RU2013151313A - Сополимеры малеинового ангидрида в качестве растворимого вспомогательного материала для принтера, использующего технологию послойного наложения расплавленной полимерной нити (fdm) - Google Patents
Сополимеры малеинового ангидрида в качестве растворимого вспомогательного материала для принтера, использующего технологию послойного наложения расплавленной полимерной нити (fdm) Download PDFInfo
- Publication number
- RU2013151313A RU2013151313A RU2013151313/04A RU2013151313A RU2013151313A RU 2013151313 A RU2013151313 A RU 2013151313A RU 2013151313/04 A RU2013151313/04 A RU 2013151313/04A RU 2013151313 A RU2013151313 A RU 2013151313A RU 2013151313 A RU2013151313 A RU 2013151313A
- Authority
- RU
- Russia
- Prior art keywords
- auxiliary material
- material according
- maleic anhydride
- copolymer
- styrene
- Prior art date
Links
- 239000000463 material Substances 0.000 title claims abstract 27
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 title claims abstract 11
- 238000005516 engineering process Methods 0.000 title claims abstract 3
- 229920000642 polymer Polymers 0.000 title 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims abstract 14
- 229920001577 copolymer Polymers 0.000 claims abstract 14
- 230000009477 glass transition Effects 0.000 claims abstract 6
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical group CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 claims abstract 5
- 239000000203 mixture Substances 0.000 claims abstract 5
- 239000012736 aqueous medium Substances 0.000 claims abstract 4
- WOBHKFSMXKNTIM-UHFFFAOYSA-N Hydroxyethyl methacrylate Chemical compound CC(=C)C(=O)OCCO WOBHKFSMXKNTIM-UHFFFAOYSA-N 0.000 claims abstract 3
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims abstract 3
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract 3
- 125000000956 methoxy group Chemical group [H]C([H])([H])O* 0.000 claims abstract 3
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract 3
- 238000010146 3D printing Methods 0.000 claims abstract 2
- 238000000034 method Methods 0.000 claims abstract 2
- 239000000178 monomer Substances 0.000 claims abstract 2
- 239000003607 modifier Substances 0.000 claims 1
- 239000000049 pigment Substances 0.000 claims 1
- 239000004014 plasticizer Substances 0.000 claims 1
- 239000006254 rheological additive Substances 0.000 claims 1
- 239000003381 stabilizer Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F222/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical and containing at least one other carboxyl radical in the molecule; Salts, anhydrides, esters, amides, imides, or nitriles thereof
- C08F222/04—Anhydrides, e.g. cyclic anhydrides
- C08F222/06—Maleic anhydride
- C08F222/08—Maleic anhydride with vinyl aromatic monomers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C41/00—Shaping by coating a mould, core or other substrate, i.e. by depositing material and stripping-off the shaped article; Apparatus therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C67/00—Shaping techniques not covered by groups B29C39/00 - B29C65/00, B29C70/00 or B29C73/00
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F212/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
- C08F212/02—Monomers containing only one unsaturated aliphatic radical
- C08F212/04—Monomers containing only one unsaturated aliphatic radical containing one ring
- C08F212/06—Hydrocarbons
- C08F212/08—Styrene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F222/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical and containing at least one other carboxyl radical in the molecule; Salts, anhydrides, esters, amides, imides, or nitriles thereof
- C08F222/04—Anhydrides, e.g. cyclic anhydrides
- C08F222/06—Maleic anhydride
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L35/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical, and containing at least one other carboxyl radical in the molecule, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C64/00—Additive manufacturing, i.e. manufacturing of three-dimensional [3D] objects by additive deposition, additive agglomeration or additive layering, e.g. by 3D printing, stereolithography or selective laser sintering
- B29C64/40—Structures for supporting 3D objects during manufacture and intended to be sacrificed after completion thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/04—Acids; Metal salts or ammonium salts thereof
- C08F220/06—Acrylic acid; Methacrylic acid; Metal salts or ammonium salts thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP11163199A EP2514775A1 (en) | 2011-04-20 | 2011-04-20 | Maleic anhydride copolymers as soluble support material for fused deposition modelling (FDM) printer |
| EP11163199.0 | 2011-04-20 | ||
| PCT/EP2012/054306 WO2012143182A1 (en) | 2011-04-20 | 2012-03-13 | Maleic anhydride copolymers as soluble support material for fused deposition modelling (fdm) printer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RU2013151313A true RU2013151313A (ru) | 2015-05-27 |
Family
ID=44560045
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2013151313/04A RU2013151313A (ru) | 2011-04-20 | 2012-03-13 | Сополимеры малеинового ангидрида в качестве растворимого вспомогательного материала для принтера, использующего технологию послойного наложения расплавленной полимерной нити (fdm) |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8822590B2 (enExample) |
| EP (2) | EP2514775A1 (enExample) |
| JP (1) | JP5893128B2 (enExample) |
| KR (1) | KR20140009442A (enExample) |
| CN (1) | CN103380156B (enExample) |
| AU (1) | AU2012244499B2 (enExample) |
| BR (1) | BR112013023429B8 (enExample) |
| CA (1) | CA2833752C (enExample) |
| IL (1) | IL227363A (enExample) |
| RU (1) | RU2013151313A (enExample) |
| WO (1) | WO2012143182A1 (enExample) |
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| US9498593B2 (en) | 2013-06-17 | 2016-11-22 | MetaMason, Inc. | Customized medical devices and apparel |
| US9029058B2 (en) * | 2013-07-17 | 2015-05-12 | Stratasys, Inc. | Soluble support material for electrophotography-based additive manufacturing |
| WO2015012862A1 (en) * | 2013-07-26 | 2015-01-29 | Hewlett-Packard Development Company, L.P. | Composite support material for three-dimensional printing |
| US10843401B2 (en) * | 2013-11-01 | 2020-11-24 | Kraton Polymers U.S. Llc | Fuse molded three dimensional article and a method for making the same |
| EP3083823B1 (de) * | 2013-12-18 | 2019-03-27 | INEOS Styrolution Group GmbH | Formmassen basierend auf vinylaromat-polymeren für den 3d druck |
| CN106029776B (zh) * | 2013-12-18 | 2019-12-31 | 英力士苯领集团股份公司 | 用于3-d打印的基于乙烯基芳族/二烯嵌段共聚物的成型材料 |
| WO2015091817A1 (de) * | 2013-12-18 | 2015-06-25 | Styrolution Group Gmbh | Formmassen basierend auf vinylaromat-copolymeren für den 3d druck |
| US10259921B2 (en) | 2014-01-16 | 2019-04-16 | Dow Global Technologies Llc | Support materials for 3D printing |
| CN105899591A (zh) | 2014-01-16 | 2016-08-24 | 陶氏环球技术有限责任公司 | 增材制造负载材料的回收 |
| US9102099B1 (en) | 2014-02-05 | 2015-08-11 | MetaMason, Inc. | Methods for additive manufacturing processes incorporating active deposition |
| KR102370310B1 (ko) * | 2014-02-19 | 2022-03-04 | 바스프 에스이 | 용융 필라멘트 압출 조형에 사용하기 위한 지지체 재료로서의 폴리머 |
| US9676159B2 (en) | 2014-05-09 | 2017-06-13 | Nike, Inc. | Method for forming three-dimensional structures with different material portions |
| KR20170017928A (ko) * | 2014-06-16 | 2017-02-15 | 사빅 글로벌 테크놀러지스 비.브이. | 적층 가공 방법 |
| CN105936130B (zh) * | 2014-09-10 | 2017-08-15 | 珠海天威飞马打印耗材有限公司 | 3d物体的成型方法、3d打印机的工作台以及3d打印机 |
| WO2016059987A1 (ja) * | 2014-10-14 | 2016-04-21 | 花王株式会社 | 三次元造形用可溶性材料 |
| JP5972335B2 (ja) | 2014-10-14 | 2016-08-17 | 花王株式会社 | 三次元造形用可溶性材料 |
| JP6491467B2 (ja) | 2014-10-14 | 2019-03-27 | 花王株式会社 | 三次元造形用可溶性材料 |
| WO2016106062A1 (en) | 2014-12-23 | 2016-06-30 | Bridgestone Americas Tire Operations, Llc | Actinic radiation curable polymeric mixtures, cured polymeric mixtures and related processes |
| FR3030529B1 (fr) * | 2014-12-23 | 2017-01-27 | Arkema France | Copolymere a blocs hydrosoluble et son utilisation comme materiau support pour impression 3d |
| KR102064816B1 (ko) | 2015-06-19 | 2020-01-10 | 스트래터시스,인코포레이티드 | 적층 제조에 사용되는 수계 분산형 중합체 |
| EP3328930B1 (en) | 2015-07-27 | 2019-05-29 | Dow Global Technologies LLC | Method to additive manufacture biocompatible material and articles made by the method |
| WO2017020020A1 (en) * | 2015-07-30 | 2017-02-02 | Wildcat Dp Llc | Material and method for 3-d fabrication |
| US10800094B2 (en) | 2015-09-14 | 2020-10-13 | Carbon, Inc. | Light-curable article of manufacture with portions of differing solubility |
| US10647873B2 (en) | 2015-10-30 | 2020-05-12 | Carbon, Inc. | Dual cure article of manufacture with portions of differing solubility |
| KR102053481B1 (ko) * | 2015-11-03 | 2019-12-06 | 주식회사 엘지화학 | 3차원 조형물의 형성 방법 |
| JP2019500646A (ja) | 2015-12-03 | 2019-01-10 | エル．スティーブン ブキャナンＬ． Ｓｔｅｐｈｅｎ Ｂｕｃｈａｎａｎ | 解剖学的構造用器具および歯科医のための遠隔かつ対話型の実践的な手術訓練用訓練システム |
| US11097531B2 (en) | 2015-12-17 | 2021-08-24 | Bridgestone Americas Tire Operations, Llc | Additive manufacturing cartridges and processes for producing cured polymeric products by additive manufacturing |
| EP3389853B1 (en) | 2015-12-18 | 2023-10-18 | University of Canterbury | Separation medium |
| US11045997B2 (en) * | 2015-12-24 | 2021-06-29 | Stratasys, Inc. | Water soluble support materials for high temperature additive manufacturing applications |
| US10953595B2 (en) | 2015-12-24 | 2021-03-23 | Stratasys, Inc. | Water soluble support materials for high temperature additive manufacturing applications |
| JP6806088B2 (ja) * | 2016-01-05 | 2021-01-06 | コニカミノルタ株式会社 | 粉末材料、立体造形物の製造方法および立体造形装置 |
| US10449713B2 (en) | 2016-01-25 | 2019-10-22 | Te Connectivity Corporation | Article and method of forming an article |
| CN109153776B (zh) | 2016-05-04 | 2021-03-12 | 科思创德国股份有限公司 | 作为3d打印中支撑材料的共聚碳酸酯 |
| WO2018049365A1 (en) | 2016-09-12 | 2018-03-15 | Sabic Global Technologies B.V. | Sacrificial high heat support materials for additive manufacturing processes |
| WO2018081053A1 (en) | 2016-10-27 | 2018-05-03 | Bridgestone Americas Tire Operations, Llc | Processes for producing cured polymeric products by additive manufacturing |
| JP6990594B2 (ja) * | 2017-02-07 | 2022-01-12 | 株式会社日本触媒 | 水性樹脂組成物 |
| EP3635045A1 (en) | 2017-05-26 | 2020-04-15 | Infinite Material Solutions, LLC | Water soluble polymer compositions |
| WO2018227094A1 (en) | 2017-06-08 | 2018-12-13 | Buchanan Stephen L | Tooth or tooth replica holding sleeve for use with an paex locator |
| JP2019064258A (ja) * | 2017-09-28 | 2019-04-25 | 花王株式会社 | 三次元造形用可溶性材料 |
| EP3689585B1 (en) * | 2017-09-28 | 2022-02-09 | Kao Corporation | Soluble material for three-dimensional modeling |
| US11220062B2 (en) | 2017-10-10 | 2022-01-11 | Stratasys, Inc. | Water-dispersible thermoplastic material comprising sulfonated copolymer for use in additive manufacturing |
| FR3074181B1 (fr) | 2017-11-28 | 2020-11-06 | Arkema France | Composition copolymerique hydrosoluble a ph neutre |
| WO2019151234A1 (ja) * | 2018-02-02 | 2019-08-08 | 三菱ケミカル株式会社 | ３次元造形用材料、３次元造形用フィラメント、該フィラメントの巻回体および３次元プリンター用カートリッジ |
| CN111630144B (zh) | 2018-02-22 | 2021-12-31 | 宝洁公司 | 用于制备单位剂量制品的方法 |
| WO2020077127A1 (en) * | 2018-10-10 | 2020-04-16 | Stratasys, Inc. | Water dispersible sulfonated thermoplastic copolymer for use in additive manufacturing |
| FR3088327B1 (fr) | 2018-11-08 | 2021-11-05 | Arkema France | Composition copolymerique hydrosoluble |
| WO2021126739A1 (en) * | 2019-12-17 | 2021-06-24 | Ticona Llc | Three-dimensional printing system employing a toughened polyarylene sulfide composition |
| EP3865302B1 (en) * | 2020-02-14 | 2024-08-14 | iSQUARED AG | Copolymer for use in a digital manufacturing process |
| US12371581B2 (en) | 2020-03-25 | 2025-07-29 | Infinite Material Solutions, Llc | High performance water soluble polymer compositions |
| WO2022029211A1 (en) * | 2020-08-06 | 2022-02-10 | Signify Holding B.V. | Continuous hollow tube printing using fdm |
| US12157800B2 (en) | 2021-04-12 | 2024-12-03 | Stratasys, Inc. | Method for underwater processing of water-dispersible materials |
| IL307707B2 (en) | 2021-04-19 | 2025-02-01 | Jabil Inc | Improved degradable support material for additive manufacturing |
| FR3124420B1 (fr) * | 2021-06-23 | 2024-09-27 | Arkema France | Utilisation de copolymères multi blocs en tant que matériau sacrificiel dans un procédé d’impression 3D |
| WO2024076464A1 (en) | 2022-10-03 | 2024-04-11 | Jabil Inc. | Additive manufactured article comprising a grafted aliphatic polyketone, filament and powder |
| NL2036419B1 (en) | 2023-12-04 | 2025-06-13 | Tectonic 3D Swip B V | Fused deposition modeling method and method to dissolve a high temperature polycarbonate support used in this method |
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| AU463914B2 (en) | 1971-09-22 | 1975-08-07 | Dow Chemical Company, The | Impact resistant polymers ofa resinous copolymer ofan alkenyl aromatic. monomer and unsaturated dicarboxylic anhydride |
| DE3034171A1 (de) * | 1980-09-11 | 1982-05-06 | Basf Ag, 6700 Ludwigshafen | Alkaliloesliche harze auf basis von copolymerisaten aus monoolefinisch ungesaettigten carbonsaeuren und durch aromaten substituierten (alpha) -olefinen und ihre verwendung als harzkomponente in polymerdispersionen |
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| JPH075302A (ja) * | 1993-06-15 | 1995-01-10 | Tosoh Corp | マイクロ集光レンズ形成用感光性組成物 |
| US5503785A (en) | 1994-06-02 | 1996-04-02 | Stratasys, Inc. | Process of support removal for fused deposition modeling |
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| US6228923B1 (en) * | 1997-04-02 | 2001-05-08 | Stratasys, Inc. | Water soluble rapid prototyping support and mold material |
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| JP2006111710A (ja) * | 2004-10-14 | 2006-04-27 | Nof Corp | 無水マレイン酸（共）重合体の製造方法、無水マレイン酸（共）重合体、及びその加水分解物 |
| CN100387419C (zh) * | 2006-01-16 | 2008-05-14 | 南京师范大学 | 采用逐层喷涂方式制作三维物体的方法 |
| CN100340388C (zh) * | 2006-03-03 | 2007-10-03 | 南京师范大学 | 制作三维物体和支撑的打印成型方法 |
| US8246888B2 (en) * | 2008-10-17 | 2012-08-21 | Stratasys, Inc. | Support material for digital manufacturing systems |
-
2011
- 2011-04-20 EP EP11163199A patent/EP2514775A1/en not_active Withdrawn
-
2012
- 2012-03-13 JP JP2014505552A patent/JP5893128B2/ja not_active Expired - Fee Related
- 2012-03-13 WO PCT/EP2012/054306 patent/WO2012143182A1/en not_active Ceased
- 2012-03-13 US US13/982,431 patent/US8822590B2/en active Active
- 2012-03-13 AU AU2012244499A patent/AU2012244499B2/en not_active Ceased
- 2012-03-13 KR KR1020137026041A patent/KR20140009442A/ko not_active Withdrawn
- 2012-03-13 EP EP12708835.9A patent/EP2699611B1/en active Active
- 2012-03-13 CA CA2833752A patent/CA2833752C/en active Active
- 2012-03-13 BR BR112013023429A patent/BR112013023429B8/pt not_active IP Right Cessation
- 2012-03-13 RU RU2013151313/04A patent/RU2013151313A/ru not_active Application Discontinuation
- 2012-03-13 CN CN201280009711.4A patent/CN103380156B/zh not_active Expired - Fee Related
-
2013
- 2013-07-07 IL IL227363A patent/IL227363A/en active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| JP2014511933A (ja) | 2014-05-19 |
| IL227363A (en) | 2016-09-29 |
| CN103380156B (zh) | 2016-01-20 |
| AU2012244499B2 (en) | 2015-05-21 |
| BR112013023429B1 (pt) | 2020-11-17 |
| US8822590B2 (en) | 2014-09-02 |
| AU2012244499A1 (en) | 2013-07-25 |
| EP2699611B1 (en) | 2015-05-06 |
| IL227363A0 (en) | 2013-09-30 |
| CA2833752A1 (en) | 2012-10-26 |
| US20130317164A1 (en) | 2013-11-28 |
| KR20140009442A (ko) | 2014-01-22 |
| EP2699611A1 (en) | 2014-02-26 |
| JP5893128B2 (ja) | 2016-03-23 |
| CN103380156A (zh) | 2013-10-30 |
| BR112013023429A2 (pt) | 2016-12-13 |
| EP2514775A1 (en) | 2012-10-24 |
| CA2833752C (en) | 2019-05-14 |
| BR112013023429B8 (pt) | 2022-07-05 |
| WO2012143182A1 (en) | 2012-10-26 |
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