NL7909081A - Werkwijze voor de bereiding van l-lysinecarbamaat. - Google Patents
Werkwijze voor de bereiding van l-lysinecarbamaat. Download PDFInfo
- Publication number
- NL7909081A NL7909081A NL7909081A NL7909081A NL7909081A NL 7909081 A NL7909081 A NL 7909081A NL 7909081 A NL7909081 A NL 7909081A NL 7909081 A NL7909081 A NL 7909081A NL 7909081 A NL7909081 A NL 7909081A
- Authority
- NL
- Netherlands
- Prior art keywords
- lysine
- carbamate
- carbon dioxide
- filtrate
- filtered
- Prior art date
Links
- XFQCPHGOMQULNH-JEDNCBNOSA-N carbamic acid;(2s)-2,6-diaminohexanoic acid Chemical compound NC(O)=O.NCCCC[C@H](N)C(O)=O XFQCPHGOMQULNH-JEDNCBNOSA-N 0.000 title claims description 12
- 238000002360 preparation method Methods 0.000 title claims description 9
- 238000000034 method Methods 0.000 title claims description 8
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 24
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 20
- KDXKERNSBIXSRK-YFKPBYRVSA-N L-lysine Chemical compound NCCCC[C@H](N)C(O)=O KDXKERNSBIXSRK-YFKPBYRVSA-N 0.000 claims description 16
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 9
- 235000019766 L-Lysine Nutrition 0.000 claims description 8
- 239000004472 Lysine Substances 0.000 claims description 8
- 239000001569 carbon dioxide Substances 0.000 claims description 8
- 239000000706 filtrate Substances 0.000 claims description 7
- 239000002244 precipitate Substances 0.000 claims description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- 239000000047 product Substances 0.000 claims description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 3
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 2
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- 229940072033 potash Drugs 0.000 claims description 2
- 235000015320 potassium carbonate Nutrition 0.000 claims description 2
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 claims 2
- 238000004042 decolorization Methods 0.000 claims 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 229940079593 drug Drugs 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 239000003826 tablet Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- 239000007938 effervescent tablet Substances 0.000 description 2
- BSYNRYMUTXBXSQ-FOQJRBATSA-N 59096-14-9 Chemical compound CC(=O)OC1=CC=CC=C1[14C](O)=O BSYNRYMUTXBXSQ-FOQJRBATSA-N 0.000 description 1
- BSYNRYMUTXBXSQ-UHFFFAOYSA-N Aspirin Chemical compound CC(=O)OC1=CC=CC=C1C(O)=O BSYNRYMUTXBXSQ-UHFFFAOYSA-N 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 229960001138 acetylsalicylic acid Drugs 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- MHJAJDCZWVHCPF-UHFFFAOYSA-L dimagnesium phosphate Chemical compound [Mg+2].OP([O-])([O-])=O MHJAJDCZWVHCPF-UHFFFAOYSA-L 0.000 description 1
- 229910000395 dimagnesium phosphate Inorganic materials 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229940068517 fruit extracts Drugs 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 1
- 235000014659 low sodium diet Nutrition 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000007968 orange flavor Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/60—Salicylic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
- A23L2/40—Effervescence-generating compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/325—Carbamic acids; Thiocarbamic acids; Anhydrides or salts thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/60—Salicylic acid; Derivatives thereof
- A61K31/618—Salicylic acid; Derivatives thereof having the carboxyl group in position 1 esterified, e.g. salsalate
- A61K31/621—Salicylic acid; Derivatives thereof having the carboxyl group in position 1 esterified, e.g. salsalate having the hydroxy group in position 2 esterified, e.g. benorylate
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0002—Galenical forms characterised by the drug release technique; Application systems commanded by energy
- A61K9/0007—Effervescent
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Public Health (AREA)
- Pharmacology & Pharmacy (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Nutrition Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Medicinal Preparation (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7836011 | 1978-12-21 | ||
| FR7836011A FR2444665B1 (fr) | 1978-12-21 | 1978-12-21 | Nouveau procede de preparation du carbamate de l-lysine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NL7909081A true NL7909081A (nl) | 1980-06-24 |
Family
ID=9216407
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NL7909081A NL7909081A (nl) | 1978-12-21 | 1979-12-17 | Werkwijze voor de bereiding van l-lysinecarbamaat. |
Country Status (9)
| Country | Link |
|---|---|
| JP (1) | JPS5587753A (enrdf_load_stackoverflow) |
| BE (1) | BE880749A (enrdf_load_stackoverflow) |
| DE (1) | DE2951132A1 (enrdf_load_stackoverflow) |
| ES (1) | ES487158A1 (enrdf_load_stackoverflow) |
| FR (1) | FR2444665B1 (enrdf_load_stackoverflow) |
| GB (1) | GB2037760B (enrdf_load_stackoverflow) |
| IT (1) | IT1119633B (enrdf_load_stackoverflow) |
| LU (1) | LU82007A1 (enrdf_load_stackoverflow) |
| NL (1) | NL7909081A (enrdf_load_stackoverflow) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4760138A (en) * | 1984-12-13 | 1988-07-26 | Nestec S. A. | Carbonating agents and their preparation |
| US4937083A (en) * | 1988-04-12 | 1990-06-26 | Mitsubishi Chemical Industries Limited | Feed additive for ruminants |
| FR3158966A1 (fr) | 2024-02-07 | 2025-08-08 | Universite Claude Bernard Lyon 1 | Procede de preparation d’un copolymere reticule et son utilisation comme materiau poreux |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2215950A2 (en) * | 1973-02-01 | 1974-08-30 | Union Pharma Scient Appl | Carbonated lysine - as carbonate source in effervescent compositions |
-
1978
- 1978-12-21 FR FR7836011A patent/FR2444665B1/fr not_active Expired
-
1979
- 1979-12-07 GB GB7942236A patent/GB2037760B/en not_active Expired
- 1979-12-17 JP JP16395479A patent/JPS5587753A/ja active Granted
- 1979-12-17 NL NL7909081A patent/NL7909081A/nl not_active Application Discontinuation
- 1979-12-18 LU LU82007A patent/LU82007A1/fr unknown
- 1979-12-19 DE DE19792951132 patent/DE2951132A1/de active Granted
- 1979-12-20 IT IT69447/79A patent/IT1119633B/it active
- 1979-12-20 ES ES487158A patent/ES487158A1/es not_active Expired
- 1979-12-20 BE BE2/58288A patent/BE880749A/fr not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DE2951132A1 (de) | 1980-07-10 |
| DE2951132C2 (enrdf_load_stackoverflow) | 1988-12-22 |
| BE880749A (fr) | 1980-06-20 |
| GB2037760A (en) | 1980-07-16 |
| LU82007A1 (fr) | 1980-07-21 |
| JPS5587753A (en) | 1980-07-02 |
| GB2037760B (en) | 1983-05-11 |
| ES487158A1 (es) | 1980-09-16 |
| IT1119633B (it) | 1986-03-10 |
| FR2444665B1 (fr) | 1985-06-28 |
| JPS6320220B2 (enrdf_load_stackoverflow) | 1988-04-26 |
| IT7969447A0 (it) | 1979-12-20 |
| FR2444665A1 (fr) | 1980-07-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP3014109B2 (ja) | 合成的ｇｔｆクロム物質及びその方法 | |
| Seifullina et al. | Design and synthesis of new homo-and heterometal coordination compounds of germanium (IV) for preparation of low toxic drugs with a wide therapeutic action | |
| JPH09503002A (ja) | 水溶性ニメスリド塩およびその製造、この塩を含む水溶液、ニメスリドを主体とする配合物およびそれらの使用 | |
| EP1569943A1 (en) | Method for preparation of amino acid chelate | |
| US5863939A (en) | Creatine ascorbates and a method of producing them | |
| CN101606715A (zh) | 一种不含干扰阴离子的食品级氨基酸亚铁螯合物的制备方法 | |
| MX2010014466A (es) | Composicion a base de flavanolignano y metodos para su preparacion. | |
| KR0143232B1 (ko) | 철 공급용 제제, 비타민 공급용 제제 및 발포 제제의 안정화 방법 | |
| JP5290975B2 (ja) | Ｌ−カルニチンフマル酸カルシウム及びその製造方法と用途 | |
| NL7909081A (nl) | Werkwijze voor de bereiding van l-lysinecarbamaat. | |
| CA2085523A1 (en) | Water soluble derivatives of biotin and related therapeutical compositions | |
| FI83879C (fi) | Aminosocker-karboneringsaemnen och deras framstaellning. | |
| US3361769A (en) | Bi-metallic salts of gluconic, glucuronic, or galacturonic acid | |
| NL8403782A (nl) | Werkwijze voor de bereiding van een heminecomplex en de therapeutische toepassing hiervan. | |
| JPH05238940A (ja) | 生体への吸収率の高い速効用薬剤及びその製造方法 | |
| FI71314C (fi) | Foerfarande foer framstaellning av en terapeutiskt anvaendbar beta-(4,5-difenyloxazol-2-yl) propionsyrakalciumsalt | |
| JP2022500507A (ja) | クエン酸及びアルギニンリガンド含有亜鉛錯化合物 | |
| JP6648700B2 (ja) | 溶解性の高いアセトン付加ピロロキノリンキノン塩 | |
| CN1523983A (zh) | 制备3-羟基-3-甲基丁酸钠固体制剂的方法 | |
| Wisniak | Paul schützenberger | |
| JPH09263573A (ja) | テアニンの製造方法 | |
| QUÉRÉ | Monographs of most frequent co-crystal formers | |
| JP2986133B2 (ja) | ミネラル吸収促進剤 | |
| JPH05501103A (ja) | ビス―アシルオキシメチル誘導体 | |
| CN113826891A (zh) | 一种含复合维生素的组合物及其压片制备方法和用途 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A85 | Still pending on 85-01-01 | ||
| BA | A request for search or an international-type search has been filed | ||
| BB | A search report has been drawn up | ||
| BC | A request for examination has been filed | ||
| CNR | Transfer of rights (patent application after its laying open for public inspection) |
Free format text: BRU GEB. MAGNIEZ. NICOLE FRANCOISE - |
|
| BV | The patent application has lapsed |