KR970705972A - 치약 조성물(dentifrice compositions) - Google Patents
치약 조성물(dentifrice compositions)Info
- Publication number
- KR970705972A KR970705972A KR1019970701953A KR19970701953A KR970705972A KR 970705972 A KR970705972 A KR 970705972A KR 1019970701953 A KR1019970701953 A KR 1019970701953A KR 19970701953 A KR19970701953 A KR 19970701953A KR 970705972 A KR970705972 A KR 970705972A
- Authority
- KR
- South Korea
- Prior art keywords
- sodium
- particle size
- rti
- precipitated silica
- sarcosinate
- Prior art date
Links
- 239000000203 mixture Substances 0.000 title claims abstract 22
- 239000000551 dentifrice Substances 0.000 title claims 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract 29
- 239000002245 particle Substances 0.000 claims abstract 14
- 239000000377 silicon dioxide Substances 0.000 claims abstract 14
- 239000000606 toothpaste Substances 0.000 claims abstract 9
- 229940034610 toothpaste Drugs 0.000 claims abstract 8
- 210000004268 dentin Anatomy 0.000 claims abstract 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims abstract 2
- 229910052753 mercury Inorganic materials 0.000 claims abstract 2
- 238000005498 polishing Methods 0.000 claims abstract 2
- 239000011148 porous material Substances 0.000 claims abstract 2
- 230000002285 radioactive effect Effects 0.000 claims abstract 2
- 239000007787 solid Substances 0.000 claims abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 10
- 239000004115 Sodium Silicate Substances 0.000 claims 7
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims 7
- 229910052911 sodium silicate Inorganic materials 0.000 claims 7
- 239000000243 solution Substances 0.000 claims 7
- 239000004094 surface-active agent Substances 0.000 claims 6
- 108010077895 Sarcosine Proteins 0.000 claims 4
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims 3
- 239000002738 chelating agent Substances 0.000 claims 3
- 239000011541 reaction mixture Substances 0.000 claims 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 claims 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims 2
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims 2
- 108700004121 sarkosyl Proteins 0.000 claims 2
- 239000011734 sodium Substances 0.000 claims 2
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 claims 2
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims 2
- 229940045885 sodium lauroyl sarcosinate Drugs 0.000 claims 2
- 238000003756 stirring Methods 0.000 claims 2
- 235000002906 tartaric acid Nutrition 0.000 claims 2
- 239000011975 tartaric acid Substances 0.000 claims 2
- 239000000080 wetting agent Substances 0.000 claims 2
- XGRSAFKZAGGXJV-UHFFFAOYSA-N 3-azaniumyl-3-cyclohexylpropanoate Chemical compound OC(=O)CC(N)C1CCCCC1 XGRSAFKZAGGXJV-UHFFFAOYSA-N 0.000 claims 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims 1
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims 1
- 208000002064 Dental Plaque Diseases 0.000 claims 1
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims 1
- 229910004298 SiO 2 Inorganic materials 0.000 claims 1
- 238000013019 agitation Methods 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- 150000001860 citric acid derivatives Chemical class 0.000 claims 1
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 238000009472 formulation Methods 0.000 claims 1
- 235000011187 glycerol Nutrition 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- SUMDYPCJJOFFON-UHFFFAOYSA-N isethionic acid Chemical compound OCCS(O)(=O)=O SUMDYPCJJOFFON-UHFFFAOYSA-N 0.000 claims 1
- 125000001421 myristyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- 229940041672 oral gel Drugs 0.000 claims 1
- 239000006072 paste Substances 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- 230000001376 precipitating effect Effects 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 229940071089 sarcosinate Drugs 0.000 claims 1
- FSYKKLYZXJSNPZ-UHFFFAOYSA-N sarcosine Chemical compound C[NH2+]CC([O-])=O FSYKKLYZXJSNPZ-UHFFFAOYSA-N 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- HELHAJAZNSDZJO-OLXYHTOASA-L sodium L-tartrate Chemical compound [Na+].[Na+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O HELHAJAZNSDZJO-OLXYHTOASA-L 0.000 claims 1
- 235000013024 sodium fluoride Nutrition 0.000 claims 1
- 239000011775 sodium fluoride Substances 0.000 claims 1
- 229960004711 sodium monofluorophosphate Drugs 0.000 claims 1
- 229960002167 sodium tartrate Drugs 0.000 claims 1
- 239000001433 sodium tartrate Substances 0.000 claims 1
- 235000011004 sodium tartrates Nutrition 0.000 claims 1
- AUHKUMFBHOJIMU-UHFFFAOYSA-M sodium;2-[hexadecanoyl(methyl)amino]acetate Chemical compound [Na+].CCCCCCCCCCCCCCCC(=O)N(C)CC([O-])=O AUHKUMFBHOJIMU-UHFFFAOYSA-M 0.000 claims 1
- VLKIFCBXANYYCK-GMFCBQQYSA-M sodium;2-[methyl-[(z)-octadec-9-enoyl]amino]acetate Chemical compound [Na+].CCCCCCCC\C=C/CCCCCCCC(=O)N(C)CC([O-])=O VLKIFCBXANYYCK-GMFCBQQYSA-M 0.000 claims 1
- 239000000600 sorbitol Substances 0.000 claims 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- 229940104261 taurate Drugs 0.000 claims 1
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 claims 1
- YUOWTJMRMWQJDA-UHFFFAOYSA-J tin(iv) fluoride Chemical compound [F-].[F-].[F-].[F-].[Sn+4] YUOWTJMRMWQJDA-UHFFFAOYSA-J 0.000 claims 1
- 239000000499 gel Substances 0.000 abstract 1
- 230000035515 penetration Effects 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
- C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
- A61K8/21—Fluorides; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/02—Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/51—Particles with a specific particle size distribution
- C01P2004/52—Particles with a specific particle size distribution highly monodisperse size distribution
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
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- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/14—Pore volume
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- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/19—Oil-absorption capacity, e.g. DBP values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/90—Other properties not specified above
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/40—Monoamines or polyamines; Salts thereof
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
- C11D1/528—Carboxylic amides (R1-CO-NR2R3), where at least one of the chains R1, R2 or R3 is interrupted by a functional group, e.g. a -NH-, -NR-, -CO-, or -CON- group
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/62—Quaternary ammonium compounds
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/722—Ethers of polyoxyalkylene glycols having mixed oxyalkylene groups; Polyalkoxylated fatty alcohols or polyalkoxylated alkylaryl alcohols with mixed oxyalkylele groups
Landscapes
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- Chemical & Material Sciences (AREA)
- Animal Behavior & Ethology (AREA)
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- Public Health (AREA)
- Veterinary Medicine (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Engineering & Computer Science (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Pharmacology & Pharmacy (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Cereal-Derived Products (AREA)
- Detergent Compositions (AREA)
- Dental Preparations (AREA)
Abstract
신규의 연마제를 함유하는 경구용 겔 및 고체 치약과 같은 경구용 조성물이 개시되어 있다. 이 치약 조성물은 (a) 침강 실리카, 상기 침상 실리카는 연질 입자의 좁은 입자 크기 범위 분포를 갖고 8 내지 14미크론, 바람직하게는 7 내지 11미크론의 평균치 입자 크기, 60 내지 120cc/100g의 흡유성, 및 1.0 내지 4.0cc/g의 수은침입(HG1) 공극 부피를 갖는 저 구조 침강 실리카이고; 치약으로 제형되었을 때 상기 침강 실리카는 70 내지 140의 지방막 세정 비율(PCR) 및 60 내지 130의 방사능 상아질 연마(RDA)치를 가지며; 상기 PCR 대 상기 RDA의 비는 적어도 1:1이고; 미크론의 입자 크기가 상기 실리카에서 증가됨에 따라 RDA값은 실질적으로 일정하게 유진된다; 및 (b) 0.1% 내지 99%의 경구적으로 허용가능한 치약 캐리어를 함유한다.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (10)
- a. 침강 실리카, 상기 침강 실리카는 연질 입자의 좁은 입자 크기 범위 분포를 갖고 8 내지 14미크론, 바람직하게는 7 내지 11미크론의 평균치(MV) 입자 크기, 60 내지 120cc/100g의 흡유성, 및 1.0 내지 4.0cc/g의 수은 침입(HG1) 공극 부피를 갖는 저 구조 침강 실리카이고; 치약으로 제형되었을 때 상기 침강 실리카는 70 내지 140의 지방막 세정 비율(PCR) 및 60 내지 130의 방사능 상아질 연마(RDA)치를 가지며; 상기 PCR대 상기 RDA의 비는 적어도 1:1이고; 입자 크기(미크론 단위)가 상기 실리카에서 증가됨에 따라 RDA값은 실질적으로 일정하게 유지된다; 및 b 1.0% SOWL 99%의 경구적으로 허용가능한 치약 캐리어를 함유하는 치약조성물.
- 제1항에 있어서, 상기 연만제가, 치약 제제로 제형되었을 때, 바람직하게는 60 내지 98의 RDA, 바람직하게는 50 내지 250㎡/g의 BET 표면적, 바람직하게는 4.0 내지 8.5의 5% 물 슬러리의 pH를 갖고, 상기 실리카입자는 실질적으로 8 내지 14미크론, 바람직하게는 7 내지 11미크론의 MV 입자 크기내에서 매우 좁은 분포를 가진 균일한 입자 크기이고, 작은 크기의 입자들이 상기 MV 입자 크기내에서 물리적 결합에 의해 서로 응집 밀착됨을 특징으로 하는 치약 조성물.
- 제1항 또는 제2항에 있어서, 상기 조성물이 플루오라이드 이온 원을 더욱 포함하고, 바람직하게는 플루오라이드 이온 원이 플루오르화나트륨, 플루오르화 주석, 모노플루오로인산 나트륨, 플루오르화 칼륨 및 이들의 혼합물로 구성된 군에서 선택됨을 특징으로 하는 치약 조성물.
- 제1항 내지 제3항 중 어느 한 항에 있어서, 상기 조성물이 계면활성제를 더욱 함유하며, 바람직하게는 상기 계면활성제는 사르코시네이트 계면활성제, 이세티오네이트 계면활성제 및 타우레이트 계면활성제로 구성된 군에서 선택되고, 더욱 바람직하게는 소듐 라우로일 사르코시네이트, 소듐 데실 사르코시네이트, 소듐 미리스틸 사르코시네이트, 소듐 스테아릴 사르코시네이트, 소듐 팔미토일 사르코시네이트, 소듐 올레오일 사르코시네이트 및 이들의 혼합물로 구성된 군에서 선택됨을 특징으로 하는 치약 조성물.
- 제1항 내지 제4항 중 어느 한 항에 있어서, 상기 조성물이 0.1 내지 2.5%의 킬레이트제를 더욱 포함하며, 바람직하게는 상기 킬레이트제는 타르타르산 및 약학적으로 허용가능한 그의 염, 시트르산 및 알칼리 금속 시트레이트 및 이들이 혼합물로 구성된 군에서 선택됨을 특징으로 하는 치약 조성물.
- 제1항 내지 제5항 중 어느 한 항에 있어서, 상기 조성물이 15% 내지 70%의 습윤제를 더욱 포함하며, 바람직하게는 상기 습윤제가 글리세린, 솔비톨, 프로필렌 글리콜 및 이들의 혼합물로 구성된 군에서 선택됨을 특징으로 하는 치약 조성물.
- 제1항 내지 제6항 중 어느 한 항에 있어서, 계면활성제가 소듐 라우로일 사르코시네이트 및 코코아미도프로필 베타인의 조합이고, 킬레이트제가 타프타르산 및 타르타르산 나트륨의 조합임을 특징으로 하는 치약 조성물.
- 제1항 내지 제7항 중 어느 한 항에 있어서, 고체 치약, 분말 치약, 치석제거용 페이스트, 정제, 고무 또는 경구용 겔의 형태임을 특징으로 하는 치약 조성물.
- 제1항 내지 제8항 중 어느 한 항에 있어서, 상기 침강 실리카의 2% 이상이 응집되고, 바람직하게는 상기 침강 실리카의 5% 이상이 응집됨을 특징으로 하는 치약 조성물.
- a. 하기 단계들: i)Na2O:SiO2의 비율이 1 내지 3.5:1 이고, 8.0 내지 35중량% 농도를 갖는 소듐 실리케이트의 수용액을 제공하고; ii) 6 내지 35%의 농도를 가진 황산 수용액을 제공하고; iii) 상기 소듐 실리케이트 용액의 화학양론적 양의 1 내지 5%를 교반하에 반응기에 도입하고; iv) 상기 소듐 실리케이트의 용액을 80 내지 90℃의 온도까지 가열하고; v) 황산 및 나머지의 소듐 실리케이트 용액을 상기 반응기에 천천히 가하고, 상기 첨가는 소듐 실리케이트가 1 분당 7 내지 12리터의 속도로 도입되고 황산이 1 분당 1 내지 4 리터의 속도로 반응기에 도입될 수 있는 시간동안 수행되며; vi) 반응기내에 소듐 실리케이트 및 황산을 40 내지 60분의 첨가 시간에 걸쳐 계속 첨가하고; vii) 소듐 실리케이트 용액의 첨가를 중지하고, 황산 용액은 반응기내에서 5.0 내지 5.8의 최종 pH가 얻어질 때까지 교반하에 계속 첨가하여 반응액중에 침강 실리카를 제공하고; viii) 상기 반응 혼합물의 온도를 연속 교반하에 10분 내지 1시간에 걸쳐 90 내지 98℃의온도로 올리고; ix) 상기 혼합물을 적어도 30분 내지 2시간동안 비등시킴으로써 반응 혼합물을 경화시켜, 실질적으로 균일한 입자 크기의 침강 실리카를 형성시키고; x) 반응 혼합물을 냉각시키고 침강 실리카를 회수하는 단계에 의해 실리카를 침강시키고, b. 상기 a와 경구적으로 허용가능한 치약 캐리어를 조합하는 단계로 구성됨을 특징으로 하는 치약 조성물의 제조방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
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US08/312,353 | 1994-09-26 | ||
US08/312,353 US5603920A (en) | 1994-09-26 | 1994-09-26 | Dentifrice compositions |
US8/312,353 | 1994-09-26 | ||
PCT/US1995/012104 WO1996009809A1 (en) | 1994-09-26 | 1995-09-25 | Dentifrice compositions |
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KR970705972A true KR970705972A (ko) | 1997-11-03 |
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- 1995-09-25 BR BRPI9509025-8A patent/BR9509025B1/pt not_active IP Right Cessation
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KR20150084787A (ko) * | 2012-11-19 | 2015-07-22 | 제이. 엠. 후버 코포레이션 | 치약의 개선된 세정을 위한 처리된 실리카 및 금속 실리케이트 |
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