KR900003345A - 윤활유 조성물 및 농축물 - Google Patents

윤활유 조성물 및 농축물 Download PDF

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KR900003345A
KR900003345A KR1019890007129A KR890007129A KR900003345A KR 900003345 A KR900003345 A KR 900003345A KR 1019890007129 A KR1019890007129 A KR 1019890007129A KR 890007129 A KR890007129 A KR 890007129A KR 900003345 A KR900003345 A KR 900003345A
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group
oil composition
alcohol
acid
value
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KR1019890007129A
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KR930010528B1 (en
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유진 리플 데이빗
브리커 체임벌린 3세 윌리엄
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지이 아아르 힐
더 루우브리졸 코오포레이션
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Abstract

내용 없음

Description

윤활유 조성물 및 농축물
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Claims (42)

  1. (A) 윤활 점도의 오일 다량, (B) (B-1)값이 약 1300 내지 약 5000이고값이 약 1.5 내지 약 4.5인 것을 특징으로 하는 플리알켄으로부터 유도된 치환체 기와 숙신산 기로 이루어져 있으며, 그 구조 내에 치환체 기 각각의 당량에 대해 평균적으로 최소한 1.3의 숙식산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 치환된 숙식산 아실화제 1 당량 당, (B-2) 그 구조 내에 최소한 하나의 HN〈 기가 존재하는 것을 특징으로 하는, 최소한 하나의 아민 화합물 1 당량-2몰을 반응시킴으로써 제조된, 최소한 하나의 카르복실산 유도체 조성물 소량, (C) 다가 알코올의, 최소한 하나의 부분적 지방산 에스테르 소량, 및 (D) (D-1) 디티오인산은, 최소한 10몰%의 이소프로필 알코올, 이차 부틸 알코올, 또는 이소프로필 알코올과 이차 부틸 알코올의 혼합물, 및 약 3- 약 13개의 탄소 원자를 함유하는 최소한 한아의 일차 지방족 올코올을 포함하는 알코올 혼합물과 오황화인을 반응시킴으로써 제조되고, (D-2) 금속은 제Ⅱ족 금속, 알루미늄, 주석, 철, 코발트, 납, 몰리부덴, 망간, 니켈 또는 구리인, 디히드로카르빌 디티오인산의, 최소한 하나의 금속염 소량을 포함하는, 내부 연소 엔진을 위한 윤활유 조성물.
  2. 제1항에 있어서, 카르복실산 유도체 조성물 (B)를 최소한 약 1중량% 함유하는 오일 조성물.
  3. 제1항에 있어서, (B)에서의값이 최소한 약 1500인 오일 조성물.
  4. 제1항에 있어서, (B)에서의값이 최소한 약 2.0인 오일 조성물.
  5. 제1항에 있어서, (B)에서의 치환체 기가, 2-약 16개의 탄소 원자를 갖는 말단 올레핀의 인터폴리머 및 호모폴리머로 구성된 군으로부터 선택된 하나 이상의 폴리알켄(단, 상기 인터폴리머는 약 6개 이하의 탄소 원자를 갖는 내부 올레핀으로부터 유도된 폴리머단위체를 약 25% 이하 함유할 수 있음)으로부터 유도되는 오일 조성물.
  6. 제1항에 있어서, 치환체 기가, 폴리부텐, 에틸렌-프로필렌 코폴리머, 폴리프로필렌, 및 이들 중 두개 이상의 어떤 것의 혼합물로 구성된 군으로부터 선택된 요소로부터 유도되는 오일 조성물.
  7. 제1항에 있어서, 아민(B-2)이 지방족, 환식 지방족 또는 방향족 폴리아민인 오일 조성물.
  8. 제1항에 있어서, 아민(B-2)이 하기 일반식(Ⅵ)을 갖는 것을 특징으로 하는 오일 조성물 :
    상기식에서, n은 1-약 10이며 ; 각각의 R3는 독립적으로 수소 원자, 히드로카르빌 기 또는 약 30개 이하의 원자를 갖는 아미노-치환 또는 히드록시-치환 히드로카르빌 기이거나, 다른 질소 원자 상의 두 개의 R3기가 함께 결합하여 U기를 형성할 수 있고, 단, 최소한 하나의 R3기는 수소 원자이고 U는 약 2-약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  9. 제1항에 있어서, (C)에서의 지방산 에스테르가 약 10-약 22개의 탄소 원자를 함유하는 오일 조성물.
  10. 제1항에 있어서, (C)의 다가 알코올이 글리세롤인 오일 조성물.
  11. 제1항에 있어서, (D-1)에서의 일차 지방족 알코올이 약 6-약 13개의 탄소 원자를 함유하는 오일 조성물.
  12. 제1항에 있어서, (D-2)의 금속이 아연, 구리, 또는 아연과 구리 혼합물인 오일 조성물.
  13. 제1항에 있어서, (D-1)의 금속이 아연인 오일 조성물.
  14. 제1항에 있어서, (D-10)에서의 알코올 혼합물이 최소한 20몰%의 이소프로필 알코올을 포함하는 오일 조성물.
  15. 제1항에 있어서, (E) (E-1) 최소한 약 700의값을 갖는 치환체 기와 숙신산 기를 포함하는, 최소한 하나의 치환된 숙식산 아실화제와 (E-2)하기 일반식(Ⅷ) :
    R3(OH)m (Ⅷ)
    (상기식에서, R3는 탄소 결합을 통해 -OH기에 연결도니 일가 또는 다가의 유기 기이며, m은 정수 1- 약 10임)을 갖는, 최소한 하나의 알코올을 반응시킴으로써 제조된 최소한 하나의 카르복실산 에스테르 유도체 조성물을 함유하는 오일 조성물.
  16. 제15항에 있어서, (E-1)에서의 치환체 기가, 폴리부텐, 에틸렌-프로필렌 코폴리머, 폴리프로필랜, 및 이들 중 두 개 이상의 어떤 것의 혼합물로 구성된 군으로부터 선택된 요소로부터 유도되는 오일 조성물.
  17. 제15항에 있어서, 알코올 (E-2)이 네오펜틸글리콜, 에틸렌 글리콜, 글리세롤, 펜타에리트리톨, 솔비톨, 폴리(옥시알킬렌)글리콜의 모노-아릴 또는 모노-알킬에테르, 또는 이들 중 어떤 것의 혼합물인 오일 조성물.
  18. 제15항에 있어서, 아실화제(E-1)와 알코올(E-2)을 반응시킴으로써 제조된 카르복실산 에스테르 유도체 조성물(E)을, (E-3) 최소한 하나의 HN〈기를 함유하는 최소한 하나의 아민과 반응시키는 오일 조성물.
  19. 제15항에 있어서, 치환된 숙식산 아실화제 (E-1)가,값이 약 1300 내지 약 5000이고값이 약 1.5 내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 숙식산 기로 구성되고, 그 구조 내에 치환체 기 각각의 당량에 대해 최소한 약 1.3의 숙식산 기가 존재하는 것을 특징으로 하는 오일 조성물.
  20. 제19항에 있어서, 아실화제와 알코올을 반응시킴으로써 제조된 카르복실 산 에스테르를. (E-3) 최소한 하나의 HN〈기를 함유하는 최소한 하나의 아민과 반응시키는 오일 조성물.
  21. 제20항에 있어서, 아민(E-3)이 폴리아민인 오일 조성물.
  22. 제20항에 있어서, 아민 (E-3)이 알킬렌 폴리아민인 오일 조성물.
  23. 제1항에 있어서, (F) 최소한 하나의 산성 유기 화합물의, 최소한 하나의 중성 또는 염기성 알카리토금속 염을 함유하는 오일 조성물.
  24. 제23항에 있어서, (F)에서의 산성 유기 화합물이 황산, 카르복실산, 인산, 페놀, 또는 이들의 혼합물인 오일 조성물.
  25. 제23항에 있어서, (F)에서의 산성 화합물이 최소환 하나의 유기 설폰산인 오일 조성물.
  26. 제25항에 있어서, 설폰산이 알킬화된 벤젠설폰산인 오일 조성물.
  27. (A) 윤활 점도의 오일 다량, (B) (B-1)값이 약 1300 내지 약 5000이고값이 약 2 내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 숙신산 기로 이루어져 있으며, 그 구조 내에 치환체 기 각각의 당량에 대해 평균적으로 최소한 1.3의 숙식산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 치환된 숙식산 아실화제 1 당량 당, (B-2) 그 구조 내에 최소한 하나의 HN〈 기가 존재하는 것을 특징으로 하는, 최소한 하나의 폴리아민 화합물 1 당량-약 2몰을 반응시킴으로써 제조된, 최소한 하나의 카르복실산 유도체 조성물 약 0.5-약 10중량%, (C) 다가 알코올의, 최소한 하나의 부분적 지방산 에스테르 약 0.01-약 2중량%, (D) (D-1) 디티오인산은, 최소한 10몰%의 이소프로필 알코올, 이차 부틸 알코올, 또는 이소프로필 알코올과 이차 부틸 알코올의 혼합물, 및 약 3- 약 13개의 탄소 원자를 함유하는 최소한 하나의 일차 지방족 알코올을 포함하는 알코올 혼합물과 오황화인을 반응시킴으로써 제조되고, (D-2) 금속은 제Ⅱ족 금속, 알루미늄, 주석, 철, 코발트, 납, 몰리부덴, 망간, 니켈 또는 구리인, 디히드로카르빌 디티오인산의, 최소한 하나의 금속 염 약 0.05-약 5중량%, (E)(E-1)값이 약 1300내지 약 5000이고,값이 약 1.5내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 숙식산 기를 포함하고, 그 구조 내에 치환체 기 각각의 당량에 대해 최소한 1.3의 숙식산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 치환된 숙식산 아실화제와 (E-2) 하기 일반식(Ⅷ) :
    R3(OH)m (Ⅷ)
    상기식에서, R3는 탄소 결합을 통해 -OH기에 연결된 일가 또는 다가의 유기 기이며, m은 정수 2-약 10임)을 갖는, 최소한 하나의 알코올, 및 (E-3) 최소한 하나의 〉NH기를 함유하는, 최소한 하나의 폴리아민 화합물을 반응시킴으로써 제조된, 최소한 하나의 카르복실산 에스테르 유도체 조성물 0.1 내지 약 10%, 및 (F) 황산, 카르복실 산, 인산, 페놀, 및 상기 산들의 혼합물로 구성된 군으로부터 선택된 유기산 화합물의, 최소한 하나의 알카리토금속 염 약 0.01-약 5중량%를 포함하는, 내부 연소 엔진을 위한 윤활유 조성물.
  28. 제27항에 있어서, 카르복실산 유도체 조성물 (B)를 최소한 약 1.0중량% 함유하는 오일 조성물.
  29. 제27항에 있어서, 아민(B-2) 및 (E-3)가 각각 독립적으로 하기 일반식(Ⅵ)을 갖는 것을 특징으로 하는 폴리아민류인 오일 조성물 :
    상기식에서, n은 정수 1-약 10이며, 각각의 R3는 독립적으로 수소 원자, 히드로카르빌 기 또는 약 30개 이하의 원자를 갖는 아미노-치환 또는 히드록시-치환 히드로 카르빌 기이거나, 다른 질소 원자 상의 두개의 R3기가 함께 결합하여 U기를 형성할 수 있고, 단, 최소한 하나의 R3기는 수소원자이며, U는 약 2 내지 약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  30. 제27항에 있어서, (D-1)에서의 일차 지방족 알코올이 약 6-약 13개의 탄소 원자를 함유하는 오일 조성물.
  31. 제27항에 있어서, (D-2)의 금속이 아연, 구리, 또는 아연과 구리의 혼합물인 오일 조성물.
  32. 제27항에 있어서, (D-2)의 금속이 아연인 오일 조성물.
  33. 제27항에 있엇, (D-1)에서의 알코올 혼합물이 최소한 20몰%의 이소프로필 알코올인 오일 조성물.
  34. 제27항에 있어서, 알코올 (E-2)이 네오펜틸 글리콜, 에틸렌 글리콜, 글리세롤, 펜타에리트리톨, 솔비톨, 폴리(옥시알킬렌)글리콜의 모노-아릴 또는 모노-알킬 에테르, 또는 이들 중 두개 이상의 어떤 것의 혼합물인 오일 조성물.
  35. (A) 윤활 점도의 오일 다량, (B) (B-1)값이 약 1300 내지 약 5000이고,값이 약 1300 내지 약 5000이고값이, 약 2 내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 숙신산 기로 이루어져 있으며, 그 구조 내에 치환체 기 각각의 당량에 대해 평균적으로 최소한 1.3의 숙식산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 챨숙식산 아실화제 1 당량 당, (B-2) 그 구조 내에 최소한 하나의 HN〈기가 존재하는 것을 특징으로 하는, 최소한 하나의 폴리아민 1.0-약 1.5 당량을 반응시킴으로써 제조된, 최소한 하나의 카르복실산 유도체 조성물 약 1-약 10중량%, (C) 글리세롤의, 최소한 하나의 부분적 지방산 에스테르 약 0.05-약 2중량%, (D) (D-1) 디티오인산은, 최소한 20몰%의 이소프로필 알코올 및 약 6-약 13개의 탄소원자를 함유하는 최소한 하나의 일차 지방족 알코올을 포함하는 알코올 혼합물과 오황화인을 반응시킴으로써 제조되고, (D-2) 금속은 제Ⅱ족 금속, 알루미늄, 주석, 철, 코발트, 납, 모리브덴, 망간, 니켈, 또는 구리 인, 디히드로카르빌 디티오인산의, 최소한 하나의 금속 염 약 0.05-약 5중량%, (E)(E-1)값이 약 1300내지 약 5000이고,값이 약 1.5내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 숙식산 기를 포함하고, 그 구조 내에 치환체 기 각각의 당량에 대해 최소한 1.3의 숙식산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 치환된 숙식산 아실화제 1몰 당, (E-2) 네오펜틸 글리콜, 에틸렌 글리콜, 글리세롤, 펜타에리트리톨, 솔비톨, 폴리(옥시알킬렌)글리콜의 모노-아릴 또는 모노-알킬 에테르 또는 이들 중 두개 이상의 어떤 것의 혼합물로 구성된 군으로부터 선태된, 최소한 하나의 폴리히드록시 화합물 약 0.1-약 2몰, 및 (E-3) 최소한 하나의 〉NH기를 함유하는 최소한 하나의 폴리아민을 반응시킴으로써 제조된, 최소한 하나의 카르복실산 에스테르 유도체 조성물 0.1-약 10%, 및 (F) 설폰산, 카르복실 산, 페놀, 및 산들의 혼합물로 구성된 군으로부터 선택된 유기산 화합물의, 최소한 하나의 알칼리 토금속 염 약 0.01-약 5중량%를 포함하는, 내부 연소 엔진을 위한 윤활유 조성물.
  36. 제35항에 있어서, 폴리아민(B-2) 및 (E-3)가 각각 독립적으로 하기 일반식(Ⅵ)을 갖는 것을 특징으로 하는 폴리아민류의 오일 조성물.
    상기식에서, n은 정수 1-약 10이며, 각각의 R3는 독립적으로 수소 원자, 히드로카르빌 기 또는 약 30개 이하의 원자를 갖는 아미노-치환 또는 히드록시-치환 히드로카르빌 기이거나, 다른 질소 원자 상의 두개의 R3기가 함께 결합하여 U기를 형성 할 수 있고, 단, 최소한 하나의 R3기는 수소원자이며, U는 약 2 내지 약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  37. 제35항에 있어서, (F)가 유기 설폰 산류의, 염기성 알카리 토금속 염의 혼합물을 포함하는 오일 조성물.
  38. 일반적으로 액체이고, 본질적으로 불활성인 유기 희석제/용매 약 20-약 90중량%, (B) (B-1)값이 약 1300 내지 약 5000이고,값이 약 1.5 내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 숙식산 기로 이루어져 있으며 그 구조 내에 치환체 기 각각의 당량에 대해 평균적으로 최소한 1.3의 숙식산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 치환된 숙식산 아실화제 1 당량 당, (B-2) 그 구조 내에 최소한 하나의 NH〈기가 존재하는 것을 특징으로하는, 최소한 하나의 아민 최소한 1당량을 반응시킨으로써 제조된, 최소한 하나의 카르복실산 유도체 조성물 약 10-약 50중량%, (C) 다가 알콜올의, 최소한 하나의 지방산 에스테르 약 0.1-약 15중량%, 및 (D) (D-1) 디티오인산은, 최소한 10몰%의 이소프로필 알코올, 이차 부틸 알코올, 또는 이소프로필 알코올과 이차부틸 알코올의 혼합물, 및 약 3-약 13개의 탄소 원자를 함유하는 최소한 하나의 일차 지방족 알코올을 포함하는 알코올 혼합물과 오황화인을 반응시킴으로써 제조되고, (D-2) 금속은 제Ⅱ족 금속, 알루미늄, 주석, 철, 코발트, 납, 폴리브덴, 망간, 니켈, 또는 구리 인, 디히드로 카르빌 디티오인산의, 최소한 하나의 금속 염 약 0.001- 약 15중량%를 포함하는, 윤활유 조성물을 배합하기 위한 농축물.
  39. 제38항에 있어서, (E) (E-1)값이 약 1300 내지 약 5000이고,값이 약 1.5 내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 숙식산 기를 포함하고, 그 구조 내에 치환체 기 각각의 당량에 대해 최소한 약 1.3의 숙식산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 치환된 숙식산 아실화제와 (E-2) 하기 일반식(Ⅷ) :
    R3(OH)m (Ⅷ)
    (상기식에서, R3는 탄소 결합을 통해 -OH기에 연결된 일가 또는 다가의 유기 기이며, m은 정수 1-약 10임)을 갖는, 최소한 하나의 알코올을 반응시킴으로써 제조된, 최소한 하나의 카르복식산 에스테르 유도체 조성물을 약 1-약 30중량% 함유하는 농축물.
  40. 제39항에 있어서, 아실화제 (E-1)와 알코올 (E-2)을 반응시킴으로써 제조된 카르복실산 에스테르(E)를 , (E-3) 최소한 하나의 HN〈기를 함유하는 최소한 하나의 폴리아민과 반응시키는 농축물.
  41. 제38항에 있어서, (F) 최소한 하나의 산성 유기 화합물의, 최소한 하나의 중성 또는 염기성 알카리 토금속 염을 약 1- 약 20중량% 함유하는 농축물.
  42. 제39항에 있어서, (F) 최소한 하나의 산성 유기 화합물의, 최소한 하나의 중성 또는 염기성 알카리 토금속염을 약 1-약 20중량% 함유하는 농축물.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
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NO892129L (no) 1990-02-02
MY104025A (en) 1993-10-30
ES2012304A6 (es) 1990-03-01
CH678733A5 (ko) 1991-10-31
DK257989D0 (da) 1989-05-26
NO175867C (no) 1994-12-21
NO892129D0 (no) 1989-05-26
EP0389573A4 (en) 1991-09-11
HUT52807A (en) 1990-08-28
FR2634780A1 (fr) 1990-02-02
GB8912121D0 (en) 1989-07-12
IT8948012A0 (it) 1989-05-29
AU612844B2 (en) 1991-07-18
US4957649A (en) 1990-09-18
IL90404A (en) 1992-07-15
CA1333279C (en) 1994-11-29
HU208034B (en) 1993-07-28
RU2012592C1 (ru) 1994-05-15
MX165945B (es) 1992-12-10
BR8902903A (pt) 1990-09-04
KR930010528B1 (en) 1993-10-25
SE8901897L (sv) 1990-02-02
EP0389573B1 (en) 1995-01-11
JPH0241396A (ja) 1990-02-09
DE68920570T2 (de) 1995-08-03
DE68920570D1 (de) 1995-02-23
NO175867B (ko) 1994-09-12
JP2799184B2 (ja) 1998-09-17
RO109556B1 (ro) 1995-03-30
NL8901330A (nl) 1990-03-01
DE3917391A1 (de) 1990-02-08
ZA894017B (en) 1990-03-28
CN1039837A (zh) 1990-02-21
FI892556A0 (fi) 1989-05-25
GB2221473B (en) 1992-01-08
IL90404A0 (en) 1990-01-18
ATE117014T1 (de) 1995-01-15
EP0389573A1 (en) 1990-10-03
IT1231515B (it) 1991-12-07
WO1990001532A1 (en) 1990-02-22
SG19092G (en) 1992-04-16
BE1001977A3 (fr) 1990-05-02
DK257989A (da) 1990-02-02
AU3518989A (en) 1990-02-01
FR2634780B1 (ko) 1993-02-26
FI892556A (fi) 1990-02-02
CN1019982C (zh) 1993-03-03
GB2221473A (en) 1990-02-07
HK34292A (en) 1992-05-15
SE8901897D0 (sv) 1989-05-26

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