TW200603875A - Process for the separation and purification of hafnium and zirconium - Google Patents

Process for the separation and purification of hafnium and zirconium

Info

Publication number
TW200603875A
TW200603875A TW094123207A TW94123207A TW200603875A TW 200603875 A TW200603875 A TW 200603875A TW 094123207 A TW094123207 A TW 094123207A TW 94123207 A TW94123207 A TW 94123207A TW 200603875 A TW200603875 A TW 200603875A
Authority
TW
Taiwan
Prior art keywords
hfcl4
zrcl4
hafnium
mixture
enriched
Prior art date
Application number
TW094123207A
Other languages
English (en)
Inventor
Laurence Delons
Stephane Lagarde
Alain Favre-Reguillon
Stephane Pellet-Rostaing
Marc Lemaire
Ludovic Poriel
Original Assignee
Cezus Co Europ Zirconium
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cezus Co Europ Zirconium filed Critical Cezus Co Europ Zirconium
Publication of TW200603875A publication Critical patent/TW200603875A/zh

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/04—Halides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G27/00—Compounds of hafnium
    • C01G27/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G27/00—Compounds of hafnium
    • C01G27/04—Halides
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Geology (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
TW094123207A 2004-07-09 2005-07-08 Process for the separation and purification of hafnium and zirconium TW200603875A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR0407721A FR2872811B1 (fr) 2004-07-09 2004-07-09 Procede de separation et purification du hafnium et du zirconium

Publications (1)

Publication Number Publication Date
TW200603875A true TW200603875A (en) 2006-02-01

Family

ID=34946998

Family Applications (1)

Application Number Title Priority Date Filing Date
TW094123207A TW200603875A (en) 2004-07-09 2005-07-08 Process for the separation and purification of hafnium and zirconium

Country Status (10)

Country Link
US (1) US7708962B2 (zh)
EP (1) EP1773720B1 (zh)
JP (2) JP5379378B2 (zh)
KR (1) KR101214821B1 (zh)
CN (1) CN1993295A (zh)
CA (1) CA2572612C (zh)
EA (1) EA009811B1 (zh)
FR (1) FR2872811B1 (zh)
TW (1) TW200603875A (zh)
WO (1) WO2006016045A2 (zh)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2872811B1 (fr) * 2004-07-09 2006-10-06 Cie Europ Du Zirconium Cezus S Procede de separation et purification du hafnium et du zirconium
JP2010013668A (ja) * 2008-06-30 2010-01-21 Toshiba Corp 金属ジルコニウムの製造方法
WO2010131970A1 (en) * 2009-05-15 2010-11-18 Technische Universiteit Delft Process for separating hafnium and zirconium
FR2963339B1 (fr) * 2010-08-02 2012-09-14 Centre Nat Rech Scient Procede de separation des tetrachlorures de zirconium et d'hafnium de leurs melanges
KR101521016B1 (ko) 2013-06-19 2015-05-15 목포대학교산학협력단 하프늄과 지르코늄의 분리방법
CN104646659B (zh) * 2013-11-22 2017-06-20 北京有色金属研究总院 一种低氧高纯金属铪粉的制造方法
CN103725901B (zh) * 2013-12-12 2015-10-28 上海哈峰新材料科技有限公司 氧化锆/氧化铪混合物的火法分离方法
CN106048242B (zh) * 2015-10-19 2018-06-08 曹长风 用高原地带精馏火法分离锆铪的方法
CN106866142B (zh) * 2017-02-23 2019-08-27 南京云启金锐新材料有限公司 纳米级高纯二氧化锆复合粉体的生产方法
CN108998683B (zh) * 2017-06-06 2020-02-21 安徽唯安科技新材料发展有限公司 分离氧化锆与氧化铪混合物的方法
CN109019682B (zh) * 2018-08-20 2020-01-17 新特能源股份有限公司 一种氧氯化锆及其制备方法
CN112076621B (zh) * 2020-10-12 2021-04-13 宝钛华神钛业有限公司 一种锆铪冶金的固相冷凝回收装置
CN112624193B (zh) * 2020-12-31 2023-11-10 三祥新材股份有限公司 一种四氯化铪的提纯方法
CN112945692A (zh) * 2021-02-05 2021-06-11 成都理工大学 一种环境水中痕量重金属的鼓泡分离在线富集系统

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1262635A (fr) * 1960-04-19 1961-06-05 Commissariat Energie Atomique Perfectionnements apportés aux procédés pour la séparation du zirconium et de l'hafnium par échange d'ions
JPS5144119B1 (zh) * 1968-03-22 1976-11-26
JPS5025413B1 (zh) * 1969-01-11 1975-08-23
US4021531A (en) * 1973-11-14 1977-05-03 Ugine Aciers Process for the separation of zirconium and hafnium tetrachlorides from mixtures thereof
FR2250707B1 (zh) * 1973-11-14 1978-11-03 Ugine Aciers
FR2629360B1 (fr) * 1988-03-31 1991-01-11 Cezus Co Europ Zirconium Procede et dispositif d'introduction de tetrachlorure de zirconium, de tetrachlorure de hafnium et de leurs melanges dans une colonne de distillation extractive en continu et sous pression desdits chlorures
US5174971A (en) * 1990-10-10 1992-12-29 Westinghouse Electric Corp. Continuous anion exchange chromatography for the separation of zirconium isotopes
US5112493A (en) * 1990-12-10 1992-05-12 Westinghouse Electric Corp. Zirconium-hafnium production in a zero liquid discharge process
US5618502A (en) * 1995-07-17 1997-04-08 Westinghouse Electric Corporation Zirconium and hafnium separation in sulfate solutions using continuous ion exchange chromatography
WO1997004141A1 (en) * 1995-07-17 1997-02-06 Westinghouse Electric Corporation Zirconium and hafnium separation in chloride solutions using continuous ion exchange chromatography
FR2813877B1 (fr) * 2000-09-11 2002-12-06 Cezus Cie Europ Du Zirconium Procede de separation de metaux tels que le zirconium et l'hafnium
FR2823740B1 (fr) * 2001-04-18 2004-02-06 Cezus Co Europ Zirconium Procede de separation des tetrachlorures de zirconium et de hafnium
FR2872811B1 (fr) * 2004-07-09 2006-10-06 Cie Europ Du Zirconium Cezus S Procede de separation et purification du hafnium et du zirconium

Also Published As

Publication number Publication date
KR101214821B1 (ko) 2012-12-26
JP2013212984A (ja) 2013-10-17
JP5379378B2 (ja) 2013-12-25
US20080031791A1 (en) 2008-02-07
FR2872811A1 (fr) 2006-01-13
EA200700294A1 (ru) 2007-08-31
EA009811B1 (ru) 2008-04-28
CA2572612A1 (fr) 2006-02-16
FR2872811B1 (fr) 2006-10-06
JP2008506037A (ja) 2008-02-28
KR20070032317A (ko) 2007-03-21
EP1773720B1 (fr) 2015-09-02
US7708962B2 (en) 2010-05-04
CN1993295A (zh) 2007-07-04
US20090117018A9 (en) 2009-05-07
WO2006016045A2 (fr) 2006-02-16
CA2572612C (fr) 2012-09-25
EP1773720A2 (fr) 2007-04-18
WO2006016045A3 (fr) 2006-04-27
JP5685623B2 (ja) 2015-03-18

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