NO324884B1 - Fremgangsmate for separering av vandige inulinopplosninger som inneholder karbohydrater i fraksjoner som har forskjellige gjennomsnittlige polymerisasjonsgrader - Google Patents
Fremgangsmate for separering av vandige inulinopplosninger som inneholder karbohydrater i fraksjoner som har forskjellige gjennomsnittlige polymerisasjonsgrader Download PDFInfo
- Publication number
- NO324884B1 NO324884B1 NO19970490A NO970490A NO324884B1 NO 324884 B1 NO324884 B1 NO 324884B1 NO 19970490 A NO19970490 A NO 19970490A NO 970490 A NO970490 A NO 970490A NO 324884 B1 NO324884 B1 NO 324884B1
- Authority
- NO
- Norway
- Prior art keywords
- inulin
- polymerization
- aqueous solution
- fractions
- degrees
- Prior art date
Links
- 229920001202 Inulin Polymers 0.000 title claims description 118
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 title claims description 116
- 229940029339 inulin Drugs 0.000 title claims description 116
- 238000000034 method Methods 0.000 title claims description 57
- 238000006116 polymerization reaction Methods 0.000 title claims description 54
- 150000001720 carbohydrates Chemical class 0.000 title claims description 20
- 235000014633 carbohydrates Nutrition 0.000 title claims description 20
- 239000012528 membrane Substances 0.000 claims description 65
- 239000012466 permeate Substances 0.000 claims description 53
- 239000007864 aqueous solution Substances 0.000 claims description 40
- 239000000243 solution Substances 0.000 claims description 29
- 238000000108 ultra-filtration Methods 0.000 claims description 23
- 239000012535 impurity Substances 0.000 claims description 16
- 108090000790 Enzymes Proteins 0.000 claims description 15
- 102000004190 Enzymes Human genes 0.000 claims description 15
- 239000012465 retentate Substances 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 12
- 239000012510 hollow fiber Substances 0.000 claims description 11
- 239000011148 porous material Substances 0.000 claims description 11
- 240000008892 Helianthus tuberosus Species 0.000 claims description 9
- 235000003230 Helianthus tuberosus Nutrition 0.000 claims description 9
- 102000004169 proteins and genes Human genes 0.000 claims description 7
- 108090000623 proteins and genes Proteins 0.000 claims description 7
- 235000007542 Cichorium intybus Nutrition 0.000 claims description 6
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 6
- 150000001413 amino acids Chemical class 0.000 claims description 6
- 238000005374 membrane filtration Methods 0.000 claims description 6
- 229930091371 Fructose Natural products 0.000 claims description 5
- 239000005715 Fructose Substances 0.000 claims description 5
- 239000003925 fat Substances 0.000 claims description 5
- 239000012634 fragment Substances 0.000 claims description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 5
- 239000011707 mineral Substances 0.000 claims description 5
- 239000013618 particulate matter Substances 0.000 claims description 5
- 244000115658 Dahlia pinnata Species 0.000 claims description 4
- 235000012040 Dahlia pinnata Nutrition 0.000 claims description 4
- 210000002421 cell wall Anatomy 0.000 claims description 4
- 238000004925 denaturation Methods 0.000 claims description 4
- 230000036425 denaturation Effects 0.000 claims description 4
- 244000005700 microbiome Species 0.000 claims description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 3
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 3
- 239000008103 glucose Substances 0.000 claims description 3
- 239000011236 particulate material Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 2
- 244000298479 Cichorium intybus Species 0.000 claims 1
- 230000002745 absorbent Effects 0.000 claims 1
- 239000002250 absorbent Substances 0.000 claims 1
- 239000012141 concentrate Substances 0.000 description 30
- 239000000203 mixture Substances 0.000 description 24
- 238000011026 diafiltration Methods 0.000 description 23
- 239000000047 product Substances 0.000 description 18
- 239000000284 extract Substances 0.000 description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 16
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 10
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 10
- 238000000926 separation method Methods 0.000 description 9
- 241000196324 Embryophyta Species 0.000 description 8
- 238000002360 preparation method Methods 0.000 description 8
- 239000011347 resin Substances 0.000 description 8
- 229920005989 resin Polymers 0.000 description 8
- 244000089742 Citrus aurantifolia Species 0.000 description 7
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 7
- 235000011941 Tilia x europaea Nutrition 0.000 description 7
- 230000003247 decreasing effect Effects 0.000 description 7
- 238000005194 fractionation Methods 0.000 description 7
- 239000004571 lime Substances 0.000 description 7
- 238000009826 distribution Methods 0.000 description 6
- 238000000605 extraction Methods 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 238000012545 processing Methods 0.000 description 6
- 241000723343 Cichorium Species 0.000 description 5
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 5
- 229930006000 Sucrose Natural products 0.000 description 5
- 229910052799 carbon Inorganic materials 0.000 description 5
- 239000001569 carbon dioxide Substances 0.000 description 5
- 229910002092 carbon dioxide Inorganic materials 0.000 description 5
- 235000013305 food Nutrition 0.000 description 5
- 150000002772 monosaccharides Chemical class 0.000 description 5
- 239000005720 sucrose Substances 0.000 description 5
- FLDFNEBHEXLZRX-RUAPLKMPSA-N (2S,5S)-2-[(2S,5R)-2-[[(2R,5R)-2-[[(2R,5R)-3,4-dihydroxy-2,5-bis(hydroxymethyl)oxolan-2-yl]oxymethyl]-3,4-dihydroxy-5-(hydroxymethyl)oxolan-2-yl]oxymethyl]-3,4-dihydroxy-5-(hydroxymethyl)oxolan-2-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound OC[C@H]1O[C@@](CO)(OC[C@@]2(OC[C@@]3(O[C@@H]4OC(CO)[C@@H](O)C(O)C4O)O[C@H](CO)C(O)C3O)O[C@H](CO)C(O)C2O)C(O)C1O FLDFNEBHEXLZRX-RUAPLKMPSA-N 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 239000008367 deionised water Substances 0.000 description 4
- 229910021641 deionized water Inorganic materials 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 238000002955 isolation Methods 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000003463 adsorbent Substances 0.000 description 3
- 239000000287 crude extract Substances 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 238000003306 harvesting Methods 0.000 description 3
- 230000007062 hydrolysis Effects 0.000 description 3
- 238000006460 hydrolysis reaction Methods 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 238000001542 size-exclusion chromatography Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical group [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- 229920002670 Fructan Polymers 0.000 description 2
- 102000004877 Insulin Human genes 0.000 description 2
- 108090001061 Insulin Proteins 0.000 description 2
- 239000005909 Kieselgur Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 238000009295 crossflow filtration Methods 0.000 description 2
- 238000005520 cutting process Methods 0.000 description 2
- 238000004042 decolorization Methods 0.000 description 2
- 238000002242 deionisation method Methods 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 150000002016 disaccharides Chemical class 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 230000004907 flux Effects 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- NOESYZHRGYRDHS-UHFFFAOYSA-N insulin Chemical compound N1C(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(NC(=O)CN)C(C)CC)CSSCC(C(NC(CO)C(=O)NC(CC(C)C)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CCC(N)=O)C(=O)NC(CC(C)C)C(=O)NC(CCC(O)=O)C(=O)NC(CC(N)=O)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CSSCC(NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2C=CC(O)=CC=2)NC(=O)C(CC(C)C)NC(=O)C(C)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2NC=NC=2)NC(=O)C(CO)NC(=O)CNC2=O)C(=O)NCC(=O)NC(CCC(O)=O)C(=O)NC(CCCNC(N)=N)C(=O)NCC(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC(O)=CC=3)C(=O)NC(C(C)O)C(=O)N3C(CCC3)C(=O)NC(CCCCN)C(=O)NC(C)C(O)=O)C(=O)NC(CC(N)=O)C(O)=O)=O)NC(=O)C(C(C)CC)NC(=O)C(CO)NC(=O)C(C(C)O)NC(=O)C1CSSCC2NC(=O)C(CC(C)C)NC(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CC(N)=O)NC(=O)C(NC(=O)C(N)CC=1C=CC=CC=1)C(C)C)CC1=CN=CN1 NOESYZHRGYRDHS-UHFFFAOYSA-N 0.000 description 2
- 108010090785 inulinase Proteins 0.000 description 2
- 239000003456 ion exchange resin Substances 0.000 description 2
- 229920003303 ion-exchange polymer Polymers 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000011020 pilot scale process Methods 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000003643 water by type Substances 0.000 description 2
- ZFTFOHBYVDOAMH-XNOIKFDKSA-N (2r,3s,4s,5r)-5-[[(2r,3s,4s,5r)-5-[[(2r,3s,4s,5r)-3,4-dihydroxy-2,5-bis(hydroxymethyl)oxolan-2-yl]oxymethyl]-3,4-dihydroxy-2-(hydroxymethyl)oxolan-2-yl]oxymethyl]-2-(hydroxymethyl)oxolane-2,3,4-triol Chemical class O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@@H]1[C@@H](O)[C@H](O)[C@](CO)(OC[C@@H]2[C@H]([C@H](O)[C@@](O)(CO)O2)O)O1 ZFTFOHBYVDOAMH-XNOIKFDKSA-N 0.000 description 1
- 244000291564 Allium cepa Species 0.000 description 1
- 235000002732 Allium cepa var. cepa Nutrition 0.000 description 1
- 240000002234 Allium sativum Species 0.000 description 1
- 235000016068 Berberis vulgaris Nutrition 0.000 description 1
- 241000335053 Beta vulgaris Species 0.000 description 1
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- 241000219130 Cucurbita pepo subsp. pepo Species 0.000 description 1
- 235000003954 Cucurbita pepo var melopepo Nutrition 0.000 description 1
- 244000019459 Cynara cardunculus Species 0.000 description 1
- 235000019106 Cynara scolymus Nutrition 0.000 description 1
- 238000002835 absorbance Methods 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 235000016520 artichoke thistle Nutrition 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 238000005341 cation exchange Methods 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 230000001066 destructive effect Effects 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 238000012869 ethanol precipitation Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 235000019211 fat replacer Nutrition 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 230000003311 flocculating effect Effects 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 235000004611 garlic Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 229940125396 insulin Drugs 0.000 description 1
- 239000004026 insulin derivative Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000013541 low molecular weight contaminant Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 238000011169 microbiological contamination Methods 0.000 description 1
- 238000000569 multi-angle light scattering Methods 0.000 description 1
- 238000001728 nano-filtration Methods 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 230000008635 plant growth Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000002390 rotary evaporation Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000002560 therapeutic procedure Methods 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 229920003169 water-soluble polymer Polymers 0.000 description 1
- -1 α-D-glucopyranosyl residue Chemical group 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0003—General processes for their isolation or fractionation, e.g. purification or extraction from biomass
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
- C08B37/0051—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid beta-D-Fructofuranans, e.g. beta-2,6-D-fructofuranan, i.e. levan; Derivatives thereof
- C08B37/0054—Inulin, i.e. beta-2,1-D-fructofuranan; Derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Molecular Biology (AREA)
- Organic Chemistry (AREA)
- Sustainable Development (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Extraction Or Liquid Replacement (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US1110496P | 1996-02-05 | 1996-02-05 | |
| US08/783,085 US5968365A (en) | 1996-02-05 | 1997-01-15 | Preparation of inulin products |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO970490D0 NO970490D0 (no) | 1997-02-04 |
| NO970490L NO970490L (no) | 1997-08-06 |
| NO324884B1 true NO324884B1 (no) | 2007-12-27 |
Family
ID=26682005
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO19970490A NO324884B1 (no) | 1996-02-05 | 1997-02-04 | Fremgangsmate for separering av vandige inulinopplosninger som inneholder karbohydrater i fraksjoner som har forskjellige gjennomsnittlige polymerisasjonsgrader |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US5968365A (de) |
| EP (1) | EP0787745B1 (de) |
| JP (1) | JP4916600B2 (de) |
| KR (1) | KR100528551B1 (de) |
| AR (1) | AR005705A1 (de) |
| AT (1) | ATE257846T1 (de) |
| AU (1) | AU718769B2 (de) |
| CA (1) | CA2196739C (de) |
| DE (1) | DE69727162T2 (de) |
| DK (1) | DK0787745T3 (de) |
| ES (1) | ES2214589T3 (de) |
| HU (1) | HUP9700359A3 (de) |
| MX (1) | MX9700916A (de) |
| NO (1) | NO324884B1 (de) |
| NZ (1) | NZ314187A (de) |
| PT (1) | PT787745E (de) |
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PT975236E (pt) | 1997-04-18 | 2005-01-31 | Mcneil Ppc Inc | Sucedaneo de acucar contendo fibras agradavel ao paladar e baixo em calorias |
| US6203797B1 (en) * | 1998-01-06 | 2001-03-20 | Stephen C. Perry | Dietary supplement and method for use as a probiotic, for alleviating the symptons associated with irritable bowel syndrome |
| EP0930317A1 (de) * | 1998-01-21 | 1999-07-21 | Tiense Suikerraffinaderij N.V. (Raffinerie Tirlemontoise S.A.) | Verfahren zur Herstellung von Inulin aus Chicorée, Inulinhydrolysate und Derivate, Produkte, Hydrolysate und Derivate von Chicorée-Inulin |
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| SU487118A1 (ru) * | 1973-03-05 | 1975-10-05 | Киевский Технологический Институт Пищевой Промышленности | Способ получени инулина |
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| DE4316425C2 (de) * | 1993-05-17 | 1998-05-20 | Suedzucker Ag | Verfahren zur Herstellung von langkettigem Inulin, das so hergestellte Inulin sowie dessen Verwendung |
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-
1997
- 1997-01-15 US US08/783,085 patent/US5968365A/en not_active Expired - Lifetime
- 1997-02-03 AU AU12495/97A patent/AU718769B2/en not_active Ceased
- 1997-02-04 EP EP97300678A patent/EP0787745B1/de not_active Expired - Lifetime
- 1997-02-04 NZ NZ314187A patent/NZ314187A/xx not_active IP Right Cessation
- 1997-02-04 ES ES97300678T patent/ES2214589T3/es not_active Expired - Lifetime
- 1997-02-04 AT AT97300678T patent/ATE257846T1/de active
- 1997-02-04 PT PT97300678T patent/PT787745E/pt unknown
- 1997-02-04 DK DK97300678T patent/DK0787745T3/da active
- 1997-02-04 MX MX9700916A patent/MX9700916A/es unknown
- 1997-02-04 DE DE69727162T patent/DE69727162T2/de not_active Expired - Lifetime
- 1997-02-04 CA CA002196739A patent/CA2196739C/en not_active Expired - Fee Related
- 1997-02-04 NO NO19970490A patent/NO324884B1/no not_active IP Right Cessation
- 1997-02-04 JP JP03428197A patent/JP4916600B2/ja not_active Expired - Fee Related
- 1997-02-04 AR ARP970100441A patent/AR005705A1/es active IP Right Grant
- 1997-02-05 HU HU9700359A patent/HUP9700359A3/hu unknown
- 1997-02-05 KR KR1019970003461A patent/KR100528551B1/ko not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| CA2196739C (en) | 2005-09-27 |
| NO970490L (no) | 1997-08-06 |
| ATE257846T1 (de) | 2004-01-15 |
| NO970490D0 (no) | 1997-02-04 |
| DK0787745T3 (da) | 2004-05-03 |
| MX9700916A (es) | 1998-04-30 |
| AR005705A1 (es) | 1999-07-14 |
| AU1249597A (en) | 1997-08-14 |
| JPH09324002A (ja) | 1997-12-16 |
| EP0787745A3 (de) | 1998-05-06 |
| DE69727162T2 (de) | 2004-08-26 |
| KR19980067429A (ko) | 1998-10-15 |
| PT787745E (pt) | 2004-05-31 |
| DE69727162D1 (de) | 2004-02-19 |
| HUP9700359A3 (en) | 2000-05-29 |
| HUP9700359A2 (hu) | 1998-03-30 |
| US5968365A (en) | 1999-10-19 |
| HU9700359D0 (en) | 1997-03-28 |
| JP4916600B2 (ja) | 2012-04-11 |
| KR100528551B1 (ko) | 2006-03-22 |
| NZ314187A (en) | 1999-01-28 |
| EP0787745A2 (de) | 1997-08-06 |
| AU718769B2 (en) | 2000-04-20 |
| CA2196739A1 (en) | 1997-08-06 |
| ES2214589T3 (es) | 2004-09-16 |
| EP0787745B1 (de) | 2004-01-14 |
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