BR112017018072A2 - processo para preparação de di(met)acrilato de isossorbida através da transesterificação de (met)acrilato de alquila com isossorbida, e, uso de di(met)acrilato de isossorbida. - Google Patents

processo para preparação de di(met)acrilato de isossorbida através da transesterificação de (met)acrilato de alquila com isossorbida, e, uso de di(met)acrilato de isossorbida.

Info

Publication number
BR112017018072A2
BR112017018072A2 BR112017018072-3A BR112017018072A BR112017018072A2 BR 112017018072 A2 BR112017018072 A2 BR 112017018072A2 BR 112017018072 A BR112017018072 A BR 112017018072A BR 112017018072 A2 BR112017018072 A2 BR 112017018072A2
Authority
BR
Brazil
Prior art keywords
meth
acrylate
isosorbide
alkyl
steps
Prior art date
Application number
BR112017018072-3A
Other languages
English (en)
Inventor
Misske Andrea
Fleischhaker Friederike
Fleckenstein Christoph
Kaller Martin
Nair Ritesh
Stengel Ulrik
Blanchot Mathieu
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of BR112017018072A2 publication Critical patent/BR112017018072A2/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D493/00—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system
    • C07D493/02—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system in which the condensed system contains two hetero rings
    • C07D493/04—Ortho-condensed systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C35/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
    • C07C35/22—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring polycyclic, at least one hydroxy group bound to a condensed ring system
    • C07C35/23—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring polycyclic, at least one hydroxy group bound to a condensed ring system with hydroxy on a condensed ring system having two rings
    • C07C35/24—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring polycyclic, at least one hydroxy group bound to a condensed ring system with hydroxy on a condensed ring system having two rings the condensed ring system containing five carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C61/00—Compounds having carboxyl groups bound to carbon atoms of rings other than six-membered aromatic rings
    • C07C61/16—Unsaturated compounds
    • C07C61/20—Unsaturated compounds having a carboxyl group bound to a five-membered ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/02—Preparation of carboxylic acid esters by interreacting ester groups, i.e. transesterification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F22/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical and containing at least one other carboxyl radical in the molecule; Salts, anhydrides, esters, amides, imides or nitriles thereof
    • C08F22/10—Esters
    • C08F22/12—Esters of phenols or saturated alcohols
    • C08F22/20—Esters containing oxygen in addition to the carboxy oxygen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/66—Polyesters containing oxygen in the form of ether groups
    • C08G63/668—Polyesters containing oxygen in the form of ether groups derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/672—Dicarboxylic acids and dihydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/426—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells for plugging
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/44—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing organic binders only

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

a invenção se refere ao processo para preparação de di(met)acrilato de isossorbida através da transesterificação de (met)acrilato de alquila com isossorbida compreendendo as etapas de: (i) permitir que o (met)acrilato de alquila reaja com isossorbida na presença de um catalisador que compreende titânio (iv) ou zircônio (iv) e um estabilizador na presença de um agente de arraste que forma um azeótropo com o álcool ligado no (met)acrilato de alquila, (ii) destilar continuamente o azeótropo que consiste em um agente de arraste e álcool, as etapas (i) e (ii) são conduzidas simultaneamente até o isossorbida ter sido essencialmente convertido completamente, (iii) adicionar água à mistura de produto que compreende (met)acrilato de isossorbida e é obtida nas etapas (i) e (ii) e remoção do hidrolisado do catalisador compreendendo titânio (iv) ou zircônio (iv), (iv) destilar o (met)acrilato de alquila não convertido e o agente de arraste para fora da mistura do produto, (v) destilar a água da mistura do produto, em que a etapa (iv) também pode ser conduzida antes da etapa (iii) e as etapas (iv) e (v) também podem ser conduzidas em uma etapa de destilação.
BR112017018072-3A 2015-02-26 2016-02-24 processo para preparação de di(met)acrilato de isossorbida através da transesterificação de (met)acrilato de alquila com isossorbida, e, uso de di(met)acrilato de isossorbida. BR112017018072A2 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201562120922P 2015-02-26 2015-02-26
US62/120922 2015-02-26
PCT/EP2016/053858 WO2016135191A1 (de) 2015-02-26 2016-02-24 Verfahren zur herstellung von isosorbiddi(meth)acrylat

Publications (1)

Publication Number Publication Date
BR112017018072A2 true BR112017018072A2 (pt) 2018-04-10

Family

ID=55436096

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112017018072-3A BR112017018072A2 (pt) 2015-02-26 2016-02-24 processo para preparação de di(met)acrilato de isossorbida através da transesterificação de (met)acrilato de alquila com isossorbida, e, uso de di(met)acrilato de isossorbida.

Country Status (14)

Country Link
US (1) US10370383B2 (pt)
EP (1) EP3262130B1 (pt)
JP (1) JP6789231B6 (pt)
KR (1) KR102572781B1 (pt)
CN (1) CN107428771B (pt)
AU (1) AU2016223466A1 (pt)
BR (1) BR112017018072A2 (pt)
CA (1) CA2976594A1 (pt)
ES (1) ES2847651T3 (pt)
MX (1) MX2017011022A (pt)
MY (1) MY185533A (pt)
RU (1) RU2703461C2 (pt)
SG (1) SG11201706500SA (pt)
WO (1) WO2016135191A1 (pt)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013066461A2 (en) 2011-08-10 2013-05-10 Palmese Giuseppe R Renewable bio-based (meth) acrylated monomers as vinyl ester cross-linkers
JP6762958B2 (ja) * 2015-04-03 2020-09-30 ヘンケル アイピー アンド ホールディング ゲゼルシャフト ミット ベシュレンクテル ハフツング 嫌気硬化性組成物
JP6813562B6 (ja) 2015-07-09 2021-02-10 ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ 硬化性組成物
WO2018098011A1 (en) * 2016-11-22 2018-05-31 Sadler Joshua Matthew Process to produce blended (meth)acrylate/vinyl ester resin cross-linkers
JP6768973B2 (ja) 2017-01-27 2020-10-14 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ （メタ）アクリル酸ノルボルニルエステルの製造方法
EP3489241A1 (de) * 2017-11-22 2019-05-29 Basf Se Verfahren zur synthese von isosorbidmono- und di-(meth)acrylat
EP3489205A1 (de) * 2017-11-28 2019-05-29 HILTI Aktiengesellschaft Isosorbidderivate als reaktive zusätze in reaktivharzen und chemischen dübeln
WO2021164893A1 (en) * 2020-02-20 2021-08-26 The University Of The Basque Country Method for producing a removable pressure-sensitive adhesive (psa) and pressure-sensitive adhesive thus produced

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DE2317226C3 (de) 1973-04-06 1980-10-30 Deutsche Texaco Ag, 2000 Hamburg Verfahren zur Herstellung von höhermolekularen Alkylacrylaten bzw. -methacrylaten
US4602073A (en) * 1985-06-07 1986-07-22 National Starch And Chemical Corporation Adhesive compositions
US4777265A (en) * 1986-03-11 1988-10-11 Basf Aktiengesellschaft Preparation of acrylates and methacrylates
DE4131458A1 (de) * 1991-09-21 1993-03-25 Basf Ag Zweikomponentenklebmasse fuer die chemische befestigungstechnik
JP4217425B2 (ja) * 2001-07-06 2009-02-04 日本乳化剤株式会社 新規な高分子電解質及びリチウム二次電池
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EP2139878A2 (en) * 2007-02-20 2010-01-06 Basf Se High refractive index monomers, compositions and uses thereof
WO2009080380A2 (en) * 2007-12-19 2009-07-02 Evonik Röhm Gmbh Process for preparing (meth)acrylates
DE102008040221A1 (de) * 2008-07-07 2010-01-14 Evonik Röhm Gmbh Verfahren zur Herstellung von (Meth)acrylsäureestern
JP5270510B2 (ja) * 2009-10-19 2013-08-21 第一工業製薬株式会社 環状（メタ）アクリレート化合物、その製造方法、及び樹脂組成物
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JP6190823B2 (ja) * 2012-01-23 2017-08-30 ヘンケル アイピー アンド ホールディング ゲゼルシャフト ミット ベシュレンクテル ハフツング 二液型シアノアクリレート／フリーラジカル硬化性接着剤システム
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Also Published As

Publication number Publication date
US20160251371A1 (en) 2016-09-01
ES2847651T3 (es) 2021-08-03
US10370383B2 (en) 2019-08-06
EP3262130A1 (de) 2018-01-03
RU2703461C2 (ru) 2019-10-17
KR20170124541A (ko) 2017-11-10
MX2017011022A (es) 2017-10-20
KR102572781B1 (ko) 2023-08-31
SG11201706500SA (en) 2017-09-28
AU2016223466A1 (en) 2017-09-07
JP2018511576A (ja) 2018-04-26
CA2976594A1 (en) 2016-09-01
JP6789231B2 (ja) 2020-11-25
RU2017133283A3 (pt) 2019-03-27
RU2017133283A (ru) 2019-03-27
JP6789231B6 (ja) 2020-12-16
MY185533A (en) 2021-05-19
WO2016135191A1 (de) 2016-09-01
EP3262130B1 (de) 2020-10-28
CN107428771A (zh) 2017-12-01
CN107428771B (zh) 2020-06-12

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Legal Events

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B11A Dismissal acc. art.33 of ipl - examination not requested within 36 months of filing
B11Y Definitive dismissal - extension of time limit for request of examination expired [chapter 11.1.1 patent gazette]