NO123757B - - Google Patents
Download PDFInfo
- Publication number
- NO123757B NO123757B NO166726A NO16672667A NO123757B NO 123757 B NO123757 B NO 123757B NO 166726 A NO166726 A NO 166726A NO 16672667 A NO16672667 A NO 16672667A NO 123757 B NO123757 B NO 123757B
- Authority
- NO
- Norway
- Prior art keywords
- parts
- weight
- bis
- hydrogen chloride
- cyclohexane
- Prior art date
Links
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 claims description 25
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 24
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims description 24
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 24
- 125000005587 carbonate group Chemical group 0.000 claims description 17
- YIMQCDZDWXUDCA-UHFFFAOYSA-N [4-(hydroxymethyl)cyclohexyl]methanol Chemical compound OCC1CCC(CO)CC1 YIMQCDZDWXUDCA-UHFFFAOYSA-N 0.000 claims description 16
- 239000011541 reaction mixture Substances 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 13
- 150000002009 diols Chemical class 0.000 claims description 10
- 238000002360 preparation method Methods 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 7
- 239000012442 inert solvent Substances 0.000 claims description 5
- 239000011261 inert gas Substances 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 48
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 20
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 19
- 238000003756 stirring Methods 0.000 description 17
- 238000004519 manufacturing process Methods 0.000 description 11
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 10
- 229910052757 nitrogen Inorganic materials 0.000 description 10
- 239000002904 solvent Substances 0.000 description 10
- 239000013557 residual solvent Substances 0.000 description 9
- 239000000203 mixture Substances 0.000 description 8
- 238000010438 heat treatment Methods 0.000 description 7
- 239000002253 acid Substances 0.000 description 6
- -1 aliphatic diols Chemical class 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 5
- 150000002148 esters Chemical class 0.000 description 5
- 239000004417 polycarbonate Substances 0.000 description 5
- 229920000515 polycarbonate Polymers 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
- 125000004965 chloroalkyl group Chemical group 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 238000006068 polycondensation reaction Methods 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 2
- 239000000370 acceptor Substances 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 150000001805 chlorine compounds Chemical class 0.000 description 2
- NEHMKBQYUWJMIP-UHFFFAOYSA-N chloromethane Chemical compound ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 229920002635 polyurethane Polymers 0.000 description 2
- 239000004814 polyurethane Substances 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 239000012429 reaction media Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 239000008096 xylene Substances 0.000 description 2
- QRMPKOFEUHIBNM-UHFFFAOYSA-N 1,4-dimethylcyclohexane Chemical group CC1CCC(C)CC1 QRMPKOFEUHIBNM-UHFFFAOYSA-N 0.000 description 1
- 238000012696 Interfacial polycondensation Methods 0.000 description 1
- 229920001328 Polyvinylidene chloride Polymers 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 238000010533 azeotropic distillation Methods 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- WSJCBMAHJRRJRX-UHFFFAOYSA-N carbonic acid;[4-(hydroxymethyl)cyclohexyl]methanol Chemical compound OC(O)=O.OCC1CCC(CO)CC1 WSJCBMAHJRRJRX-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229940059864 chlorine containing product ectoparasiticides Drugs 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 125000005442 diisocyanate group Chemical group 0.000 description 1
- 238000000921 elemental analysis Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 229920001291 polyvinyl halide Polymers 0.000 description 1
- 239000005033 polyvinylidene chloride Substances 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/02—Aliphatic polycarbonates
- C08G64/0208—Aliphatic polycarbonates saturated
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C68/00—Preparation of esters of carbonic or haloformic acids
- C07C68/02—Preparation of esters of carbonic or haloformic acids from phosgene or haloformates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
- C08G18/3203—Polyhydroxy compounds
- C08G18/3212—Polyhydroxy compounds containing cycloaliphatic groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/42—Polycondensates having carboxylic or carbonic ester groups in the main chain
- C08G18/44—Polycarbonates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Polyesters Or Polycarbonates (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEC0038191 | 1966-02-11 | ||
| DEC0040189 | 1966-09-24 | ||
| DEC0040188 | 1966-09-24 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO123757B true NO123757B (fr) | 1972-01-10 |
Family
ID=27209603
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO166726A NO123757B (fr) | 1966-02-11 | 1967-02-06 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US3631200A (fr) |
| BE (1) | BE693956A (fr) |
| CH (1) | CH472358A (fr) |
| DE (3) | DE1568248A1 (fr) |
| FR (1) | FR1509851A (fr) |
| GB (1) | GB1169072A (fr) |
| NL (1) | NL6702063A (fr) |
| NO (1) | NO123757B (fr) |
| SE (1) | SE325025B (fr) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1695513C3 (de) * | 1966-12-10 | 1974-12-19 | Chemische Werke Huels Ag, 4370 Marl | Verfahren zur Herstellung von schlagfesten, elastisch und harten Überzügen |
| FR2247483B1 (fr) * | 1973-10-16 | 1976-06-18 | Poudres & Explosifs Ste Nale | |
| US4089888A (en) * | 1976-07-12 | 1978-05-16 | Idemitsu Petrochemical Co. Ltd. | Method for producing a polycarbonate oligomer |
| JPS53138446A (en) * | 1977-05-10 | 1978-12-02 | Adeka Argus Chem Co Ltd | Resin composition |
| DE19513164A1 (de) * | 1995-04-07 | 1996-10-10 | Bayer Ag | Polycarbonat-Diole, ihre Herstellung und Verwendung als Ausgangsprodukte für Polyurethan-Kunststoffe |
| DE19900554A1 (de) * | 1999-01-09 | 2000-07-13 | Bayer Ag | Verfahren zur Herstellung von aliphatischen Oligocarbonatdiolen aus Dimethylcarbonat und aliphatischen Diolen |
| KR100520185B1 (ko) * | 1999-10-11 | 2005-10-10 | 주식회사 하이닉스반도체 | 신규한 포토레지스트 중합체 및 이를 함유하는 포토레지스트 조성물 |
| DE10027907A1 (de) | 2000-06-06 | 2001-12-13 | Bayer Ag | Verfahren zur Herstellung von aliphatischen Oligocarbanatdiolen |
| US7112693B2 (en) * | 2001-06-27 | 2006-09-26 | Bayer Aktiengesellschaft | Process for producing aliphatic oligocarbonate diols |
| DE10130882A1 (de) | 2001-06-27 | 2003-01-16 | Bayer Ag | Verfahren zur Herstellung von aliphatischen Oligocarbonatdiolen |
| DE10156896A1 (de) * | 2001-11-20 | 2003-05-28 | Bayer Ag | Verwendung von Katalysatoren zur Herstellung von aliphatischen Oligocarbonatpolyolen |
| DE10303881A1 (de) * | 2003-01-31 | 2004-08-12 | Bayer Ag | Verfahren zur Herstellung von oligomeren aliphatischen Diolen, darauf basierenden Polycarbonatdiolen und deren Prepolymeren |
| DE10321149A1 (de) * | 2003-05-12 | 2004-12-02 | Bayer Materialscience Ag | Ytterbium(III)acetylacetonat als Katalysator zur Herstellung von aliphatischen Oligocarbonatpolyolen |
| DE102004042843A1 (de) * | 2004-09-04 | 2006-03-09 | Bayer Materialscience Ag | Metallacetylacetonate als Umesterungskatalysatoren |
| DE102005011448A1 (de) * | 2005-03-12 | 2006-09-21 | Bayer Materialscience Ag | Poly(urethancarbonat)polyole |
| DE102005018691A1 (de) * | 2005-04-22 | 2006-10-26 | Bayer Materialscience Ag | Niederviskose Oligocarbonatpolyole |
| DE102006002154A1 (de) * | 2006-01-17 | 2007-07-19 | Bayer Materialscience Ag | Polyurethan-Polyharnstoff-Beschichtungen |
| DE102006002156A1 (de) * | 2006-01-17 | 2007-07-19 | Bayer Materialscience Ag | Polyurethan-Polyharnstoff-Dispersionen auf Basis von Polyether-Polycarbonat-Polyolen |
| KR101820988B1 (ko) * | 2010-04-14 | 2018-03-08 | 다우 글로벌 테크놀로지스 엘엘씨 | 폴리카르보네이트 폴리올 및 그로부터 제조된 폴리우레탄 |
| TWI761404B (zh) | 2016-12-19 | 2022-04-21 | 德商科思創德意志股份有限公司 | 製備具有低反應性（環）脂族聚碳酸酯多元醇之方法 |
| EP4378972A1 (fr) | 2022-11-30 | 2024-06-05 | Covestro Deutschland AG | Composition de polyol de polycarbonate (cyclo)aliphatiques |
-
1966
- 1966-02-11 DE DE19661568248 patent/DE1568248A1/de active Pending
- 1966-09-24 DE DE1595446A patent/DE1595446C3/de not_active Expired
- 1966-09-24 DE DE1568333A patent/DE1568333C3/de not_active Expired
-
1967
- 1967-01-19 US US610230A patent/US3631200A/en not_active Expired - Lifetime
- 1967-02-02 FR FR93419A patent/FR1509851A/fr not_active Expired
- 1967-02-06 NO NO166726A patent/NO123757B/no unknown
- 1967-02-08 CH CH187167A patent/CH472358A/de not_active IP Right Cessation
- 1967-02-10 GB GB6387/67A patent/GB1169072A/en not_active Expired
- 1967-02-10 NL NL6702063A patent/NL6702063A/xx unknown
- 1967-02-10 SE SE1922/67A patent/SE325025B/xx unknown
- 1967-02-10 BE BE693956D patent/BE693956A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE693956A (fr) | 1967-07-17 |
| FR1509851A (fr) | 1968-01-12 |
| DE1568333A1 (de) | 1970-07-16 |
| DE1568333C3 (de) | 1974-11-07 |
| DE1595446A1 (de) | 1970-02-05 |
| DE1595446C3 (de) | 1975-03-13 |
| DE1568248A1 (de) | 1970-02-05 |
| DE1568333B2 (de) | 1974-02-21 |
| NL6702063A (fr) | 1967-08-14 |
| DE1595446B2 (de) | 1974-07-18 |
| CH472358A (de) | 1969-05-15 |
| GB1169072A (en) | 1969-10-29 |
| US3631200A (en) | 1971-12-28 |
| SE325025B (fr) | 1970-06-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| NO123757B (fr) | ||
| US3062781A (en) | Process for the production of polycarbonates | |
| KR102342167B1 (ko) | 고투명 고내열 폴리카보네이트 에스테르의 신규 제조방법 | |
| US3046255A (en) | Process for preparing polycarbonates | |
| US2943095A (en) | Process for preparing glycidyl polyethers of polyhydric phenols | |
| JP4732643B2 (ja) | カルボン酸ジアリールエステルの製造法 | |
| KR20010080259A (ko) | 방향족 폴리카보네이트를 제조하는 연속 계면 방법 | |
| JPS62187725A (ja) | ポリカ−ボネ−トジオ−ルの製造方法 | |
| EP0008492B1 (fr) | Procédé de préparation d'un polyester-polycarbonate aromatique | |
| US7122613B1 (en) | Method for the production of polycarbonates | |
| US3069385A (en) | Chain extending polycarbonate | |
| US3193529A (en) | Process for preparation of polycarbonates employing phosphonium catalysts | |
| US2384143A (en) | Vinyl esters | |
| EP0031975B1 (fr) | Composition de peroxydicarbonate et son utilisation pour polymériser des composés à insaturation éthylénique | |
| US3248365A (en) | Non-crystalline polycarbonate prepared from alpha, alpha'-bis(p-hydroxyphenyl)-p-xylene | |
| US2983749A (en) | Preparation of benzyl carbonates | |
| JPH032216A (ja) | 低割合のホスゲンを使用するオリゴマー状カーボネートビスクロルホルメートの製造法 | |
| US3000909A (en) | Process of preparing butylene oxide from butylene chlorohydrin | |
| DE2546717A1 (de) | Verfahren zur herstellung von polykarbonaten | |
| US2532036A (en) | Process of preparing polyhydric alcohols | |
| US3414542A (en) | Polycarbonates | |
| US2916521A (en) | Substituted styrenes | |
| US3152174A (en) | Manufacture of monochloroacetic acid | |
| US3062799A (en) | 2-(2, 2, 2-trifluoroethoxy)-butadiene and polymers thereof | |
| DE1199499B (de) | Verfahren zur Herstellung von hochpolymeren Mischpolycarbonaten |