TW200630376A - Process for preparing acylphosphanes and derivatives thereof - Google Patents
Process for preparing acylphosphanes and derivatives thereofInfo
- Publication number
- TW200630376A TW200630376A TW094140925A TW94140925A TW200630376A TW 200630376 A TW200630376 A TW 200630376A TW 094140925 A TW094140925 A TW 094140925A TW 94140925 A TW94140925 A TW 94140925A TW 200630376 A TW200630376 A TW 200630376A
- Authority
- TW
- Taiwan
- Prior art keywords
- formula
- metal
- optionally
- c18alkenyl
- c18alkyl
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 229910052751 metal Inorganic materials 0.000 abstract 4
- 239000002184 metal Substances 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 2
- 239000012190 activator Substances 0.000 abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 2
- 150000001340 alkali metals Chemical class 0.000 abstract 2
- 150000001733 carboxylic acid esters Chemical class 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- 150000004820 halides Chemical class 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 2
- UQRONKZLYKUEMO-UHFFFAOYSA-N 4-methyl-1-(2,4,6-trimethylphenyl)pent-4-en-2-one Chemical group CC(=C)CC(=O)Cc1c(C)cc(C)cc1C UQRONKZLYKUEMO-UHFFFAOYSA-N 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 238000005917 acylation reaction Methods 0.000 abstract 1
- 238000005804 alkylation reaction Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 abstract 1
- SAWKFRBJGLMMES-UHFFFAOYSA-N methylphosphine Chemical compound PC SAWKFRBJGLMMES-UHFFFAOYSA-N 0.000 abstract 1
- 125000001624 naphthyl group Chemical group 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 150000003568 thioethers Chemical class 0.000 abstract 1
- YWWDBCBWQNCYNR-UHFFFAOYSA-N trimethylphosphine Chemical compound CP(C)C YWWDBCBWQNCYNR-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
- G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
- G03F7/004—Photosensitive materials
- G03F7/027—Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds
- G03F7/028—Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds with photosensitivity-increasing substances, e.g. photoinitiators
- G03F7/029—Inorganic compounds; Onium compounds; Organic compounds having hetero atoms other than oxygen, nitrogen or sulfur
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/5036—Phosphines containing the structure -C(=X)-P or NC-P
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
- C07F9/5337—Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
- C07F9/5537—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom the heteroring containing the structure -C(=O)-N-C(=O)- (both carbon atoms belong to the heteroring)
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/655—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms
- C07F9/65515—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms the oxygen atom being part of a five-membered ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/655—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms
- C07F9/6552—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms the oxygen atom being part of a six-membered ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Molecular Biology (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- General Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Polymerisation Methods In General (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP04105987 | 2004-11-23 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TW200630376A true TW200630376A (en) | 2006-09-01 |
Family
ID=34929912
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW094140925A TW200630376A (en) | 2004-11-23 | 2005-11-22 | Process for preparing acylphosphanes and derivatives thereof |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US7687657B2 (zh) |
| EP (1) | EP1814891B1 (zh) |
| JP (1) | JP5148283B2 (zh) |
| KR (1) | KR101230940B1 (zh) |
| CN (1) | CN101065388B (zh) |
| AT (1) | ATE496928T1 (zh) |
| DE (1) | DE602005026156D1 (zh) |
| TW (1) | TW200630376A (zh) |
| WO (1) | WO2006056541A1 (zh) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI635361B (zh) * | 2013-07-08 | 2018-09-11 | 德商巴地斯顏料化工廠 | 液態雙醯基氧化膦光引發劑 |
| TWI675040B (zh) * | 2017-05-30 | 2019-10-21 | 荷蘭商Ｉｇｍ集團 | 藉由不具反應性金屬磷化物的活化來合成雙(醯基)膦 |
Families Citing this family (34)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7470819B2 (en) | 2005-01-17 | 2008-12-30 | Ciba Specialty Chemicals Corporation | Process for preparing acylphosphanes and their oxides and sulphides |
| EP2199273B1 (en) | 2008-12-18 | 2018-02-21 | Agfa Nv | Polymerizable photoinitiators and radiation curable compositions |
| CN102405239B (zh) * | 2009-04-20 | 2014-10-15 | 瑞士联邦苏黎世技术大学 | 聚合物纳米颗粒 |
| US8883873B2 (en) | 2009-05-18 | 2014-11-11 | Agfa Graphics Nv | Polymerizable polymeric photoinitiators and radiation curable compositions |
| JP5832430B2 (ja) * | 2009-07-06 | 2015-12-16 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | ポリマーに固定されたビスアシルホスフィンオキシド |
| DK2588549T3 (en) | 2010-06-30 | 2015-01-12 | Dsm Ip Assets Bv | D1479-STABLE LIQUID BAP photoinitiator AND ITS USE IN radiation-FORMATIONS |
| US8633258B2 (en) | 2010-06-30 | 2014-01-21 | Dsm Ip Assets B.V. | D1492 liquid BAPO photoinitiator and its use in radiation curable compositions |
| WO2012052148A1 (en) | 2010-10-19 | 2012-04-26 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Ultra fast process for the preparation of polymer nanoparticles |
| WO2012052147A1 (en) | 2010-10-19 | 2012-04-26 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Process for the modification of polymers, in particular polymer nanoparticles |
| CN102924509A (zh) * | 2011-08-09 | 2013-02-13 | 陈婷 | 双膦酰膦酸酯化合物 |
| CN103073658A (zh) * | 2011-10-26 | 2013-05-01 | 深圳市有为化学技术有限公司 | 新型芳香羟基酮和膦酰氧化物的光引发剂混合物及其与光吸收剂的复合体系 |
| CN103130831A (zh) * | 2011-12-01 | 2013-06-05 | 深圳市有为化学技术有限公司 | 巯基取代的酰基膦氧化合物及含有该化合物的光引发剂 |
| EP2902456B1 (en) * | 2012-09-27 | 2020-10-21 | FUJIFILM Corporation | Ink composition, ink jet recording method, printed material, bisacyl phosphine oxide compound, and monoacyl phosphine oxide compound |
| ES2720760T3 (es) * | 2012-10-01 | 2019-07-24 | Eth Zuerich | Un procedimiento para la preparación de acilofosfanos |
| KR101798739B1 (ko) | 2012-12-18 | 2017-11-16 | 바스프 에스이 | 나프탈렌디이미드-비닐렌-올리고티오펜-비닐렌 중합체를 기재로 하는 반도체 물질 |
| WO2014095724A1 (en) * | 2012-12-19 | 2014-06-26 | Basf Se | Derivatives of bisacylphosphinic acid, their preparation and use as photoinitiators |
| JP6599446B2 (ja) | 2014-05-30 | 2019-10-30 | アイジーエム レシンス イタリア ソチエタ レスポンサビリタ リミタータ | 多官能性アシルホスフィンオキシド光重合開始剤 |
| CN105884824A (zh) * | 2014-10-16 | 2016-08-24 | 郑成 | 酰基膦(氧)或磺酰膦(氧)类化合物的制备方法 |
| EP3031798B1 (en) * | 2014-12-10 | 2017-09-27 | Belenos Clean Power Holding AG | A novel cross-linker for the preparation of a new family of single ion conduction polymers for electrochemical devices and such polymers |
| CN104592298B (zh) * | 2014-12-31 | 2016-07-06 | 湖北固润科技股份有限公司 | 一种酰基膦高效光引发剂及其制备方法 |
| CN104910207B (zh) * | 2015-02-12 | 2019-03-05 | 天津墨森科技有限公司 | 双苯甲酰基苯基氧化膦和苯甲酰基二苯基氧化膦的制备方法 |
| EP3296301A1 (en) | 2016-09-19 | 2018-03-21 | ETH Zürich | A versatile process for the preparation of acylphosphines |
| CA3043849A1 (en) | 2016-11-16 | 2018-05-24 | Ecole Polytechnique Federale De Lausanne (Epfl) | Photopolymerizable bone filler material |
| WO2018186822A1 (en) | 2017-04-03 | 2018-10-11 | Hewlett-Packard Development Company, L.P. | Photo active agents |
| CN107400144B (zh) * | 2017-08-03 | 2020-04-14 | 深圳有为技术控股集团有限公司 | 酰基膦(氧)化合物及其制备方法和应用 |
| EP3665232A4 (en) | 2017-08-10 | 2021-04-07 | Sun Chemical Corporation | UV CURABLE COMPOSITIONS CONTAINING ACYLPHOSPHINE OXIDE PHOTOINITIATORS |
| EP3539924A1 (en) | 2018-03-14 | 2019-09-18 | ETH Zurich | Novel vinyl phosphines and photo-initiators obtainable therefrom |
| EP3788083A1 (en) | 2018-04-30 | 2021-03-10 | Basf Se | High molar mass polymers from a continuous process |
| CN112334551B (zh) | 2018-06-19 | 2022-11-08 | 爱克发有限公司 | 酰基氧化膦引发剂 |
| KR20210055724A (ko) | 2018-09-07 | 2021-05-17 | 아이지엠 레진스 이탈리아 에스.알.엘. | 다관능성 비스아실포스핀 옥사이드 광개시제 |
| EP4114339A1 (en) | 2020-05-29 | 2023-01-11 | Lumendo AG | Crosslinkable prepolymers for chemically stable polymer gels |
| US20220380549A1 (en) | 2021-05-12 | 2022-12-01 | Elkem Silicones USA Corp. | Method for producing a three-dimensional printed article |
| US11964425B2 (en) | 2021-05-12 | 2024-04-23 | Elkem Silicones USA Corp. | Method for producing a three-dimensional printed article |
| CN115612112B (zh) * | 2021-07-16 | 2023-11-10 | 常州强力先端电子材料有限公司 | 有机磷类大分子类引发剂及其制备方法、光固化组合物 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3397039A (en) * | 1967-05-17 | 1968-08-13 | Procter & Gamble | Preparation of alkali metal phosphides |
| JPS4741114Y1 (zh) * | 1968-02-14 | 1972-12-12 | ||
| DE2007535C3 (de) * | 1970-02-19 | 1974-12-12 | Basf Ag, 6700 Ludsigshafen | Verfahren zur Herstellung von Triarylphosphinen |
| US3668093A (en) * | 1971-05-06 | 1972-06-06 | Du Pont | Photoinitiation of vinyl polymerization by triaroylphosphines |
| DE3020092A1 (de) | 1980-05-27 | 1981-12-10 | Basf Ag, 6700 Ludwigshafen | Acylphosphinverbindungen und ihre verwendung |
| DE3443221A1 (de) * | 1984-11-27 | 1986-06-05 | ESPE Fabrik pharmazeutischer Präparate GmbH, 8031 Seefeld | Bisacylphosphinoxide, ihre herstellung und verwendung |
| US5218009A (en) * | 1989-08-04 | 1993-06-08 | Ciba-Geigy Corporation | Mono- and di-acylphosphine oxides |
| EP0495751A1 (de) * | 1991-01-14 | 1992-07-22 | Ciba-Geigy Ag | Bisacylphosphine |
| CN1211388C (zh) | 1998-11-30 | 2005-07-20 | 西巴特殊化学品控股有限公司 | 酰基膦和其衍生物的制备方法 |
| GB2360283B (en) * | 2000-02-08 | 2002-08-21 | Ciba Sc Holding Ag | Monoacylarylphosphines and acylphosphine oxides and sulphides |
| GB2365430B (en) * | 2000-06-08 | 2002-08-28 | Ciba Sc Holding Ag | Acylphosphine photoinitiators and intermediates |
| EP1423757B1 (en) * | 2001-08-21 | 2009-04-29 | Ciba Holding Inc. | Bathochromic mono- and bis-acylphosphine oxides and sulfides and their use as photoinitiators |
| WO2003044030A1 (en) * | 2001-11-20 | 2003-05-30 | Ciba Specialty Chemicals Holding Inc. | Multimer forms of acylphosphines and their derivatives |
| DE60328219D1 (de) * | 2002-12-04 | 2009-08-13 | Ciba Holding Inc | Verfahren zur synthese von cycloorganylphosphanen und von di(alkali/erdalkalimetall)oligophosphandiiden |
| JP4949025B2 (ja) * | 2003-07-18 | 2012-06-06 | チバ ホールディング インコーポレーテッド | アシルホスファンおよびそれらの誘導体の製造方法 |
| TW200523265A (en) * | 2003-07-31 | 2005-07-16 | Basf Ag | A process for the preparation of acylphosphines |
| EP1675814A1 (en) | 2003-10-14 | 2006-07-05 | Eli Lilly And Company | Phenoxyether derivatives as ppar modulators |
-
2005
- 2005-11-14 AT AT05817544T patent/ATE496928T1/de not_active IP Right Cessation
- 2005-11-14 EP EP05817544A patent/EP1814891B1/en active Active
- 2005-11-14 US US11/667,780 patent/US7687657B2/en active Active
- 2005-11-14 WO PCT/EP2005/055935 patent/WO2006056541A1/en active Application Filing
- 2005-11-14 DE DE602005026156T patent/DE602005026156D1/de active Active
- 2005-11-14 KR KR1020077014374A patent/KR101230940B1/ko active IP Right Grant
- 2005-11-14 JP JP2007541935A patent/JP5148283B2/ja active Active
- 2005-11-14 CN CN2005800401612A patent/CN101065388B/zh active Active
- 2005-11-22 TW TW094140925A patent/TW200630376A/zh unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI635361B (zh) * | 2013-07-08 | 2018-09-11 | 德商巴地斯顏料化工廠 | 液態雙醯基氧化膦光引發劑 |
| TWI675040B (zh) * | 2017-05-30 | 2019-10-21 | 荷蘭商Ｉｇｍ集團 | 藉由不具反應性金屬磷化物的活化來合成雙(醯基)膦 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP1814891B1 (en) | 2011-01-26 |
| CN101065388B (zh) | 2011-12-21 |
| KR101230940B1 (ko) | 2013-02-08 |
| JP5148283B2 (ja) | 2013-02-20 |
| US20080004464A1 (en) | 2008-01-03 |
| KR20070086609A (ko) | 2007-08-27 |
| EP1814891A1 (en) | 2007-08-08 |
| US7687657B2 (en) | 2010-03-30 |
| JP2008520623A (ja) | 2008-06-19 |
| DE602005026156D1 (de) | 2011-03-10 |
| WO2006056541A1 (en) | 2006-06-01 |
| CN101065388A (zh) | 2007-10-31 |
| ATE496928T1 (de) | 2011-02-15 |
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