NO119633B - - Google Patents
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- Publication number
- NO119633B NO119633B NO166696A NO16669667A NO119633B NO 119633 B NO119633 B NO 119633B NO 166696 A NO166696 A NO 166696A NO 16669667 A NO16669667 A NO 16669667A NO 119633 B NO119633 B NO 119633B
- Authority
- NO
- Norway
- Prior art keywords
- extract
- acid
- cation exchanger
- alcohol
- extraction
- Prior art date
Links
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 32
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 30
- NOESYZHRGYRDHS-UHFFFAOYSA-N insulin Chemical compound N1C(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(NC(=O)CN)C(C)CC)CSSCC(C(NC(CO)C(=O)NC(CC(C)C)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CCC(N)=O)C(=O)NC(CC(C)C)C(=O)NC(CCC(O)=O)C(=O)NC(CC(N)=O)C(=O)NC(CC=2C=CC(O)=CC=2)C(=O)NC(CSSCC(NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2C=CC(O)=CC=2)NC(=O)C(CC(C)C)NC(=O)C(C)NC(=O)C(CCC(O)=O)NC(=O)C(C(C)C)NC(=O)C(CC(C)C)NC(=O)C(CC=2NC=NC=2)NC(=O)C(CO)NC(=O)CNC2=O)C(=O)NCC(=O)NC(CCC(O)=O)C(=O)NC(CCCNC(N)=N)C(=O)NCC(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC=CC=3)C(=O)NC(CC=3C=CC(O)=CC=3)C(=O)NC(C(C)O)C(=O)N3C(CCC3)C(=O)NC(CCCCN)C(=O)NC(C)C(O)=O)C(=O)NC(CC(N)=O)C(O)=O)=O)NC(=O)C(C(C)CC)NC(=O)C(CO)NC(=O)C(C(C)O)NC(=O)C1CSSCC2NC(=O)C(CC(C)C)NC(=O)C(NC(=O)C(CCC(N)=O)NC(=O)C(CC(N)=O)NC(=O)C(NC(=O)C(N)CC=1C=CC=CC=1)C(C)C)CC1=CN=CN1 NOESYZHRGYRDHS-UHFFFAOYSA-N 0.000 claims description 24
- 239000000284 extract Substances 0.000 claims description 21
- 239000000783 alginic acid Substances 0.000 claims description 13
- 229960001126 alginic acid Drugs 0.000 claims description 13
- 235000010443 alginic acid Nutrition 0.000 claims description 13
- 229920000615 alginic acid Polymers 0.000 claims description 13
- 150000004781 alginic acids Chemical class 0.000 claims description 13
- 238000000605 extraction Methods 0.000 claims description 13
- 102000004877 Insulin Human genes 0.000 claims description 12
- 108090001061 Insulin Proteins 0.000 claims description 12
- 150000001768 cations Chemical class 0.000 claims description 12
- 229940125396 insulin Drugs 0.000 claims description 12
- 210000004907 gland Anatomy 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 11
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 9
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 4
- -1 ammonium ions Chemical class 0.000 claims description 4
- 230000007935 neutral effect Effects 0.000 claims description 4
- 229910021529 ammonia Inorganic materials 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 150000003839 salts Chemical class 0.000 claims description 3
- QCVGEOXPDFCNHA-UHFFFAOYSA-N 5,5-dimethyl-2,4-dioxo-1,3-oxazolidine-3-carboxamide Chemical compound CC1(C)OC(=O)N(C(N)=O)C1=O QCVGEOXPDFCNHA-UHFFFAOYSA-N 0.000 claims description 2
- 102000002322 Egg Proteins Human genes 0.000 claims description 2
- 108010000912 Egg Proteins Proteins 0.000 claims description 2
- 229920002230 Pectic acid Polymers 0.000 claims description 2
- 235000014103 egg white Nutrition 0.000 claims description 2
- 210000000969 egg white Anatomy 0.000 claims description 2
- 239000012535 impurity Substances 0.000 claims description 2
- LCLHHZYHLXDRQG-ZNKJPWOQSA-N pectic acid Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)O[C@H](C(O)=O)[C@@H]1OC1[C@H](O)[C@@H](O)[C@@H](OC2[C@@H]([C@@H](O)[C@@H](O)[C@H](O2)C(O)=O)O)[C@@H](C(O)=O)O1 LCLHHZYHLXDRQG-ZNKJPWOQSA-N 0.000 claims description 2
- 239000010318 polygalacturonic acid Substances 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- 235000019441 ethanol Nutrition 0.000 description 22
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 14
- 150000002500 ions Chemical class 0.000 description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 238000003756 stirring Methods 0.000 description 8
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 6
- 238000005119 centrifugation Methods 0.000 description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 238000010828 elution Methods 0.000 description 6
- 235000002639 sodium chloride Nutrition 0.000 description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 5
- 229960000583 acetic acid Drugs 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 210000000496 pancreas Anatomy 0.000 description 4
- 239000002244 precipitate Substances 0.000 description 4
- 239000011780 sodium chloride Substances 0.000 description 4
- 239000012153 distilled water Substances 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 150000007524 organic acids Chemical class 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- 241000283690 Bos taurus Species 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 244000309466 calf Species 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 235000006408 oxalic acid Nutrition 0.000 description 2
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- DPEYHNFHDIXMNV-UHFFFAOYSA-N (9-amino-3-bicyclo[3.3.1]nonanyl)-(4-benzyl-5-methyl-1,4-diazepan-1-yl)methanone dihydrochloride Chemical compound Cl.Cl.CC1CCN(CCN1Cc1ccccc1)C(=O)C1CC2CCCC(C1)C2N DPEYHNFHDIXMNV-UHFFFAOYSA-N 0.000 description 1
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 241000283086 Equidae Species 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 241000282887 Suidae Species 0.000 description 1
- 239000012675 alcoholic extract Substances 0.000 description 1
- 230000003178 anti-diabetic effect Effects 0.000 description 1
- 239000003472 antidiabetic agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000011083 clear filtration Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 230000000762 glandular Effects 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 229940093915 gynecological organic acid Drugs 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Natural products OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/01—Recovery of luminescent materials
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F17/00—Compounds of rare earth metals
- C01F17/10—Preparation or treatment, e.g. separation or purification
- C01F17/17—Preparation or treatment, e.g. separation or purification involving a liquid-liquid extraction
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F17/00—Compounds of rare earth metals
- C01F17/20—Compounds containing only rare earth metals as the metal element
- C01F17/253—Halides
- C01F17/271—Chlorides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F17/00—Compounds of rare earth metals
- C01F17/20—Compounds containing only rare earth metals as the metal element
- C01F17/276—Nitrates
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Analytical Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Extraction Or Liquid Replacement (AREA)
- Peptides Or Proteins (AREA)
- Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NO312968A NO120189B (en, 2012) | 1966-02-04 | 1968-08-08 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB495266A GB1180921A (en) | 1966-02-04 | 1966-02-04 | Improvements in Separation Procedures. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO119633B true NO119633B (en, 2012) | 1970-06-15 |
Family
ID=9786979
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO166696A NO119633B (en, 2012) | 1966-02-04 | 1967-02-03 |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US3514267A (en, 2012) |
| JP (1) | JPS505129B1 (en, 2012) |
| AT (2) | AT280210B (en, 2012) |
| BE (1) | BE693515A (en, 2012) |
| CH (1) | CH529578A (en, 2012) |
| DE (1) | DE1592177C3 (en, 2012) |
| ES (1) | ES336406A1 (en, 2012) |
| FI (1) | FI47587C (en, 2012) |
| FR (1) | FR1514428A (en, 2012) |
| GB (1) | GB1180921A (en, 2012) |
| MY (1) | MY7100075A (en, 2012) |
| NL (1) | NL143877B (en, 2012) |
| NO (1) | NO119633B (en, 2012) |
| SE (2) | SE359569B (en, 2012) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA902932A (en) * | 1970-02-03 | 1972-06-20 | Her Majesty The Queen, In Right Of Canada As Represented By The Minister Of Natural Resources Canada | Liquid-liquid separation of cobalt from ammoniacal solutions |
| US3640678A (en) * | 1970-06-01 | 1972-02-08 | Molybdenum Corp | Yttrium purification process |
| US3615171A (en) * | 1970-06-15 | 1971-10-26 | George W Mason | Process of separating yttrium from lanthanide rare earths |
| JPS5545495B2 (en, 2012) * | 1972-09-27 | 1980-11-18 | ||
| JPS52144535U (en, 2012) * | 1976-04-27 | 1977-11-01 | ||
| FR2617829A1 (fr) * | 1987-07-10 | 1989-01-13 | Rhone Poulenc Chimie | Procede de separation des terres rares par extraction liquide-liquide mettant en oeuvre des diluants halogenes ou du type acides carboxyliques |
| US6544442B1 (en) * | 1999-09-22 | 2003-04-08 | Ut-Battelle, Llc | Method of loading organic materials with group III plus lanthanide and actinide elements |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2955913A (en) * | 1953-03-27 | 1960-10-11 | Donald F Peppard | Separation of rare earths by solvent extraction |
| US2798789A (en) * | 1954-02-11 | 1957-07-09 | Frank H Spedding | Method of separating rare earths |
| US3387944A (en) * | 1961-09-12 | 1968-06-11 | Thorium Ltd | Batch separation of components of a mixture by total solute reflux |
| BE635283A (en, 2012) * | 1961-09-14 | 1900-01-01 | ||
| US3328116A (en) * | 1963-10-09 | 1967-06-27 | Dow Chemical Co | Solvent extraction process for the recovery of be-values |
| FR1382467A (fr) * | 1964-01-28 | 1964-12-18 | Atomic Energy Authority Uk | Procédé d'extraction par solvant |
| US3323857A (en) * | 1965-12-16 | 1967-06-06 | Donald J Bauer | Selective extraction and separation of lanthanides with a quaternary ammonium compound |
-
1966
- 1966-02-04 GB GB495266A patent/GB1180921A/en not_active Expired
-
1967
- 1967-01-28 DE DE1592177A patent/DE1592177C3/de not_active Expired
- 1967-01-30 JP JP565667A patent/JPS505129B1/ja active Pending
- 1967-01-30 NL NL6701417A patent/NL143877B/xx unknown
- 1967-02-01 BE BE693515D patent/BE693515A/xx unknown
- 1967-02-01 FR FR93376A patent/FR1514428A/fr not_active Expired
- 1967-02-02 US US3514267D patent/US3514267A/en not_active Expired - Lifetime
- 1967-02-03 NO NO166696A patent/NO119633B/no unknown
- 1967-02-03 SE SE1299568A patent/SE359569B/xx unknown
- 1967-02-03 AT AT706968A patent/AT280210B/de not_active IP Right Cessation
- 1967-02-03 CH CH161967A patent/CH529578A/fr not_active IP Right Cessation
- 1967-02-03 AT AT105367A patent/AT278703B/de not_active IP Right Cessation
- 1967-02-03 ES ES0336406A patent/ES336406A1/es not_active Expired
- 1967-02-03 SE SE158967A patent/SE321581B/xx unknown
- 1967-02-04 FI FI32267A patent/FI47587C/fi active
-
1971
- 1971-12-31 MY MY7100075A patent/MY7100075A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BE693515A (en, 2012) | 1967-07-17 |
| US3514267A (en) | 1970-05-26 |
| NL143877B (nl) | 1974-11-15 |
| MY7100075A (en) | 1971-12-31 |
| SE359569B (en, 2012) | 1973-09-03 |
| FR1514428A (fr) | 1968-02-23 |
| DE1592177A1 (de) | 1972-02-03 |
| NL6701417A (en, 2012) | 1967-08-07 |
| ES336406A1 (es) | 1967-12-16 |
| AT280210B (de) | 1970-04-10 |
| FI47587B (en, 2012) | 1973-10-01 |
| JPS505129B1 (en, 2012) | 1975-02-28 |
| GB1180921A (en) | 1970-02-11 |
| AT278703B (de) | 1970-02-10 |
| FI47587C (fi) | 1974-01-10 |
| DE1592177B2 (de) | 1974-09-05 |
| DE1592177C3 (de) | 1975-05-15 |
| SE321581B (en, 2012) | 1970-03-09 |
| CH529578A (fr) | 1972-10-31 |
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