SU577997A3 - Способ получени оптических антиподов пантолактона - Google Patents
Способ получени оптических антиподов пантолактонаInfo
- Publication number
- SU577997A3 SU577997A3 SU7402031936A SU2031936A SU577997A3 SU 577997 A3 SU577997 A3 SU 577997A3 SU 7402031936 A SU7402031936 A SU 7402031936A SU 2031936 A SU2031936 A SU 2031936A SU 577997 A3 SU577997 A3 SU 577997A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- piti
- pantolactone
- pantoate
- preparing
- optical antipodes
- Prior art date
Links
- 230000003287 optical effect Effects 0.000 title description 6
- 229940115458 pantolactone Drugs 0.000 title description 3
- SERHXTVXHNVDKA-UHFFFAOYSA-N pantolactone Chemical compound CC1(C)COC(=O)C1O SERHXTVXHNVDKA-UHFFFAOYSA-N 0.000 title description 2
- SIEVQTNTRMBCHO-UHFFFAOYSA-N pantolactone Natural products CC1(C)OC(=O)CC1O SIEVQTNTRMBCHO-UHFFFAOYSA-N 0.000 title description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- OTOIIPJYVQJATP-BYPYZUCNSA-M (R)-pantoate Chemical compound OCC(C)(C)[C@@H](O)C([O-])=O OTOIIPJYVQJATP-BYPYZUCNSA-M 0.000 description 7
- 229910052744 lithium Inorganic materials 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- 239000012452 mother liquor Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 150000004679 hydroxides Chemical class 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 150000004682 monohydrates Chemical class 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 1
- CPGKMLVTFNUAHL-UHFFFAOYSA-N [Ca].[Ca] Chemical compound [Ca].[Ca] CPGKMLVTFNUAHL-UHFFFAOYSA-N 0.000 description 1
- 229910000288 alkali metal carbonate Inorganic materials 0.000 description 1
- 150000008041 alkali metal carbonates Chemical class 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- JEGUKCSWCFPDGT-UHFFFAOYSA-M hydroxide;hydrate Chemical compound O.[OH-] JEGUKCSWCFPDGT-UHFFFAOYSA-M 0.000 description 1
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 1
- 229910052808 lithium carbonate Inorganic materials 0.000 description 1
- -1 lithium-pantoate Chemical compound 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000006340 racemization Effects 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000012047 saturated solution Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/26—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
- C07D307/30—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D307/32—Oxygen atoms
- C07D307/33—Oxygen atoms in position 2, the oxygen atom being in its keto or unsubstituted enol form
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
- C07C59/01—Saturated compounds having only one carboxyl group and containing hydroxy or O-metal groups
- C07C59/10—Polyhydroxy carboxylic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Furan Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DD171272A DD109380A1 (enrdf_load_stackoverflow) | 1973-06-04 | 1973-06-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU577997A3 true SU577997A3 (ru) | 1977-10-25 |
Family
ID=5491480
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU7402031936A SU577997A3 (ru) | 1973-06-04 | 1974-06-03 | Способ получени оптических антиподов пантолактона |
Country Status (18)
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2401898A1 (fr) * | 1977-09-05 | 1979-03-30 | Aec Chim Organ Biolog | Nouveau sel de l'acide patoique |
| CN112047906A (zh) * | 2019-06-07 | 2020-12-08 | 帝斯曼知识产权资产管理有限公司 | 泛酰内酯的外消旋化方法 |
| CN111499602B (zh) * | 2020-05-14 | 2022-06-07 | 安徽泰格生物科技有限公司 | 一种钙盐法提取dl-泛解酸内酯拆分液中d-泛解酸内酯的方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1522111A (fr) * | 1966-05-10 | 1968-04-19 | Fuji Chemical Ind | Procédé de dédoublement du pantoate d'ammonium racémique |
| JPS5021448B1 (enrdf_load_stackoverflow) * | 1966-05-10 | 1975-07-23 |
-
1973
- 1973-06-04 DD DD171272A patent/DD109380A1/xx unknown
- 1973-10-09 DE DE2350610A patent/DE2350610C3/de not_active Expired
- 1973-10-29 GB GB5016973A patent/GB1395458A/en not_active Expired
-
1974
- 1974-01-14 JP JP745374A patent/JPS5512433B2/ja not_active Expired
- 1974-01-22 IE IE126/74A patent/IE38777B1/xx unknown
- 1974-05-17 IT IT51089/74A patent/IT1035078B/it active
- 1974-05-24 AR AR253919A patent/AR201439A1/es active
- 1974-05-27 AT AT435974A patent/AT339511B/de not_active IP Right Cessation
- 1974-05-31 FR FR7419015A patent/FR2231638B1/fr not_active Expired
- 1974-05-31 CS CS7400003903A patent/CS179302B1/cs unknown
- 1974-05-31 SE SE7407275A patent/SE417511B/xx unknown
- 1974-05-31 IS IS2215A patent/IS949B6/is unknown
- 1974-05-31 NL NL7407401A patent/NL7407401A/xx not_active Application Discontinuation
- 1974-06-03 RO RO7400079036A patent/RO63651A/ro unknown
- 1974-06-03 YU YU1528/74A patent/YU36945B/xx unknown
- 1974-06-03 RO RO7487342A patent/RO69917A/ro unknown
- 1974-06-03 SU SU7402031936A patent/SU577997A3/ru active
- 1974-06-04 CH CH758674A patent/CH602691A5/xx not_active IP Right Cessation
- 1974-06-04 CH CH1318077A patent/CH603613A5/xx not_active IP Right Cessation
-
1975
- 1975-04-25 BE BE155773A patent/BE828391Q/xx not_active IP Right Cessation
Also Published As
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