RU2206498C2 - Способ очистки перфторированных продуктов - Google Patents
Способ очистки перфторированных продуктов Download PDFInfo
- Publication number
- RU2206498C2 RU2206498C2 RU2000114632/12A RU2000114632A RU2206498C2 RU 2206498 C2 RU2206498 C2 RU 2206498C2 RU 2000114632/12 A RU2000114632/12 A RU 2000114632/12A RU 2000114632 A RU2000114632 A RU 2000114632A RU 2206498 C2 RU2206498 C2 RU 2206498C2
- Authority
- RU
- Russia
- Prior art keywords
- pfc
- nitrogen trifluoride
- tetrafluoromethane
- mixture
- composition
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 25
- 238000000746 purification Methods 0.000 title abstract 2
- 239000000203 mixture Substances 0.000 claims abstract 42
- TXEYQDLBPFQVAA-UHFFFAOYSA-N tetrafluoromethane Chemical compound FC(F)(F)F TXEYQDLBPFQVAA-UHFFFAOYSA-N 0.000 claims abstract 41
- QKCGXXHCELUCKW-UHFFFAOYSA-N n-[4-[4-(dinaphthalen-2-ylamino)phenyl]phenyl]-n-naphthalen-2-ylnaphthalen-2-amine Chemical compound C1=CC=CC2=CC(N(C=3C=CC(=CC=3)C=3C=CC(=CC=3)N(C=3C=C4C=CC=CC4=CC=3)C=3C=C4C=CC=CC4=CC=3)C3=CC4=CC=CC=C4C=C3)=CC=C21 QKCGXXHCELUCKW-UHFFFAOYSA-N 0.000 claims abstract 32
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract 14
- 238000004821 distillation Methods 0.000 claims abstract 14
- 150000001875 compounds Chemical class 0.000 claims abstract 12
- 239000003795 chemical substances by application Substances 0.000 claims abstract 11
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims abstract 10
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims abstract 10
- 229930195733 hydrocarbon Natural products 0.000 claims abstract 4
- 150000002430 hydrocarbons Chemical class 0.000 claims abstract 3
- 238000000605 extraction Methods 0.000 claims abstract 2
- MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical compound O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 claims 8
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 6
- 229910052731 fluorine Inorganic materials 0.000 claims 6
- 239000011737 fluorine Substances 0.000 claims 6
- 238000009835 boiling Methods 0.000 claims 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims 4
- XPDWGBQVDMORPB-UHFFFAOYSA-N Fluoroform Chemical compound FC(F)F XPDWGBQVDMORPB-UHFFFAOYSA-N 0.000 claims 4
- RWRIWBAIICGTTQ-UHFFFAOYSA-N difluoromethane Chemical compound FCF RWRIWBAIICGTTQ-UHFFFAOYSA-N 0.000 claims 4
- NEHMKBQYUWJMIP-UHFFFAOYSA-N chloromethane Chemical group ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 claims 3
- 239000012535 impurity Substances 0.000 claims 3
- UJPMYEOUBPIPHQ-UHFFFAOYSA-N 1,1,1-trifluoroethane Chemical compound CC(F)(F)F UJPMYEOUBPIPHQ-UHFFFAOYSA-N 0.000 claims 2
- VOPWNXZWBYDODV-UHFFFAOYSA-N Chlorodifluoromethane Chemical compound FC(F)Cl VOPWNXZWBYDODV-UHFFFAOYSA-N 0.000 claims 2
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 claims 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims 2
- 229910002092 carbon dioxide Inorganic materials 0.000 claims 2
- 239000001569 carbon dioxide Substances 0.000 claims 2
- UHCBBWUQDAVSMS-UHFFFAOYSA-N fluoroethane Chemical compound CCF UHCBBWUQDAVSMS-UHFFFAOYSA-N 0.000 claims 2
- NBVXSUQYWXRMNV-UHFFFAOYSA-N monofluoromethane Natural products FC NBVXSUQYWXRMNV-UHFFFAOYSA-N 0.000 claims 2
- QYSGYZVSCZSLHT-UHFFFAOYSA-N octafluoropropane Chemical compound FC(F)(F)C(F)(F)C(F)(F)F QYSGYZVSCZSLHT-UHFFFAOYSA-N 0.000 claims 2
- GTLACDSXYULKMZ-UHFFFAOYSA-N pentafluoroethane Chemical compound FC(F)C(F)(F)F GTLACDSXYULKMZ-UHFFFAOYSA-N 0.000 claims 2
- 238000000926 separation method Methods 0.000 claims 2
- ZRNSSRODJSSVEJ-UHFFFAOYSA-N 2-methylpentacosane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCC(C)C ZRNSSRODJSSVEJ-UHFFFAOYSA-N 0.000 claims 1
- 239000004215 Carbon black (E152) Substances 0.000 claims 1
- 241000252505 Characidae Species 0.000 claims 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims 1
- 239000005977 Ethylene Substances 0.000 claims 1
- 229910018503 SF6 Inorganic materials 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- KYKAJFCTULSVSH-UHFFFAOYSA-N chloro(fluoro)methane Chemical compound F[C]Cl KYKAJFCTULSVSH-UHFFFAOYSA-N 0.000 claims 1
- 238000005352 clarification Methods 0.000 claims 1
- WMIYKQLTONQJES-UHFFFAOYSA-N hexafluoroethane Chemical compound FC(F)(F)C(F)(F)F WMIYKQLTONQJES-UHFFFAOYSA-N 0.000 claims 1
- -1 hydrocarbon chloride Chemical class 0.000 claims 1
- 230000003993 interaction Effects 0.000 claims 1
- 229940050176 methyl chloride Drugs 0.000 claims 1
- 229960004065 perflutren Drugs 0.000 claims 1
- 239000001294 propane Substances 0.000 claims 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims 1
- SFZCNBIFKDRMGX-UHFFFAOYSA-N sulfur hexafluoride Chemical compound FS(F)(F)(F)(F)F SFZCNBIFKDRMGX-UHFFFAOYSA-N 0.000 claims 1
- 229960000909 sulfur hexafluoride Drugs 0.000 claims 1
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 claims 1
- 238000003889 chemical engineering Methods 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/36—Azeotropic distillation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/083—Compounds containing nitrogen and non-metals and optionally metals containing one or more halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/083—Compounds containing nitrogen and non-metals and optionally metals containing one or more halogen atoms
- C01B21/0832—Binary compounds of nitrogen with halogens
- C01B21/0835—Nitrogen trifluoride
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/083—Compounds containing nitrogen and non-metals and optionally metals containing one or more halogen atoms
- C01B21/0832—Binary compounds of nitrogen with halogens
- C01B21/0835—Nitrogen trifluoride
- C01B21/0837—Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US6499397P | 1997-11-10 | 1997-11-10 | |
| US60/064,993 | 1997-11-10 | ||
| US8614698P | 1998-05-20 | 1998-05-20 | |
| US60/086,146 | 1998-05-20 | ||
| US09/189,322 US6458249B2 (en) | 1997-11-10 | 1998-11-09 | Process for purifying perfluorinated products |
| US09/189,322 | 1998-11-09 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2000114632A RU2000114632A (ru) | 2002-05-27 |
| RU2206498C2 true RU2206498C2 (ru) | 2003-06-20 |
Family
ID=27370715
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2000114632/12A RU2206498C2 (ru) | 1997-11-10 | 1998-11-10 | Способ очистки перфторированных продуктов |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP1030818B1 (enExample) |
| JP (1) | JP2001522774A (enExample) |
| KR (1) | KR100588025B1 (enExample) |
| CN (4) | CN1252011C (enExample) |
| AT (1) | ATE222215T1 (enExample) |
| AU (1) | AU1455099A (enExample) |
| CA (1) | CA2306800A1 (enExample) |
| DE (1) | DE69807254T2 (enExample) |
| RU (1) | RU2206498C2 (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2248321C1 (ru) * | 2004-03-16 | 2005-03-20 | Общество с ограниченной ответственностью "НьюКем" | Способ очистки трифторида азота от тетрафторметана |
| RU2754857C1 (ru) * | 2017-10-23 | 2021-09-08 | Дайкин Индастриз, Лтд. | Способ получения гексафторбутадиена |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050016829A1 (en) * | 2003-04-14 | 2005-01-27 | Miller Ralph Newton | Distillation process for reducing the concentration of dinitrogen difluoride and dinitrogen tetrafluoride in nitrogen trifluoride |
| CN1328160C (zh) * | 2005-07-27 | 2007-07-25 | 中国船舶重工集团公司第七一八研究所 | 三氟化氮气体的纯化方法 |
| KR100703875B1 (ko) * | 2005-09-07 | 2007-04-04 | 주식회사 소디프신소재 | 삼불화질소의 정제방법 |
| TW200808649A (en) * | 2006-05-31 | 2008-02-16 | Du Pont | Process for purifying perfluorinated products |
| CN101920944A (zh) * | 2010-08-30 | 2010-12-22 | 天津市泰源工业气体有限公司 | 一种萃取精馏分离三氟化氮与四氟化碳制备高纯三氟化氮的技术 |
| CN102516018A (zh) * | 2011-12-16 | 2012-06-27 | 天津市泰亨气体有限公司 | 一种制备高纯四氟化碳的方法 |
| KR101514801B1 (ko) * | 2013-06-25 | 2015-04-24 | (주)파인텍 | 과불화화합물의 분리 및 재활용시스템 |
| ES2937914T3 (es) * | 2019-01-23 | 2023-04-03 | Weiss Technik Gmbh | Refrigerante |
| CN112279234B (zh) * | 2019-07-23 | 2023-08-08 | 中化近代环保化工(西安)有限公司 | 碳酰氟与二氧化碳的共沸组合物 |
| CN114288702A (zh) * | 2021-12-24 | 2022-04-08 | 天津海嘉斯迪新材料合伙企业(有限合伙) | 一种三氟化氮气体中氧化亚氮的回收系统及方法 |
| CN114191829A (zh) * | 2021-12-31 | 2022-03-18 | 天津海嘉斯迪新材料合伙企业(有限合伙) | 一种三氟化氮粗品中氧化亚氮的去除方法和系统 |
| CN114538391B (zh) * | 2022-03-01 | 2023-11-03 | 中船(邯郸)派瑞特种气体股份有限公司 | 一种从nf3废气中回收高纯n2o的装置及其回收方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5069887A (en) * | 1990-01-10 | 1991-12-03 | Central Glass Company, Limited | Method of refining nitrogen trifluoride gas |
| US5637285A (en) * | 1996-01-30 | 1997-06-10 | Air Products And Chemicals, Inc. | Process for nitrogen trifluoride synthesis |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63306383A (ja) * | 1987-06-04 | 1988-12-14 | 三井東圧化学株式会社 | フッ化窒素の精製方法 |
-
1998
- 1998-11-10 CA CA002306800A patent/CA2306800A1/en not_active Abandoned
- 1998-11-10 JP JP2000520379A patent/JP2001522774A/ja active Pending
- 1998-11-10 RU RU2000114632/12A patent/RU2206498C2/ru not_active IP Right Cessation
- 1998-11-10 CN CNB031314635A patent/CN1252011C/zh not_active Expired - Fee Related
- 1998-11-10 EP EP98958520A patent/EP1030818B1/en not_active Expired - Lifetime
- 1998-11-10 KR KR1020007005058A patent/KR100588025B1/ko not_active Expired - Fee Related
- 1998-11-10 AT AT98958520T patent/ATE222215T1/de not_active IP Right Cessation
- 1998-11-10 AU AU14550/99A patent/AU1455099A/en not_active Abandoned
- 1998-11-10 DE DE69807254T patent/DE69807254T2/de not_active Expired - Fee Related
- 1998-11-10 CN CNB031314678A patent/CN1246216C/zh not_active Expired - Fee Related
- 1998-11-10 CN CNB988109646A patent/CN1137043C/zh not_active Expired - Fee Related
- 1998-11-10 CN CNB031314643A patent/CN1219739C/zh not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5069887A (en) * | 1990-01-10 | 1991-12-03 | Central Glass Company, Limited | Method of refining nitrogen trifluoride gas |
| US5637285A (en) * | 1996-01-30 | 1997-06-10 | Air Products And Chemicals, Inc. | Process for nitrogen trifluoride synthesis |
Non-Patent Citations (1)
| Title |
|---|
| КАСАТКИН А.Г. Основные процессы и аппараты химической технологии. - М.: Гос. научно-техническое из-во химической литературы, 1950, с. 544-545. Краткая химическая энциклопедия. - М.: Гос. научное из-во "Советская энциклопедия", 1961, т.1, с. 53. ГЕЛЬПЕРИН Н.И. Основные процессы и аппараты химической технологии. Книга 2. - М.: Химия, 1981, с. 529. * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2248321C1 (ru) * | 2004-03-16 | 2005-03-20 | Общество с ограниченной ответственностью "НьюКем" | Способ очистки трифторида азота от тетрафторметана |
| WO2005087659A1 (en) * | 2004-03-16 | 2005-09-22 | Obschesctvo S Ogranichennoy Otvetstvennostyu 'newchem' | Method for removing tetrafluormethane from nitrogen trifluoride |
| RU2754857C1 (ru) * | 2017-10-23 | 2021-09-08 | Дайкин Индастриз, Лтд. | Способ получения гексафторбутадиена |
Also Published As
| Publication number | Publication date |
|---|---|
| ATE222215T1 (de) | 2002-08-15 |
| KR100588025B1 (ko) | 2006-06-13 |
| CN1219739C (zh) | 2005-09-21 |
| CA2306800A1 (en) | 1999-05-20 |
| CN1515488A (zh) | 2004-07-28 |
| CN1137043C (zh) | 2004-02-04 |
| CN1278779A (zh) | 2001-01-03 |
| CN1252011C (zh) | 2006-04-19 |
| JP2001522774A (ja) | 2001-11-20 |
| KR20010031951A (ko) | 2001-04-16 |
| AU1455099A (en) | 1999-05-31 |
| CN1246216C (zh) | 2006-03-22 |
| DE69807254T2 (de) | 2003-04-10 |
| EP1030818B1 (en) | 2002-08-14 |
| EP1030818A1 (en) | 2000-08-30 |
| CN1515527A (zh) | 2004-07-28 |
| CN1515529A (zh) | 2004-07-28 |
| DE69807254D1 (de) | 2002-09-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| RU2206498C2 (ru) | Способ очистки перфторированных продуктов | |
| CA1325996C (en) | Process for the separation of hf via azeotropic distillation | |
| US6458249B2 (en) | Process for purifying perfluorinated products | |
| EP0864554B1 (en) | Method for purifying crude 1,1,1,3,3-pentafluoropropane | |
| JP2011042570A (ja) | 弗化水素を精製する方法 | |
| RU2000114632A (ru) | Способ очистки перфорированных продуктов | |
| RU98108542A (ru) | Способ извлечения фтороводорода | |
| JP2001522774A5 (enExample) | ||
| JP4187798B2 (ja) | 弗化水素の回収方法 | |
| RU2088562C1 (ru) | Способ разделения хлористого водорода и тетрафторэтилена | |
| WO1995021147A1 (en) | Process for separating pentafluoroethane from a mixture comprising halogenated hydrocarbons and chloropentafluoroethane | |
| RU99123531A (ru) | Способ извлечения фтористого водорода | |
| JPH06172228A (ja) | フッ化水素と1,1,1−トリフルオロ−2−クロロエタンとの混合物からのフッ化水素分離方法 | |
| KR20040012885A (ko) | 공비-성 조성물, 및 펜타플로오로에탄과 염화수소의분리방법 | |
| EP1773745B1 (en) | AZEOTROPE-LIKE COMPOSITIONS OF DIFLUOROMETHANE AND HCl | |
| JP4275313B2 (ja) | フッ化水素から1,1,1,3,3−ペンタフルオロプロパンを分離する方法 | |
| JPH08143486A (ja) | ペンタフルオロエタンの精製方法 | |
| JP2001342007A (ja) | フッ化水素の分離方法 | |
| RU2005135131A (ru) | Способ дистилляции для уменьшения концентрации дифтордиазина и тетрафторгидразина в трифториде азота | |
| KR100197153B1 (ko) | 디플루오로메탄 혼합물로부터 디클로로디플루오로메탄을 제거하는 방법 | |
| EP1229000A2 (en) | Process for purifying perfluorinated products | |
| WO1998015511A1 (en) | Process for separating pentafluoroethane and chloropentafluoroethane | |
| JPH09255597A (ja) | ペンタフルオロエタンの精製方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20091111 |