TWI275790B - Analysis method - Google Patents

Analysis method Download PDF

Info

Publication number
TWI275790B
TWI275790B TW093111195A TW93111195A TWI275790B TW I275790 B TWI275790 B TW I275790B TW 093111195 A TW093111195 A TW 093111195A TW 93111195 A TW93111195 A TW 93111195A TW I275790 B TWI275790 B TW I275790B
Authority
TW
Taiwan
Prior art keywords
bath
working electrode
range
metal
electrode
Prior art date
Application number
TW093111195A
Other languages
English (en)
Chinese (zh)
Other versions
TW200508605A (en
Inventor
Wade Sonnenberg
Leon R Barstad
Raymond Cruz
Gary Hamm
Mark J Kapeckas
Original Assignee
Rohm & Haas Elect Mat
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rohm & Haas Elect Mat filed Critical Rohm & Haas Elect Mat
Publication of TW200508605A publication Critical patent/TW200508605A/zh
Application granted granted Critical
Publication of TWI275790B publication Critical patent/TWI275790B/zh

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D21/00Processes for servicing or operating cells for electrolytic coating
    • C25D21/12Process control or regulation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23GTHREAD CUTTING; WORKING OF SCREWS, BOLT HEADS, OR NUTS, IN CONJUNCTION THEREWITH
    • B23G1/00Thread cutting; Automatic machines specially designed therefor
    • B23G1/02Thread cutting; Automatic machines specially designed therefor on an external or internal cylindrical or conical surface, e.g. on recesses
    • B23G1/04Machines with one working-spindle
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23GTHREAD CUTTING; WORKING OF SCREWS, BOLT HEADS, OR NUTS, IN CONJUNCTION THEREWITH
    • B23G1/00Thread cutting; Automatic machines specially designed therefor
    • B23G1/44Equipment or accessories specially designed for machines or devices for thread cutting
    • B23G1/50Equipment or accessories specially designed for machines or devices for thread cutting for cutting thread by successive operations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23GTHREAD CUTTING; WORKING OF SCREWS, BOLT HEADS, OR NUTS, IN CONJUNCTION THEREWITH
    • B23G5/00Thread-cutting tools; Die-heads
    • B23G5/08Thread-cutting tools; Die-heads with means for adjustment
    • B23G5/083Adjustable dies
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/26Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
    • G01N27/416Systems
    • G01N27/42Measuring deposition or liberation of materials from an electrolyte; Coulometry, i.e. measuring coulomb-equivalent of material in an electrolyte
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/26Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
    • G01N27/416Systems
    • G01N27/42Measuring deposition or liberation of materials from an electrolyte; Coulometry, i.e. measuring coulomb-equivalent of material in an electrolyte
    • G01N27/423Coulometry
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23GTHREAD CUTTING; WORKING OF SCREWS, BOLT HEADS, OR NUTS, IN CONJUNCTION THEREWITH
    • B23G2210/00Details of threads produced
    • B23G2210/08External threads

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Biochemistry (AREA)
  • Pathology (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Molecular Biology (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Mechanical Engineering (AREA)
  • Automation & Control Theory (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Electroplating Methods And Accessories (AREA)
  • Electroplating And Plating Baths Therefor (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
TW093111195A 2003-04-25 2004-04-22 Analysis method TWI275790B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US46538803P 2003-04-25 2003-04-25

Publications (2)

Publication Number Publication Date
TW200508605A TW200508605A (en) 2005-03-01
TWI275790B true TWI275790B (en) 2007-03-11

Family

ID=32962779

Family Applications (1)

Application Number Title Priority Date Filing Date
TW093111195A TWI275790B (en) 2003-04-25 2004-04-22 Analysis method

Country Status (6)

Country Link
US (1) US20060151327A1 (enExample)
EP (1) EP1471348A1 (enExample)
JP (1) JP2004325441A (enExample)
KR (1) KR20040092432A (enExample)
CN (1) CN1550578A (enExample)
TW (1) TWI275790B (enExample)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004323971A (ja) * 2003-04-25 2004-11-18 Rohm & Haas Electronic Materials Llc 改良された浴分析
KR100649725B1 (ko) * 2005-08-31 2006-11-27 엘지전자 주식회사 플라즈마 디스플레이 패널의 에너지 회수장치 및 회수방법
CN101470097B (zh) * 2007-12-25 2013-05-29 比亚迪股份有限公司 一种电镀液中有机添加剂浓度的测定方法
CN102272356A (zh) * 2008-11-07 2011-12-07 克斯塔里克公司 电沉积液、系统及方法
WO2011038463A1 (en) * 2009-10-02 2011-04-07 Newcastle Innovation Limited Supercapacitor electrodes
JP5888152B2 (ja) * 2012-07-05 2016-03-16 住友金属鉱山株式会社 パラジウムめっき液の劣化状態評価方法、パラジウムめっき方法
US9783908B2 (en) 2012-10-23 2017-10-10 Moses Lake Industries, Inc. Plating bath metrology
JP6426336B2 (ja) * 2013-10-25 2018-11-21 理研計器株式会社 定電位電解式ガスセンサ
CN103698384B (zh) * 2013-12-17 2016-02-10 上海交通大学 深孔镀铜加速剂的测量方法
EP2937686B1 (en) * 2014-04-22 2017-03-08 Rohm and Haas Electronic Materials LLC Electroplating bath analysis
KR101711293B1 (ko) * 2015-08-06 2017-03-03 서울대학교산학협력단 도금용액에 포함된 가속제 농도의 측정방법
CA3092515A1 (en) * 2018-03-23 2019-09-26 Mara Nanotech Korea, Inc. Methods of manufacturing biosensor nanowells
KR102101941B1 (ko) 2018-03-23 2020-05-29 주식회사 마라나노텍코리아 바이오 센서 제조방법
CN110872724A (zh) * 2018-09-03 2020-03-10 东莞市脉拓表面处理科技有限公司 调配电镀药水的方法及装置
CN114005759A (zh) * 2021-10-29 2022-02-01 华天科技(宝鸡)有限公司 一种引线框架及其制备方法

Family Cites Families (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4038161A (en) * 1976-03-05 1977-07-26 R. O. Hull & Company, Inc. Acid copper plating and additive composition therefor
US4132605A (en) * 1976-12-27 1979-01-02 Rockwell International Corporation Method for evaluating the quality of electroplating baths
US4666567A (en) * 1981-07-31 1987-05-19 The Boeing Company Automated alternating polarity pulse electrolytic processing of electrically conductive substances
US4479852A (en) * 1983-01-21 1984-10-30 International Business Machines Corporation Method for determination of concentration of organic additive in plating bath
US4631116A (en) * 1985-06-05 1986-12-23 Hughes Aircraft Company Method of monitoring trace constituents in plating baths
US4917774A (en) * 1986-04-24 1990-04-17 Shipley Company Inc. Method for analyzing additive concentration
US4917777A (en) * 1986-04-24 1990-04-17 Shipley Company Inc. Method for analyzing additive concentration
US4812210A (en) * 1987-10-16 1989-03-14 The United States Department Of Energy Measuring surfactant concentration in plating solutions
US5004525A (en) * 1988-08-23 1991-04-02 Shipley Company Inc. Copper electroplating composition
US5049246A (en) * 1989-06-20 1991-09-17 Hull Harry F Electrolytic processing apparatus and method with time multiplexed power supply
US5223118A (en) * 1991-03-08 1993-06-29 Shipley Company Inc. Method for analyzing organic additives in an electroplating bath
US5192403A (en) * 1991-05-16 1993-03-09 International Business Machines Corporation Cyclic voltammetric method for the measurement of concentrations of subcomponents of plating solution additive mixtures
US5252196A (en) * 1991-12-05 1993-10-12 Shipley Company Inc. Copper electroplating solutions and processes
US5298132A (en) * 1993-03-25 1994-03-29 Hughes Aircraft Company Method for monitoring purification treatment in plating baths
US5972192A (en) * 1997-07-23 1999-10-26 Advanced Micro Devices, Inc. Pulse electroplating copper or copper alloys
US6365033B1 (en) * 1999-05-03 2002-04-02 Semitoof, Inc. Methods for controlling and/or measuring additive concentration in an electroplating bath
US6471845B1 (en) * 1998-12-15 2002-10-29 International Business Machines Corporation Method of controlling chemical bath composition in a manufacturing environment
JP2001152398A (ja) * 1999-08-05 2001-06-05 Fujitsu Ltd 電気めっき方法、めっき液評価方法、めっき装置、半導体装置の製造方法
US6280602B1 (en) * 1999-10-20 2001-08-28 Advanced Technology Materials, Inc. Method and apparatus for determination of additives in metal plating baths
US6508924B1 (en) * 2000-05-31 2003-01-21 Shipley Company L.L.C. Control of breakdown products in electroplating baths
US6645364B2 (en) * 2000-10-20 2003-11-11 Shipley Company, L.L.C. Electroplating bath control
DE60113214T2 (de) * 2000-11-02 2006-06-08 Shipley Co., L.L.C., Marlborough Plattierungsbadanalyse
US20020125142A1 (en) * 2001-01-18 2002-09-12 Zhi-Wen Sun Plating bath organic additive analyzer
US6572753B2 (en) * 2001-10-01 2003-06-03 Eci Technology, Inc. Method for analysis of three organic additives in an acid copper plating bath
US20030201191A1 (en) * 2002-04-29 2003-10-30 Applied Materials, Inc. Electrochemical method for direct organic additives analysis in copper baths
US6773569B2 (en) * 2002-05-08 2004-08-10 Applied Materials Inc. Potential pulse-scan methods of analyzing organic additives in plating baths with multi-component additives
US6808611B2 (en) * 2002-06-27 2004-10-26 Applied Materials, Inc. Methods in electroanalytical techniques to analyze organic components in plating baths
US6749739B2 (en) * 2002-10-07 2004-06-15 Eci Technology, Inc. Detection of suppressor breakdown contaminants in a plating bath
US6709561B1 (en) * 2002-11-06 2004-03-23 Eci Technology, Inc. Measurement of the concentration of a reducing agent in an electroless plating bath
US6673226B1 (en) * 2002-12-20 2004-01-06 Eci Technology Voltammetric measurement of halide ion concentration

Also Published As

Publication number Publication date
US20060151327A1 (en) 2006-07-13
TW200508605A (en) 2005-03-01
EP1471348A1 (en) 2004-10-27
CN1550578A (zh) 2004-12-01
JP2004325441A (ja) 2004-11-18
KR20040092432A (ko) 2004-11-03

Similar Documents

Publication Publication Date Title
JP4041667B2 (ja) めっき浴分析方法
TWI275790B (en) Analysis method
US4479852A (en) Method for determination of concentration of organic additive in plating bath
US5223118A (en) Method for analyzing organic additives in an electroplating bath
JPS6019455B2 (ja) 有機レベリング剤の有効量を決定する方法
JP5335096B2 (ja) 無電解金属または金属合金めっき電解質中の安定化添加剤の濃度測定方法およびその制御方法
JPWO2004085715A1 (ja) 電気銅めっき液の分析方法、その分析装置及び半導体製品の製造方法
US6508924B1 (en) Control of breakdown products in electroplating baths
US7384535B2 (en) Bath analysis
US7427344B2 (en) Methods for determining organic component concentrations in an electrolytic solution
EP3384066B1 (en) Method for monitoring the total amount of sulphur containing compounds in a metal plating bath
JP6409291B2 (ja) 電気銅めっき液分析装置、及び電気銅めっき液分析方法
JP4191303B2 (ja) 複数金属微量濃度の同時迅速測定法
Robertson et al. An introductory electrochemical approach to studying hydrometallurgical reactions
US20050224370A1 (en) Electrochemical deposition analysis system including high-stability electrode
JP6011874B2 (ja) めっき液に含まれる抑制剤の評価方法
JP2005290413A (ja) 電気銅めっき液の分析方法及び分析装置
CN109072468A (zh) 监测增亮剂在酸性铜/铜合金电镀浴中的总量的方法和受控的电镀过程
JP2005226085A (ja) 電気銅めっき液の分析方法及びその分析装置
Ning et al. Research on the effect of inorganic components on brightener in horizontal pulse plating solution by Cyclic Voltammetric Stripping method
CN119352116A (zh) 一种电镀铜氧化还原型添加剂的定量方法

Legal Events

Date Code Title Description
MM4A Annulment or lapse of patent due to non-payment of fees