SU786856A3 - Способ получени эсцина - Google Patents
Способ получени эсцина Download PDFInfo
- Publication number
- SU786856A3 SU786856A3 SU762377644A SU2377644A SU786856A3 SU 786856 A3 SU786856 A3 SU 786856A3 SU 762377644 A SU762377644 A SU 762377644A SU 2377644 A SU2377644 A SU 2377644A SU 786856 A3 SU786856 A3 SU 786856A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- escin
- resulting
- seeds
- cation exchanger
- concentrated
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 7
- 150000001768 cations Chemical class 0.000 claims abstract description 6
- 229940011399 escin Drugs 0.000 claims abstract description 6
- 229930186222 escin Natural products 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 238000000605 extraction Methods 0.000 claims abstract description 4
- 235000010181 horse chestnut Nutrition 0.000 claims abstract description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- 239000000243 solution Substances 0.000 claims description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 230000000694 effects Effects 0.000 claims description 3
- 230000008719 thickening Effects 0.000 claims description 3
- 241000157282 Aesculus Species 0.000 claims description 2
- 150000001298 alcohols Chemical class 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 238000002955 isolation Methods 0.000 claims description 2
- 238000000746 purification Methods 0.000 claims description 2
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims 1
- 239000003729 cation exchange resin Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 abstract description 2
- 241000157280 Aesculus hippocastanum Species 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 abstract 1
- 230000001741 anti-phlogistic effect Effects 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 239000003814 drug Substances 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 238000005115 demineralization Methods 0.000 description 1
- 230000002328 demineralizing effect Effects 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
- C07H15/20—Carbocyclic rings
- C07H15/24—Condensed ring systems having three or more rings
- C07H15/256—Polyterpene radicals
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Medicinal Chemistry (AREA)
- Veterinary Medicine (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Pharmacology & Pharmacy (AREA)
- Rheumatology (AREA)
- Animal Behavior & Ethology (AREA)
- Pain & Pain Management (AREA)
- Public Health (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Saccharide Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Medicines Containing Plant Substances (AREA)
- Peptides Or Proteins (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2530941A DE2530941C2 (de) | 1975-07-11 | 1975-07-11 | Verfahren zur Gewinnung von kristallinem Aescin und zur Herstellung von bestimmten Aescin-Salzen sowie Triethanolammoniumaescinat und dieses Salz enthaltende Arzneimittel |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU786856A3 true SU786856A3 (ru) | 1980-12-07 |
Family
ID=5951217
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU762377644A SU786856A3 (ru) | 1975-07-11 | 1976-07-07 | Способ получени эсцина |
Country Status (21)
| Country | Link |
|---|---|
| JP (1) | JPS5234913A (enExample) |
| AR (1) | AR210498A1 (enExample) |
| AU (1) | AU510202B2 (enExample) |
| BE (1) | BE844052A (enExample) |
| BG (1) | BG27378A3 (enExample) |
| CA (1) | CA1049497A (enExample) |
| CS (1) | CS193077B2 (enExample) |
| DE (1) | DE2530941C2 (enExample) |
| ES (1) | ES449747A1 (enExample) |
| FI (1) | FI63418C (enExample) |
| FR (1) | FR2316962A1 (enExample) |
| GB (1) | GB1551387A (enExample) |
| HK (1) | HK33781A (enExample) |
| HU (1) | HU175394B (enExample) |
| PH (1) | PH13088A (enExample) |
| PL (1) | PL99027B1 (enExample) |
| PT (1) | PT65301B (enExample) |
| RO (1) | RO71026A (enExample) |
| SU (1) | SU786856A3 (enExample) |
| YU (1) | YU39215B (enExample) |
| ZA (1) | ZA764064B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2290189C1 (ru) * | 2005-06-17 | 2006-12-27 | Игорь Юрьевич Макаров | Средство, обладающее венотонизирующим, противовоспалительным и капилляропротекторным действием, и способ его получения |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE60214046T2 (de) * | 2002-03-25 | 2007-02-15 | Council Of Scientific And Industrial Research | Ein einfaches verfahren zur gewinnung von beta-aescin aus der indischen rosskastanie (aesculus indica) |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1095989B (de) * | 1959-03-11 | 1960-12-29 | Madaus & Co Dr | Verfahren zur Gewinnung eines kristallisierten sauren Saponins aus dem Samen der Rosskastanie |
| FR1267224A (fr) * | 1960-06-07 | 1961-07-21 | Madaus & Co Dr | Procédé de préparation de saponine acide cristallisée à partir de marrons d'inde |
| DE1667884B2 (de) * | 1968-01-20 | 1976-09-30 | Knoll Ag, Chemische Fabriken, 6700 Ludwigshafen | Verfahren zur gewinnung von reinem aescin |
| DE2118916A1 (en) * | 1971-04-19 | 1972-11-09 | Schwabe, Willmar, Dr., 7500 Karlsruhe-Durlach | Water-soluble acid saponin mixts prodn - by extraction of horse-chestnuts and complex formation with (alkyl)benzene |
| YU37063B (en) * | 1971-12-06 | 1984-08-31 | Lek Tovarna Farmacevtskih | Process for preparing x-ray amorphous water-sulubleascin |
-
1975
- 1975-07-11 DE DE2530941A patent/DE2530941C2/de not_active Expired - Lifetime
-
1976
- 1976-06-23 AR AR263714A patent/AR210498A1/es active
- 1976-06-30 PT PT65301A patent/PT65301B/pt unknown
- 1976-07-05 FI FI761957A patent/FI63418C/fi not_active IP Right Cessation
- 1976-07-05 BG BG033672A patent/BG27378A3/xx unknown
- 1976-07-07 SU SU762377644A patent/SU786856A3/ru active
- 1976-07-07 GB GB28232/76A patent/GB1551387A/en not_active Expired
- 1976-07-08 ZA ZA764064A patent/ZA764064B/xx unknown
- 1976-07-08 AU AU15730/76A patent/AU510202B2/en not_active Expired
- 1976-07-08 YU YU01669/76A patent/YU39215B/xx unknown
- 1976-07-09 CS CS764568A patent/CS193077B2/cs unknown
- 1976-07-09 CA CA256,649A patent/CA1049497A/en not_active Expired
- 1976-07-09 HU HU76MA2796A patent/HU175394B/hu not_active IP Right Cessation
- 1976-07-10 PL PL1976191113A patent/PL99027B1/pl unknown
- 1976-07-10 ES ES449747A patent/ES449747A1/es not_active Expired
- 1976-07-10 RO RO7686933A patent/RO71026A/ro unknown
- 1976-07-12 JP JP51082845A patent/JPS5234913A/ja active Granted
- 1976-07-12 BE BE168848A patent/BE844052A/xx not_active IP Right Cessation
- 1976-07-12 FR FR7621314A patent/FR2316962A1/fr active Granted
- 1976-07-12 PH PH18679A patent/PH13088A/en unknown
-
1981
- 1981-07-16 HK HK337/81A patent/HK33781A/xx unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2290189C1 (ru) * | 2005-06-17 | 2006-12-27 | Игорь Юрьевич Макаров | Средство, обладающее венотонизирующим, противовоспалительным и капилляропротекторным действием, и способ его получения |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2530941A1 (de) | 1977-01-27 |
| YU39215B (en) | 1984-08-31 |
| ES449747A1 (es) | 1977-08-16 |
| FI761957A7 (enExample) | 1977-01-12 |
| FR2316962B1 (enExample) | 1979-03-02 |
| AU510202B2 (en) | 1980-06-12 |
| PL99027B1 (pl) | 1978-06-30 |
| HU175394B (hu) | 1980-07-28 |
| BE844052A (fr) | 1977-01-12 |
| GB1551387A (en) | 1979-08-30 |
| PT65301B (de) | 1977-12-13 |
| PH13088A (en) | 1979-11-23 |
| JPS5234913A (en) | 1977-03-17 |
| AU1573076A (en) | 1978-01-12 |
| HK33781A (en) | 1981-07-24 |
| PT65301A (de) | 1976-07-01 |
| BG27378A3 (bg) | 1979-10-12 |
| CS193077B2 (en) | 1979-09-17 |
| YU166976A (en) | 1982-08-31 |
| CA1049497A (en) | 1979-02-27 |
| FI63418B (fi) | 1983-02-28 |
| ZA764064B (en) | 1977-07-27 |
| FI63418C (fi) | 1983-06-10 |
| RO71026A (ro) | 1981-09-24 |
| DE2530941C2 (de) | 1991-10-10 |
| JPS5539560B2 (enExample) | 1980-10-13 |
| AR210498A1 (es) | 1977-08-15 |
| FR2316962A1 (fr) | 1977-02-04 |
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