020-155144 | 2020-09-16 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| TW202217014A TW202217014A (zh) | 2022-05-01 |
| TWI789013B true TWI789013B (zh) | 2023-01-01 |
Family
ID=80776116
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW110134275A TWI789013B (zh) | 2020-09-16 | 2021-09-14 | 鈦材及鈦材之製造方法 |
Country Status (7)
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002047589A (ja) * | 2000-07-28 | 2002-02-15 | Nippon Steel Corp | 変色を生じにくいチタン材とその製造方法 |
| CN102146577A (zh) * | 2010-02-05 | 2011-08-10 | 佳木斯大学 | 一种纯钛金属表面微弧氧化处理电解液及其抗菌性生物活性涂层制备方法 |
| CN104674320A (zh) * | 2013-11-29 | 2015-06-03 | 中国科学院金属研究所 | 一种钛或钛合金表面耐磨抑菌生物活性陶瓷膜制备方法和应用 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6267181A (ja) * | 1985-09-19 | 1987-03-26 | Nippon Parkerizing Co Ltd | チタン又はその合金材料の化成処理方法 |
| JP3382040B2 (ja) * | 1994-11-30 | 2003-03-04 | 日本パーカライジング株式会社 | チタン又はチタン合金用化成処理液及びその表面処理方法 |
| JP3219690B2 (ja) * | 1996-06-18 | 2001-10-15 | 株式会社神戸製鋼所 | 耐変色性に優れた屋外用チタンまたはチタン合金材 |
| JP3566930B2 (ja) * | 2000-02-23 | 2004-09-15 | 新日本製鐵株式会社 | 大気環境中において変色を生じにくいチタンおよびその製造方法 |
| JP4261820B2 (ja) * | 2002-05-02 | 2009-04-30 | 新日本製鐵株式会社 | 耐変色性に優れた酸性雨大気環境用チタンの製造方法 |
| JP4541726B2 (ja) | 2003-03-20 | 2010-09-08 | 株式会社神戸製鋼所 | 建材用純チタン材の製造方法 |
| JP4038171B2 (ja) | 2003-10-29 | 2008-01-23 | 新日本製鐵株式会社 | 大気環境中において耐変色性に優れたチタン |
| JP4221340B2 (ja) * | 2004-07-23 | 2009-02-12 | 新日本製鐵株式会社 | 大気環境中において変色を生じにくいチタンおよびチタン合金とその製造方法 |
| JP4542449B2 (ja) * | 2005-03-10 | 2010-09-15 | 新日本製鐵株式会社 | 屋内環境で使用される製品の部材に用いられるチタンまたはチタン合金の表面の白色度および耐変色性を向上させる処理方法、およびそのチタンまたはチタン合金 |
| JP4603934B2 (ja) * | 2005-05-31 | 2010-12-22 | 新日本製鐵株式会社 | 大気環境中において変色を生じにくい発色の純チタン |
| JP2016068145A (ja) * | 2014-10-01 | 2016-05-09 | 新日鐵住金株式会社 | チタン板およびその製造方法 |
| CN107841778B (zh) * | 2016-09-18 | 2019-04-16 | 中国科学院上海硅酸盐研究所 | 一种医用金属材料的表面改性方法 |
| US10465292B2 (en) * | 2016-10-07 | 2019-11-05 | Goodrich Corporation | Anti-corrosion and/or passivation composition for metal-containing substrates and methods for making, enhancing, and applying the same |
-
2021
- 2021-09-14 CN CN202180062490.6A patent/CN116133765B/zh active Active
- 2021-09-14 WO PCT/JP2021/033742 patent/WO2022059672A1/ja active Application Filing
- 2021-09-14 KR KR1020237008169A patent/KR20230048534A/ko active Pending
- 2021-09-14 JP JP2022550563A patent/JP7389393B2/ja active Active
- 2021-09-14 US US18/022,771 patent/US20230357893A1/en active Pending
- 2021-09-14 TW TW110134275A patent/TWI789013B/zh active
-
2023
- 2023-03-12 SA SA523442925A patent/SA523442925B1/ar unknown
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002047589A (ja) * | 2000-07-28 | 2002-02-15 | Nippon Steel Corp | 変色を生じにくいチタン材とその製造方法 |
| CN102146577A (zh) * | 2010-02-05 | 2011-08-10 | 佳木斯大学 | 一种纯钛金属表面微弧氧化处理电解液及其抗菌性生物活性涂层制备方法 |
| CN104674320A (zh) * | 2013-11-29 | 2015-06-03 | 中国科学院金属研究所 | 一种钛或钛合金表面耐磨抑菌生物活性陶瓷膜制备方法和应用 |
Also Published As
| Publication number | Publication date |
|---|---|
| US20230357893A1 (en) | 2023-11-09 |
| CN116133765A (zh) | 2023-05-16 |
| WO2022059672A1 (ja) | 2022-03-24 |
| JP7389393B2 (ja) | 2023-11-30 |
| KR20230048534A (ko) | 2023-04-11 |
| JPWO2022059672A1 (enrdf_load_stackoverflow) | 2022-03-24 |
| TW202217014A (zh) | 2022-05-01 |
| SA523442925B1 (ar) | 2024-02-01 |
| CN116133765B (zh) | 2025-04-15 |
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