ATE496928T1 - Bisacylphosphane und ihre verwendung als photoinitiatoren, verfahren zur herstellung von acylphosphanen - Google Patents
Bisacylphosphane und ihre verwendung als photoinitiatoren, verfahren zur herstellung von acylphosphanenInfo
- Publication number
- ATE496928T1 ATE496928T1 AT05817544T AT05817544T ATE496928T1 AT E496928 T1 ATE496928 T1 AT E496928T1 AT 05817544 T AT05817544 T AT 05817544T AT 05817544 T AT05817544 T AT 05817544T AT E496928 T1 ATE496928 T1 AT E496928T1
- Authority
- AT
- Austria
- Prior art keywords
- formula
- metal
- optionally
- c18alkenyl
- c18alkyl
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 3
- 229910052751 metal Inorganic materials 0.000 abstract 4
- 239000002184 metal Substances 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 2
- 239000012190 activator Substances 0.000 abstract 2
- 229910052783 alkali metal Inorganic materials 0.000 abstract 2
- 150000001340 alkali metals Chemical class 0.000 abstract 2
- 150000001733 carboxylic acid esters Chemical class 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- 150000004820 halides Chemical class 0.000 abstract 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 2
- UQRONKZLYKUEMO-UHFFFAOYSA-N 4-methyl-1-(2,4,6-trimethylphenyl)pent-4-en-2-one Chemical group CC(=C)CC(=O)Cc1c(C)cc(C)cc1C UQRONKZLYKUEMO-UHFFFAOYSA-N 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 238000005917 acylation reaction Methods 0.000 abstract 1
- 238000005804 alkylation reaction Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 abstract 1
- SAWKFRBJGLMMES-UHFFFAOYSA-N methylphosphine Chemical compound PC SAWKFRBJGLMMES-UHFFFAOYSA-N 0.000 abstract 1
- 125000001624 naphthyl group Chemical group 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 150000003568 thioethers Chemical class 0.000 abstract 1
- YWWDBCBWQNCYNR-UHFFFAOYSA-N trimethylphosphine Chemical compound CP(C)C YWWDBCBWQNCYNR-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03F—PHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
- G03F7/00—Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
- G03F7/004—Photosensitive materials
- G03F7/027—Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds
- G03F7/028—Non-macromolecular photopolymerisable compounds having carbon-to-carbon double bonds, e.g. ethylenic compounds with photosensitivity-increasing substances, e.g. photoinitiators
- G03F7/029—Inorganic compounds; Onium compounds; Organic compounds having hetero atoms other than oxygen, nitrogen or sulfur
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/5036—Phosphines containing the structure -C(=X)-P or NC-P
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/50—Organo-phosphines
- C07F9/53—Organo-phosphine oxides; Organo-phosphine thioxides
- C07F9/5337—Phosphine oxides or thioxides containing the structure -C(=X)-P(=X) or NC-P(=X) (X = O, S, Se)
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
- C07F9/5537—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom the heteroring containing the structure -C(=O)-N-C(=O)- (both carbon atoms belong to the heteroring)
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/655—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms
- C07F9/65515—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms the oxygen atom being part of a five-membered ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/655—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms
- C07F9/6552—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having oxygen atoms, with or without sulfur, selenium, or tellurium atoms, as the only ring hetero atoms the oxygen atom being part of a six-membered ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Molecular Biology (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- General Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polymerisation Methods In General (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP04105987 | 2004-11-23 | ||
| PCT/EP2005/055935 WO2006056541A1 (en) | 2004-11-23 | 2005-11-14 | Process for preparing acylphosphanes and derivatives thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE496928T1 true ATE496928T1 (de) | 2011-02-15 |
Family
ID=34929912
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT05817544T ATE496928T1 (de) | 2004-11-23 | 2005-11-14 | Bisacylphosphane und ihre verwendung als photoinitiatoren, verfahren zur herstellung von acylphosphanen |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US7687657B2 (de) |
| EP (1) | EP1814891B1 (de) |
| JP (1) | JP5148283B2 (de) |
| KR (1) | KR101230940B1 (de) |
| CN (1) | CN101065388B (de) |
| AT (1) | ATE496928T1 (de) |
| DE (1) | DE602005026156D1 (de) |
| TW (1) | TW200630376A (de) |
| WO (1) | WO2006056541A1 (de) |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ATE538126T1 (de) | 2005-01-17 | 2012-01-15 | Basf Se | Verfahren zur herstellung von acylphosphan und deren oxide und sulfide |
| EP2199273B1 (de) | 2008-12-18 | 2018-02-21 | Agfa Nv | Polymerisierbare Fotoinitiatoren und strahlungshärtbare Zusammensetzungen |
| EP2421903B1 (de) | 2009-04-20 | 2014-11-19 | ETH Zurich | Polymernanopartikel |
| US8883873B2 (en) | 2009-05-18 | 2014-11-11 | Agfa Graphics Nv | Polymerizable polymeric photoinitiators and radiation curable compositions |
| EP2451847B1 (de) * | 2009-07-06 | 2021-11-24 | IGM Group B.V. | Polymergebundene bisacylphosphinoxide |
| WO2012003106A1 (en) | 2010-06-30 | 2012-01-05 | Dsm Ip Assets B.V. | D1479 stable liquid bap photoinitiator and its use in radiation curable compositions |
| EP2558427B1 (de) * | 2010-06-30 | 2017-05-31 | DSM IP Assets B.V. | Flüssiger d1492 bapo-fotoinitiator und seine verwendung bei strahlungshärtbaren zusammensetzungen |
| WO2012052148A1 (en) | 2010-10-19 | 2012-04-26 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Ultra fast process for the preparation of polymer nanoparticles |
| US8921444B2 (en) | 2010-10-19 | 2014-12-30 | Max-Planck-Gesellschaft Zur Foerderung Der Wissenschaften E.V. | Process for the modification of polymers, in particular polymer nanoparticles |
| CN102924509A (zh) * | 2011-08-09 | 2013-02-13 | 陈婷 | 双膦酰膦酸酯化合物 |
| CN103073658A (zh) * | 2011-10-26 | 2013-05-01 | 深圳市有为化学技术有限公司 | 新型芳香羟基酮和膦酰氧化物的光引发剂混合物及其与光吸收剂的复合体系 |
| CN103130831A (zh) * | 2011-12-01 | 2013-06-05 | 深圳市有为化学技术有限公司 | 巯基取代的酰基膦氧化合物及含有该化合物的光引发剂 |
| WO2014051026A1 (ja) * | 2012-09-27 | 2014-04-03 | 富士フイルム株式会社 | インク組成物、インクジェット記録方法、印刷物、ビスアシルホスフィンオキシド化合物、及び、モノアシルホスフィンオキシド化合物 |
| RU2719592C2 (ru) * | 2012-10-01 | 2020-04-21 | Этх Цюрих | Способ получения ацилфосфатов |
| CN105051087A (zh) | 2012-12-18 | 2015-11-11 | 巴斯夫欧洲公司 | 基于萘二酰亚胺-亚乙烯基-低聚噻吩-亚乙烯基聚合物的半导体材料 |
| EP2935289B1 (de) * | 2012-12-19 | 2019-06-26 | IGM Group B.V. | Derivate von bisacylphosphinsäure, ihre herstellung und verwendung als photoinitiatoren |
| CN111116777A (zh) * | 2013-07-08 | 2020-05-08 | Igm集团公司 | 液态双酰基氧化膦光引发剂 |
| JP6599446B2 (ja) * | 2014-05-30 | 2019-10-30 | アイジーエム レシンス イタリア ソチエタ レスポンサビリタ リミタータ | 多官能性アシルホスフィンオキシド光重合開始剤 |
| CN105884824A (zh) * | 2014-10-16 | 2016-08-24 | 郑成 | 酰基膦(氧)或磺酰膦(氧)类化合物的制备方法 |
| EP3031798B1 (de) | 2014-12-10 | 2017-09-27 | Belenos Clean Power Holding AG | Neuartiger Vernetzer zur Herstellung einer neuen Familie einzelner Ionenleitungspolymere für elektrochemische Vorrichtungen und diese Polymere |
| CN104592298B (zh) * | 2014-12-31 | 2016-07-06 | 湖北固润科技股份有限公司 | 一种酰基膦高效光引发剂及其制备方法 |
| CN104910207B (zh) * | 2015-02-12 | 2019-03-05 | 天津墨森科技有限公司 | 双苯甲酰基苯基氧化膦和苯甲酰基二苯基氧化膦的制备方法 |
| EP3296301A1 (de) | 2016-09-19 | 2018-03-21 | ETH Zürich | Vielseitiges verfahren zur herstellung von acylphosphinen |
| US20190275201A1 (en) | 2016-11-16 | 2019-09-12 | Ecole Polytechnique Federale De Lausanne (Epfl) | Photopolymerizable bone filler material |
| WO2018186822A1 (en) | 2017-04-03 | 2018-10-11 | Hewlett-Packard Development Company, L.P. | Photo active agents |
| EP3409680B1 (de) * | 2017-05-30 | 2021-01-06 | IGM Group B.V. | Synthese von bis(acyl)phosphinen durch aktivierung von nicht-reaktiven metallphosphiden |
| CN107400144B (zh) * | 2017-08-03 | 2020-04-14 | 深圳有为技术控股集团有限公司 | 酰基膦(氧)化合物及其制备方法和应用 |
| US11267977B2 (en) | 2017-08-10 | 2022-03-08 | Sun Chemical Corporation | UV-curable compositions comprising acylphosphine oxide photoinitiators |
| EP3539924A1 (de) | 2018-03-14 | 2019-09-18 | ETH Zurich | Neuartige vinylphosphine und daraus erhältliche photoinitiatoren |
| CN112469739A (zh) | 2018-04-30 | 2021-03-09 | 巴斯夫欧洲公司 | 来自连续法的高分子量聚合物 |
| EP4036178A1 (de) | 2018-06-19 | 2022-08-03 | Agfa Nv | Uv-härtbare zusammensetzungen und tintenstrahldruckverfahren |
| WO2020049378A1 (en) | 2018-09-07 | 2020-03-12 | Igm Resins Italia S.R.L. | Multifunctional bisacylphosphine oxide photoinitiators |
| US20230167209A1 (en) | 2020-05-29 | 2023-06-01 | Lumendo Ag | Crosslinkable prepolymers for chemically stable polymer gels |
| US11964425B2 (en) | 2021-05-12 | 2024-04-23 | Elkem Silicones USA Corp. | Method for producing a three-dimensional printed article |
| US20220380549A1 (en) | 2021-05-12 | 2022-12-01 | Elkem Silicones USA Corp. | Method for producing a three-dimensional printed article |
| CN115612112B (zh) * | 2021-07-16 | 2023-11-10 | 常州强力先端电子材料有限公司 | 有机磷类大分子类引发剂及其制备方法、光固化组合物 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3397039A (en) * | 1967-05-17 | 1968-08-13 | Procter & Gamble | Preparation of alkali metal phosphides |
| JPS4741114Y1 (de) * | 1968-02-14 | 1972-12-12 | ||
| DE2007535C3 (de) * | 1970-02-19 | 1974-12-12 | Basf Ag, 6700 Ludsigshafen | Verfahren zur Herstellung von Triarylphosphinen |
| US3668093A (en) * | 1971-05-06 | 1972-06-06 | Du Pont | Photoinitiation of vinyl polymerization by triaroylphosphines |
| DE3020092A1 (de) * | 1980-05-27 | 1981-12-10 | Basf Ag, 6700 Ludwigshafen | Acylphosphinverbindungen und ihre verwendung |
| DE3443221A1 (de) * | 1984-11-27 | 1986-06-05 | ESPE Fabrik pharmazeutischer Präparate GmbH, 8031 Seefeld | Bisacylphosphinoxide, ihre herstellung und verwendung |
| US5218009A (en) * | 1989-08-04 | 1993-06-08 | Ciba-Geigy Corporation | Mono- and di-acylphosphine oxides |
| EP0495751A1 (de) * | 1991-01-14 | 1992-07-22 | Ciba-Geigy Ag | Bisacylphosphine |
| ES2180347T5 (es) * | 1998-11-30 | 2007-04-01 | Ciba Specialty Chemicals Holding Inc. | Procedimiento para la preparacion de acilfosfinas y derivados. |
| GB2360283B (en) * | 2000-02-08 | 2002-08-21 | Ciba Sc Holding Ag | Monoacylarylphosphines and acylphosphine oxides and sulphides |
| GB2365430B (en) * | 2000-06-08 | 2002-08-28 | Ciba Sc Holding Ag | Acylphosphine photoinitiators and intermediates |
| ATE430329T1 (de) * | 2001-08-21 | 2009-05-15 | Ciba Holding Inc | Bathochromische mono- und bis-acylphosphinoxide und sulfide und ihre verwendung als photoinitiatoren |
| JP2005509685A (ja) * | 2001-11-20 | 2005-04-14 | チバ スペシャルティ ケミカルズ ホールディング インコーポレーテッド | アシルホスフィン及びその誘導体のマルチマー形態 |
| JP4599169B2 (ja) | 2002-12-04 | 2010-12-15 | チバ ホールディング インコーポレーテッド | シクロオルガニルホスファンおよびジ（アルカリ金属／アルカリ土類金属）オリゴホスファンジイドの合成方法 |
| US7439401B2 (en) | 2003-07-18 | 2008-10-21 | Ciba Specialty Chemicals Corporation | Process for preparing acylphosphanes and derivatives thereof |
| TW200523265A (en) * | 2003-07-31 | 2005-07-16 | Basf Ag | A process for the preparation of acylphosphines |
| CA2541751A1 (en) | 2003-10-14 | 2005-04-28 | Eli Lilly And Company | Phenoxyether derivatives as ppar modulators |
-
2005
- 2005-11-14 DE DE602005026156T patent/DE602005026156D1/de active Active
- 2005-11-14 CN CN2005800401612A patent/CN101065388B/zh active Active
- 2005-11-14 EP EP05817544A patent/EP1814891B1/de active Active
- 2005-11-14 JP JP2007541935A patent/JP5148283B2/ja active Active
- 2005-11-14 KR KR1020077014374A patent/KR101230940B1/ko active IP Right Grant
- 2005-11-14 WO PCT/EP2005/055935 patent/WO2006056541A1/en active Application Filing
- 2005-11-14 AT AT05817544T patent/ATE496928T1/de not_active IP Right Cessation
- 2005-11-14 US US11/667,780 patent/US7687657B2/en active Active
- 2005-11-22 TW TW094140925A patent/TW200630376A/zh unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE602005026156D1 (de) | 2011-03-10 |
| CN101065388A (zh) | 2007-10-31 |
| EP1814891A1 (de) | 2007-08-08 |
| US20080004464A1 (en) | 2008-01-03 |
| JP5148283B2 (ja) | 2013-02-20 |
| WO2006056541A1 (en) | 2006-06-01 |
| CN101065388B (zh) | 2011-12-21 |
| KR20070086609A (ko) | 2007-08-27 |
| JP2008520623A (ja) | 2008-06-19 |
| US7687657B2 (en) | 2010-03-30 |
| EP1814891B1 (de) | 2011-01-26 |
| TW200630376A (en) | 2006-09-01 |
| KR101230940B1 (ko) | 2013-02-08 |
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