KR900003092A - 조제글리세롤의 정제방법 - Google Patents

조제글리세롤의 정제방법 Download PDF

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Publication number
KR900003092A
KR900003092A KR1019890011329A KR890011329A KR900003092A KR 900003092 A KR900003092 A KR 900003092A KR 1019890011329 A KR1019890011329 A KR 1019890011329A KR 890011329 A KR890011329 A KR 890011329A KR 900003092 A KR900003092 A KR 900003092A
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KR
South Korea
Prior art keywords
glycerol
microfiltration
purification
starting material
crude glycerol
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Application number
KR1019890011329A
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English (en)
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KR920003099B1 (ko
Inventor
부에네만 토마스
코르넬리스 오우데잔스 요하네스
감바 피에트로
람피 알도
Original Assignee
유니레버 엔브이
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by 유니레버 엔브이 filed Critical 유니레버 엔브이
Publication of KR900003092A publication Critical patent/KR900003092A/ko
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Publication of KR920003099B1 publication Critical patent/KR920003099B1/ko

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/22—Trihydroxylic alcohols, e.g. glycerol
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/22—Trihydroxylic alcohols, e.g. glycerol
    • C07C31/225—Glycerol

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Medicines That Contain Protein Lipid Enzymes And Other Medicines (AREA)
  • Cosmetics (AREA)

Abstract

내용 없음

Description

조제글리세롤의 정제방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (10)

  1. 세라믹 지지물로 지지되는 여재를 사용하는 미세여과(상술한 바와 같음)의 단계를 포함하는 것을 특징으로 하는 조제글리세롤의 정제방법.
  2. 제1항에 있어서, 세라믹 지지물 재료는 알루미나인 것을 특징으로 하는 정제방법.
  3. 제1항에 있어서, 여재는 세라믹 물질로 된 것을 특징으로 하는 정제방법.
  4. 제1항에 있어서, 조제 글리세롤의 정제공정은 미세여과와 한외여과(상술한 바와 같음)의 병용을 포함하는 것을 특징으로 하는 정제방법.
  5. 제1항에 있어서, 정제공정은 이온교환수지처리 및/또는 증류단계도 또한 포함하는 것을 특징으로 하는 정제 방법.
  6. 제4항에 있어서, 한외여과단계는 유기중합체 물질로 이루어진 여재를 사용하여 수행되는 것을 특징으로 하는 정제방법.
  7. 제1항에 있어서, 조제글리세롤 출발물질은 수용액이고 8-80%(w.w)의 글리세롤을 함유하며, 오일 또는 지방의 비누화, 가수분해 또는 메탄올 분해에 의해 얻어지는 것을 특징으로 하는 정제방법.
  8. 제7항에 있어서, 조제글리세롤 출발물질은 20-55%(w.w)의 글리세롤을 함유하는 수용액인 것을 특징으로 하는 정제방법.
  9. 제1항에 있어서, 여과이전에 조제글리세롤 출발물질의 pH는 60-100℃ 온도에서 9-12되도록 조절되는 것을 특징으로 하는 정제방법.
  10. 제1항에 있어서, 미세여과는 5.10-8m-20.10-8m의 세공직경을 가지는 여재를 사용하여 수행되는 것을 특징으로 하는 정제 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019890011329A 1988-08-09 1989-08-09 조제글리세롤의 정제방법 KR920003099B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP88201702.3 1988-08-09
EP88201702 1988-08-09

Publications (2)

Publication Number Publication Date
KR900003092A true KR900003092A (ko) 1990-03-23
KR920003099B1 KR920003099B1 (ko) 1992-04-18

Family

ID=8199834

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019890011329A KR920003099B1 (ko) 1988-08-09 1989-08-09 조제글리세롤의 정제방법

Country Status (12)

Country Link
US (1) US4990695A (ko)
EP (1) EP0358255B1 (ko)
JP (1) JPH068259B2 (ko)
KR (1) KR920003099B1 (ko)
AU (1) AU617506B2 (ko)
BR (1) BR8904007A (ko)
CA (1) CA1329782C (ko)
DE (1) DE68911239T2 (ko)
ES (1) ES2047106T3 (ko)
IN (1) IN170612B (ko)
MY (1) MY105093A (ko)
ZA (1) ZA896078B (ko)

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DE4203157A1 (de) * 1992-02-05 1993-08-12 Henkel Kgaa Verfahren zum reinigen von glycerinwasser
DE4220639A1 (de) * 1992-06-24 1994-01-05 Henkel Kgaa Verfahren zur chemischen Reinigung natürlicher Öle und Fette
US5501741A (en) * 1994-01-11 1996-03-26 Uss-Posco Process for purifying aqueous rinse solutions used in metal forming operations
DE19938874B4 (de) * 1999-08-17 2005-11-17 Peter Greven Fettchemie Gmbh & Co. Kg Verfahren zum Entfernen von kurzkettigen Fettsäuren aus einer wäßrigen Glycerinlösung
EA200800129A1 (ru) * 2003-11-20 2008-04-28 Солвей (Сосьете Аноним) Псевдоазеотропная композиция, содержащая дихлорпропанол, и способ ее получения
US8067645B2 (en) 2005-05-20 2011-11-29 Solvay (Societe Anonyme) Process for producing a chlorhydrin from a multihydroxylated aliphatic hydrocarbon and/or ester thereof in the presence of metal salts
TWI320036B (en) * 2005-05-20 2010-02-01 Process for preparing a chlorohydrin starting from a polyhydroxylated aliphatic hydrocarbon
AR057255A1 (es) 2005-11-08 2007-11-28 Solvay Proceso para la elaboracion de dicloropropanol por cloracion de glicerol
GB2437516A (en) * 2006-04-26 2007-10-31 Bai Leng Method and apparatus for purifying glycerine using filter membranes and a deionisation means
CA2654717A1 (en) * 2006-06-14 2007-12-21 Solvay (Societe Anonyme) Crude glycerol-based product, process for its purification and its use in the manufacture of dichloropropanol
US20100032617A1 (en) * 2007-02-20 2010-02-11 Solvay (Societe Anonyme) Process for manufacturing epichlorohydrin
FR2913421B1 (fr) 2007-03-07 2009-05-15 Solvay Procede de fabrication de dichloropropanol.
MY148450A (en) * 2007-03-08 2013-04-30 Adcuram Nutrition Holding Gmbh Process for the preparation of citric acid employing filamentous fungi in a culture medium comprising glycerol
FR2913684B1 (fr) 2007-03-14 2012-09-14 Solvay Procede de fabrication de dichloropropanol
JP4805201B2 (ja) * 2007-03-22 2011-11-02 月島環境エンジニアリング株式会社 膜分離を用いた目的物質の分離方法と装置
EP1978009A1 (en) * 2007-04-04 2008-10-08 Rohm and Haas Company Method for purification of glycerol
TW200911740A (en) * 2007-06-01 2009-03-16 Solvay Process for manufacturing a chlorohydrin
TW200911693A (en) 2007-06-12 2009-03-16 Solvay Aqueous composition containing a salt, manufacturing process and use
TW200911773A (en) 2007-06-12 2009-03-16 Solvay Epichlorohydrin, manufacturing process and use
WO2008156612A1 (en) * 2007-06-15 2008-12-24 Cargill, Incorporated Process for the purification of crude glycerol compositions
EP2207617A1 (en) 2007-10-02 2010-07-21 SOLVAY (Société Anonyme) Use of compositions containing silicon for improving the corrosion resistance of vessels
FR2925045B1 (fr) 2007-12-17 2012-02-24 Solvay Produit a base de glycerol, procede pour son obtention et son utilisation dans la fabrication de dichloropropanol
DE102007062409A1 (de) 2007-12-20 2009-06-25 New Environmental Technology Gmbh Verfahren zur Reinigung von Rohglyzerin
TWI478875B (zh) 2008-01-31 2015-04-01 Solvay 使水性組成物中之有機物質降解之方法
WO2009121853A1 (en) 2008-04-03 2009-10-08 Solvay (Société Anonyme) Composition comprising glycerol, process for obtaining same and use thereof in the manufacture of dichloropropanol
GB2459738B (en) * 2008-05-07 2013-03-06 Bai Leng Method of purification
KR100877384B1 (ko) * 2008-06-30 2009-01-07 바이오원 (주) 필터링 기술을 이용한 조 글리세린의 정제방법
FR2935968B1 (fr) * 2008-09-12 2010-09-10 Solvay Procede pour la purification de chlorure d'hydrogene
FR2939434B1 (fr) * 2008-12-08 2012-05-18 Solvay Procede de traitement de glycerol.
DE102008060888A1 (de) * 2008-12-09 2010-06-10 Evonik Stockhausen Gmbh Verfahren zur Herstellung von Acrolein umfassend die Aufarbeitung einer Rohglycerin-Phase
CN101445425B (zh) * 2008-12-22 2012-01-04 湖南尔康制药股份有限公司 一种注射用甘油的制备方法
US20110004031A1 (en) * 2009-05-06 2011-01-06 S.I.I., Llc Glycerin purification
EP2295394A1 (en) 2009-09-11 2011-03-16 Rhodia Poliamida E Especialidades Ltda Process for the purification of crude glycerol
FR2964657B1 (fr) 2010-09-15 2013-01-18 Rhodia Operations Procede de purification du glycerol brut
KR20140009163A (ko) 2010-09-30 2014-01-22 솔베이(소시에떼아노님) 천연유래 에피클로로히드린의 유도체
CN102229521B (zh) * 2011-05-14 2013-11-06 江门市鸿捷精细化工有限公司 一种粗甘油精制及副产物回收工艺
CN102408309B (zh) * 2011-09-19 2013-09-11 鲁东大学 一种甘油废液的纯化方法
JP6385199B2 (ja) * 2014-08-22 2018-09-05 花王株式会社 軽油添加剤
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CN105906476B (zh) * 2016-05-26 2018-08-24 淮南天力生物工程开发有限公司 一种从生物柴油生产废水中提取甘油的方法

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Also Published As

Publication number Publication date
ES2047106T3 (es) 1994-02-16
US4990695A (en) 1991-02-05
BR8904007A (pt) 1990-03-20
KR920003099B1 (ko) 1992-04-18
IN170612B (ko) 1992-04-18
CA1329782C (en) 1994-05-24
MY105093A (en) 1994-08-30
DE68911239T2 (de) 1994-04-14
EP0358255B1 (en) 1993-12-08
DE68911239D1 (de) 1994-01-20
EP0358255A1 (en) 1990-03-14
ZA896078B (en) 1991-04-24
JPH068259B2 (ja) 1994-02-02
JPH02101031A (ja) 1990-04-12
AU617506B2 (en) 1991-11-28
AU3943689A (en) 1990-03-15

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