MX2019008908A - Metodos para producir norbornilesteres del acido (met) acrilico. - Google Patents

Metodos para producir norbornilesteres del acido (met) acrilico.

Info

Publication number
MX2019008908A
MX2019008908A MX2019008908A MX2019008908A MX2019008908A MX 2019008908 A MX2019008908 A MX 2019008908A MX 2019008908 A MX2019008908 A MX 2019008908A MX 2019008908 A MX2019008908 A MX 2019008908A MX 2019008908 A MX2019008908 A MX 2019008908A
Authority
MX
Mexico
Prior art keywords
meth
acrylic acid
producing
methods
norbornyl
Prior art date
Application number
MX2019008908A
Other languages
English (en)
Inventor
Misske Andrea
Fleckenstein Christoph
Fleischhaker Friederike
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2019008908A publication Critical patent/MX2019008908A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/62—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/04—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/04—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds
    • C07C67/05—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds with oxidation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/36—Systems containing two condensed rings the rings having more than two atoms in common
    • C07C2602/40—Systems containing two condensed rings the rings having more than two atoms in common the bicyclo ring system containing six carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/36—Systems containing two condensed rings the rings having more than two atoms in common
    • C07C2602/42—Systems containing two condensed rings the rings having more than two atoms in common the bicyclo ring system containing seven carbon atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Un método para preparar norbornil (met)acrilato al hacer reaccionar norborneno con ácido (met)acrílico en presencia de trifluoruro de boro como catalizador, en donde e) se carga inicialmente el trifluoruro de boro en ácido (met)acrílico, f) se calienta la carga inicial hasta una temperatura de 75 a 110°C, g) se agrega norborneno y h) se aísla el norbornil (met)acrilato obtenido de la mezcla de reacción. Un método para preparar norbornil (met)acrilato al hacer reaccionar norborneno con ácido (met)acrílico en presencia de trifluoruro de boro como catalizador, en donde e) se carga inicialmente el trifluoruro de boro en un solvente orgánico, f) se calienta la carga inicial hasta una temperatura de 75 a 110°C, g) se agrega una mezcla que comprende norborneno y ácido (met)acrílico y h) se aísla el norbornil (met)acrilato obtenido de la mezcla de reacción.
MX2019008908A 2017-01-27 2018-01-22 Metodos para producir norbornilesteres del acido (met) acrilico. MX2019008908A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP17153566 2017-01-27
PCT/EP2018/051381 WO2018138025A1 (de) 2017-01-27 2018-01-22 Verfahren zur herstellung von (meth)acrylsäurenorbornylestern

Publications (1)

Publication Number Publication Date
MX2019008908A true MX2019008908A (es) 2019-09-13

Family

ID=57909543

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019008908A MX2019008908A (es) 2017-01-27 2018-01-22 Metodos para producir norbornilesteres del acido (met) acrilico.

Country Status (15)

Country Link
US (1) US11028040B2 (es)
EP (1) EP3573946B1 (es)
JP (1) JP6768973B2 (es)
KR (1) KR102112235B1 (es)
CN (1) CN110198925B (es)
AU (1) AU2018213816B2 (es)
BR (1) BR112019015152B1 (es)
CA (1) CA3050038C (es)
ES (1) ES2859667T3 (es)
MX (1) MX2019008908A (es)
MY (1) MY197504A (es)
RU (1) RU2730856C1 (es)
SG (1) SG11201906488RA (es)
WO (1) WO2018138025A1 (es)
ZA (1) ZA201905540B (es)

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1954548C3 (de) 1969-10-30 1975-11-13 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Dihydrodicyclopentadienylacrylat aus Dicyclopentadien und Acrylsäure in Gegenwart saurer Katalysatoren
US4319009A (en) * 1978-01-03 1982-03-09 The Dow Chemical Company Cycloaliphatic acrylate compositions
JPH03148239A (ja) 1989-11-02 1991-06-25 Mitsui Petrochem Ind Ltd カルボン酸多環式アルキルエステルの製造方法
JP4163400B2 (ja) * 2000-07-28 2008-10-08 三菱化学株式会社 （メタ）アクリル酸エステルの製造方法
JP2004210732A (ja) * 2003-01-06 2004-07-29 Fuji Photo Film Co Ltd 不飽和モノカルボン酸エステルの製造方法、光学部材用重合性組成物および光学部材
CN101010286A (zh) * 2004-08-19 2007-08-01 三菱化学株式会社 2－甲基金刚烷－2－基(甲基)丙烯酸酯的制造方法以及2－甲基金刚烷－2－基(甲基)丙烯酸酯
CN101348543B (zh) 2008-07-28 2011-01-26 北京大学 一种单体组合物的制备方法
CN102108051A (zh) * 2010-12-03 2011-06-29 上海博康精细化工有限公司 冰片烯酯及其制备方法
CN107428771B (zh) 2015-02-26 2020-06-12 巴斯夫欧洲公司 制备异山梨醇二(甲基)丙烯酸酯的方法
RU2702013C2 (ru) 2015-02-26 2019-10-03 Басф Се Способ получения изосорбидэтоксилатди(мет)акрилата
JP2018511492A (ja) 2015-03-03 2018-04-26 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ３ｄプリンティングによる三次元構造の製造方法
SG11201706614XA (en) 2015-03-03 2017-09-28 Basf Se Method for producing a tridimensional structure using two pre-supporting materials
TWI695848B (zh) 2015-03-03 2020-06-11 德商巴斯夫歐洲公司 銀奈米線與基於（甲基）丙烯酸酯之封端劑的合成
WO2016165979A1 (de) 2015-04-15 2016-10-20 Basf Se Dihydrooligocyclopentadienyl(meth)acrylate
ES2917178T3 (es) 2015-07-09 2022-07-07 Basf Se Composiciones curables
EP3322764B1 (de) 2015-07-16 2020-09-09 Basf Se Schmelzklebstoff, enthaltend poly(meth)acrylat aus alky(meth)acrylaten und aus bestimmten heterocyclische gruppen enthaltenden (meth)acrylaten
JP2019500362A (ja) 2015-12-15 2019-01-10 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ヒドロキシベンゾフェノンポリグリコールエーテル（メタ）アクリレートの製造方法
SG11201900007VA (en) 2016-08-05 2019-02-27 Basf Se Macromonomers containing polyisobutene groups, and homopolymers or copolymers thereof

Also Published As

Publication number Publication date
CA3050038A1 (en) 2018-08-02
KR102112235B1 (ko) 2020-05-19
KR20190094473A (ko) 2019-08-13
CA3050038C (en) 2020-06-09
EP3573946B1 (de) 2020-12-16
AU2018213816B2 (en) 2020-01-02
US11028040B2 (en) 2021-06-08
MY197504A (en) 2023-06-19
BR112019015152A2 (pt) 2020-03-24
JP6768973B2 (ja) 2020-10-14
US20200407309A1 (en) 2020-12-31
RU2730856C1 (ru) 2020-08-26
CN110198925B (zh) 2022-08-30
JP2020506185A (ja) 2020-02-27
BR112019015152B1 (pt) 2023-05-09
CN110198925A (zh) 2019-09-03
SG11201906488RA (en) 2019-08-27
AU2018213816A1 (en) 2019-08-22
ZA201905540B (en) 2021-05-26
EP3573946A1 (de) 2019-12-04
WO2018138025A1 (de) 2018-08-02
ES2859667T3 (es) 2021-10-04

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