MX2010007376A - Metodo y reactor para la preparacion de metanol. - Google Patents
Metodo y reactor para la preparacion de metanol.Info
- Publication number
- MX2010007376A MX2010007376A MX2010007376A MX2010007376A MX2010007376A MX 2010007376 A MX2010007376 A MX 2010007376A MX 2010007376 A MX2010007376 A MX 2010007376A MX 2010007376 A MX2010007376 A MX 2010007376A MX 2010007376 A MX2010007376 A MX 2010007376A
- Authority
- MX
- Mexico
- Prior art keywords
- methanol
- reactor
- catalyst
- gaseous phase
- cooling surface
- Prior art date
Links
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0285—Heating or cooling the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
- B01J8/009—Membranes, e.g. feeding or removing reactants or products to or from the catalyst bed through a membrane
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0207—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal
- B01J8/0214—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid flow within the bed being predominantly horizontal in a cylindrical annular shaped bed
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/0292—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds with stationary packing material in the bed, e.g. bricks, wire rings, baffles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
- B01J8/065—Feeding reactive fluids
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
- B01J8/067—Heating or cooling the reactor
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
- C07C29/151—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases
- C07C29/152—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively with hydrogen or hydrogen-containing gases characterised by the reactor used
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/02—Monohydroxylic acyclic alcohols
- C07C31/04—Methanol
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
- B01J2208/00123—Fingers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
- B01J2208/00132—Tubes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
- B01J2208/0015—Plates; Cylinders
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
- B01J2208/00212—Plates; Jackets; Cylinders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
- B01J2219/00763—Baffles
- B01J2219/00765—Baffles attached to the reactor wall
- B01J2219/0077—Baffles attached to the reactor wall inclined
- B01J2219/00772—Baffles attached to the reactor wall inclined in a helix
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Fluid Mechanics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
Un diseño mejorado de un método y reactor catalítico para la producción de metanol en condiciones de equilibrio, con lo cual el metanol a medida que se forma es separado de la fase gaseosa en la fase líquida dentro del reactor sin reducir la actividad catalítica del catalizador de metanol. Esto se logra al ajustar el punto de ebullición o la temperatura de un agente de enfriamiento líquido que está en contacto indirecto con las partículas de catalizador y al proporcionar una relación específica del volumen de lecho de catalizador con respecto al área de superficie de enfriamiento. Por esa razón, la condensación de metanol a medida que se forma en la fase gaseosa toma lugar para la mayoría en la superficie de enfriamiento dispuesta que está distribuida uniformemente dentro del reactor y si acaso dentro de una región muy limitada del lecho de catalizador. La figura más representativa de la invención es la número 1a.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DKPA200800260 | 2008-02-25 | ||
DKPA200800261 | 2008-02-25 | ||
PCT/EP2009/000974 WO2009106232A1 (en) | 2008-02-25 | 2009-02-12 | Method and reactor for the preparation of methanol |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2010007376A true MX2010007376A (es) | 2010-08-11 |
Family
ID=40586790
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2010008947A MX2010008947A (es) | 2008-02-25 | 2009-02-12 | Reactor para la preparacion de metanol. |
MX2010007376A MX2010007376A (es) | 2008-02-25 | 2009-02-12 | Metodo y reactor para la preparacion de metanol. |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2010008947A MX2010008947A (es) | 2008-02-25 | 2009-02-12 | Reactor para la preparacion de metanol. |
Country Status (17)
Country | Link |
---|---|
US (3) | US8513314B2 (es) |
EP (3) | EP2249958B1 (es) |
JP (2) | JP2011515334A (es) |
KR (2) | KR20100138884A (es) |
CN (2) | CN101959586B (es) |
AT (2) | ATE516876T1 (es) |
AU (2) | AU2009218828B2 (es) |
BR (2) | BRPI0906447B1 (es) |
CA (2) | CA2713874C (es) |
EA (2) | EA019311B1 (es) |
ES (3) | ES2409714T3 (es) |
MX (2) | MX2010008947A (es) |
NZ (2) | NZ587453A (es) |
PL (3) | PL2374533T3 (es) |
RU (1) | RU2481151C2 (es) |
WO (2) | WO2009106231A1 (es) |
ZA (2) | ZA201004473B (es) |
Families Citing this family (29)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BR112012029429B1 (pt) | 2010-05-20 | 2018-07-17 | Haldor Topsoe A/S | método e aparelho para a separação de líquido de um fluxo de alimentação de gás em um reator catalítico. |
WO2011160745A1 (en) | 2010-06-24 | 2011-12-29 | Haldor Topsøe A/S | Co-production of methanol and ammonia |
US20130153188A1 (en) * | 2011-12-16 | 2013-06-20 | L'air Liquide Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude | Advanced smr reactor design featuring high thermal efficiency |
EP3034161A1 (en) | 2014-12-18 | 2016-06-22 | Haldor Topsøe A/S | Method and reactor design for the production of methanol |
DE102015202680A1 (de) | 2015-02-13 | 2016-08-18 | Friedrich-Alexander-Universität Erlangen-Nürnberg | Verfahren zur Durchführung einer chemischen Synthese und Synthesereaktor |
CN107835713B (zh) * | 2015-07-15 | 2021-07-13 | 托普索公司 | 催化反应器 |
WO2017019961A1 (en) * | 2015-07-29 | 2017-02-02 | Primus Green Energy Inc. | Two-stage reactor for exothermal and reversible reactions and methods thereof |
DK3400099T3 (da) | 2016-01-07 | 2020-06-02 | Total Raffinage Chimie | Fremgangsmåde til methanolsyntese under anvendelse af en indiumoxidbaseret katalysator |
WO2017118572A1 (en) | 2016-01-07 | 2017-07-13 | Total Research & Technology Feluy | Supported indium oxide catalyst and process for methanol synthesis using the same |
CN105797653A (zh) * | 2016-03-19 | 2016-07-27 | 江苏怡达化学股份有限公司 | 直接氧化法制备环氧丙烷的绿色合成反应装置及工艺 |
DE102016204718A1 (de) | 2016-03-22 | 2017-09-28 | Siemens Aktiengesellschaft | Reaktor |
DE102016204717A1 (de) * | 2016-03-22 | 2017-09-28 | Siemens Aktiengesellschaft | Reaktor zur Durchführung von gleichgewichtslimitierten Reaktionen |
AU2017242105B2 (en) * | 2016-03-30 | 2021-04-22 | Haldor Topsøe A/S | A methanol synthesis process layout for large production capacity |
EP3401300B1 (de) * | 2017-05-12 | 2021-06-23 | L'air Liquide, Société Anonyme Pour L'Étude Et L'exploitation Des Procédés Georges Claude | Verfahren zur herstellung von methanol |
WO2018210827A1 (en) | 2017-05-17 | 2018-11-22 | Total Research & Technology Feluy | Mto-ocp upgrading process to maximize the selectivity to propylene |
WO2018210826A1 (en) | 2017-05-17 | 2018-11-22 | Total Research & Technology Feluy | Process for ethylene aromatisation from diluted stream |
EP3404005A1 (en) | 2017-05-17 | 2018-11-21 | Total Research & Technology Feluy | Process for ethylene oligomerisation from diluted stream |
AR113649A1 (es) | 2017-12-20 | 2020-05-27 | Haldor Topsoe As | Convertidor de flujo axial enfriado |
EP3593900A1 (en) | 2018-07-10 | 2020-01-15 | Total Raffinage Chimie | Copper-iron-based catalytic composition for the conversion of syngas to higher alcohols and process using such catalyst composition |
EP3599075A1 (de) | 2018-07-27 | 2020-01-29 | Siemens Aktiengesellschaft | Reaktor zur durchführung einer chemischen gleichgewichtsreaktion |
EP3846936A1 (en) | 2018-09-06 | 2021-07-14 | Total Se | Noble metal promoted supported indium oxide catalyst for the hydrogenation of co2 to methanol and process using said catalyst |
WO2020157049A1 (en) | 2019-02-01 | 2020-08-06 | Total S.A. | Process using catalytic composition for the conversion of syngas to higher alcohols |
EP3917669B1 (en) | 2019-02-01 | 2023-08-16 | TotalEnergies OneTech | Copper-iron-based catalytic composition comprising zeolites, method for producing such catalytic composition and process using such catalytic composition for the conversion of syngas to higher alcohols |
WO2021038441A1 (en) * | 2019-08-27 | 2021-03-04 | Sabic Global Technologies B.V. | Mass transfer swirler including distribution member |
WO2021052978A1 (en) * | 2019-09-20 | 2021-03-25 | Sabic Global Technologies B.V. | Reactor tube assembly |
AU2020355652A1 (en) * | 2019-09-27 | 2022-05-19 | Sumitomo Chemical Company, Limited | Chemical reaction method and chemical reaction device |
EP4234521A3 (en) * | 2020-08-31 | 2023-09-27 | Sumitomo Chemical Company, Limited | Chemical reaction method, chemical reaction apparatus and production method |
CN116457325A (zh) | 2020-11-17 | 2023-07-18 | 道达尔能源一技术 | 用于由富co2合成气合成甲醇的工艺 |
ES2914350B2 (es) * | 2020-12-09 | 2023-01-30 | Blueplasma Power S L | Dispositivo y proceso para producir carbonato de dimetilo |
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2009
- 2009-02-12 JP JP2010547086A patent/JP2011515334A/ja active Pending
- 2009-02-12 CN CN2009801064012A patent/CN101959586B/zh active Active
- 2009-02-12 BR BRPI0906447-8A patent/BRPI0906447B1/pt active IP Right Grant
- 2009-02-12 ES ES11005512T patent/ES2409714T3/es active Active
- 2009-02-12 BR BRPI0907815-0A patent/BRPI0907815B1/pt active IP Right Grant
- 2009-02-12 AU AU2009218828A patent/AU2009218828B2/en active Active
- 2009-02-12 EP EP09714360A patent/EP2249958B1/en active Active
- 2009-02-12 ES ES09715912T patent/ES2368027T3/es active Active
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