KR870007743A - 리티오써미아 방법에 의한 금속분말의 제조방법 - Google Patents

리티오써미아 방법에 의한 금속분말의 제조방법 Download PDF

Info

Publication number
KR870007743A
KR870007743A KR870001741A KR870001741A KR870007743A KR 870007743 A KR870007743 A KR 870007743A KR 870001741 A KR870001741 A KR 870001741A KR 870001741 A KR870001741 A KR 870001741A KR 870007743 A KR870007743 A KR 870007743A
Authority
KR
South Korea
Prior art keywords
bed
reduced
metal
mentioned
molten salt
Prior art date
Application number
KR870001741A
Other languages
English (en)
Other versions
KR910006946B1 (ko
Inventor
쎄옹 프랑소아즈
나따 필리쁘
Original Assignee
롱쁠랑 쉬미
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 롱쁠랑 쉬미 filed Critical 롱쁠랑 쉬미
Publication of KR870007743A publication Critical patent/KR870007743A/ko
Application granted granted Critical
Publication of KR910006946B1 publication Critical patent/KR910006946B1/ko

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1263Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
    • C22B34/1268Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
    • C22B34/1272Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/20Obtaining niobium, tantalum or vanadium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00General methods of reducing to metals
    • C22B5/02Dry methods smelting of sulfides or formation of mattes
    • C22B5/04Dry methods smelting of sulfides or formation of mattes by aluminium, other metals or silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B59/00Obtaining rare earth metals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Electrolytic Production Of Metals (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

내용 없음

Description

리티오써미아 방법에 의한 금속분말의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (20)

  1. 원소 주기율 표의 IVB 또는 VB 족 금속의 염 또는 란타니트 계열 금속의 염을, 용융된 염의 배드중에 분산 유지시킨 리튬을 함유하는 액체혼합물과 접촉시킴을 특징으로 하여, 언급된 금속 염을 리튬으로 환원시켜 주기율 표의 IVB 또는 VB족 금속 또는 란타니드 계열 금속을 제조하는 방법.
  2. 제 1 항에 있어서, 언급된 리튬을 기계적 교반 특히 블레이드가 장치된 교반기 및 대향 블레이드 시스템에 의하여 용융된 염의 배드중에 분산유지 시킴을 특징으로 하는 방법.
  3. 전술된 항들중 어느 한 항에 있어서, 언급된 물질을 접촉시킨후, 환원된 금속을 배드로부터 분리시키고, 분리된 금속을 산 세척하고 건조시켜 고-순도의 금속 분말을 수득함으로써 생성물을 제조함을 특징으로 하는 방법.
  4. 전술된 항들중 어느 한항에 잇어서, 산화된 리튬을 전기 화학적으로 재생시킴을 특징으로 하는 방법.
  5. 제 4 항에 있어서, 재생된 리튬을 사용하여 언급된 금속염을 환원시킴을 특징으로 하는 방법.
  6. 전술된 항들중 어느 한항에 있어서, 환원시키려는 금속염을 액체형태로 용융된 염의 배드중에 위치시킴을 특징으로 하는 방법.
  7. 제 1 내지 5 항중 어느 한항에 있어서, 환원시키려는 금속염을 개스 형태로 용융된 염의 배드중에 위치시킴을 특징으로 하는 방법
  8. 제 1 내지 5 항중 어느 한항에 있어서, 환원시키려는 금속염을 고체형태로 용융된 염의 배드중에 위치시킴을 특징으로 하는 방법.
  9. 전술된 항들중 어느 한항에 있어서, 리튬을 환원시키려는 금속염에 관한 화학양론적 양으로 도입시킴을 특징으로 하는 방법.
  10. 전술된 항들중 어느 한항에 있어서, 환원시키려는 금속염이 할라이드임을 특징으로 하는 방법.
  11. 제 10 항에 있어서, 환원시키려는 금속염이 염화물임을 특징으로 하는 방법.
  12. 제 11 항에 있어서, 환원시키려는 금속염이 사염화티탄임을 특징으로 하는 방법.
  13. 제 11 항에 있어서, 환원시키려는 금속염이 삼염화 네오디뮴임을 특징으로 하는 방법.
  14. 제 11 항에 있어서, 환원시키려는 금속염이 염화니오븀 임을 특징으로 하는 방법.
  15. 전술된 항들중 어느 한항에 있어서, 언급된 용융염의 배드가 알칼리금속 및 알칼리토금속 할라이드 중에서 선택된 할라이드의 혼합물로 이루어짐을 특징으로 하는 방법.
  16. 제 15 항에 있어서, 언급된 용융 염의 배드가 공융 혼합물에 상당함을 특징으로 하는 방법.
  17. 제 15 또는 15 항에 있어서, 언급된 용융 염의 배드가 염화리튬과 염화칼륨과의 공융 혼합물임을 특징으로 하는 방법.
  18. 전술된 항들중 어느 한항에 있어서, 언급된 용융염의 배드가 온도가 400o내지 550oC 임을 특징으로 하는 방법.
  19. 제 18 항에 있어서, 언급된 온도가 500oC 임을 특징으로 하는 방법.
  20. 전술된 항들중 어느 하나의 항에서 청구된 방법으로 제조된 금속 분말.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019870001741A 1986-02-28 1987-02-27 리티오써미아 방법에 의한 금속분말의 제조방법 KR910006946B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR8602792 1986-02-28
FR2792/86 1986-02-28
FR8602792A FR2595101A1 (fr) 1986-02-28 1986-02-28 Procede de preparation par lithiothermie de poudres metalliques

Publications (2)

Publication Number Publication Date
KR870007743A true KR870007743A (ko) 1987-09-21
KR910006946B1 KR910006946B1 (ko) 1991-09-14

Family

ID=9332628

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019870001741A KR910006946B1 (ko) 1986-02-28 1987-02-27 리티오써미아 방법에 의한 금속분말의 제조방법

Country Status (8)

Country Link
US (1) US4725312A (ko)
EP (1) EP0236221B1 (ko)
JP (1) JPS62240704A (ko)
KR (1) KR910006946B1 (ko)
AT (1) ATE64627T1 (ko)
CA (1) CA1286507C (ko)
DE (1) DE3770834D1 (ko)
FR (1) FR2595101A1 (ko)

Families Citing this family (38)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4865644A (en) * 1987-07-23 1989-09-12 Westinghouse Electric Corporation Superconducting niobium alloys
US4897116A (en) * 1988-05-25 1990-01-30 Teledyne Industries, Inc. High purity Zr and Hf metals and their manufacture
US5259862A (en) * 1992-10-05 1993-11-09 The United States Of America As Represented By The Secretary Of The Interior Continuous production of granular or powder Ti, Zr and Hf or their alloy products
US5442978A (en) * 1994-05-19 1995-08-22 H. C. Starck, Inc. Tantalum production via a reduction of K2TAF7, with diluent salt, with reducing agent provided in a fast series of slug additions
KR100241134B1 (ko) * 1994-08-01 2000-03-02 리차드 피. 앤더슨 금속 및 다른 원소들의 제조방법
US7435282B2 (en) 1994-08-01 2008-10-14 International Titanium Powder, Llc Elemental material and alloy
US7445658B2 (en) 1994-08-01 2008-11-04 Uchicago Argonne, Llc Titanium and titanium alloys
US20030145682A1 (en) * 1994-08-01 2003-08-07 Kroftt-Brakston International, Inc. Gel of elemental material or alloy and liquid metal and salt
US20030061907A1 (en) * 1994-08-01 2003-04-03 Kroftt-Brakston International, Inc. Gel of elemental material or alloy and liquid metal and salt
US7621977B2 (en) * 2001-10-09 2009-11-24 Cristal Us, Inc. System and method of producing metals and alloys
US7416697B2 (en) 2002-06-14 2008-08-26 General Electric Company Method for preparing a metallic article having an other additive constituent, without any melting
USRE45353E1 (en) * 2002-07-17 2015-01-27 Crucible Intellectual Property, Llc Method of making dense composites of bulk-solidifying amorphous alloys and articles thereof
UA79310C2 (en) * 2002-09-07 2007-06-11 Int Titanium Powder Llc Methods for production of alloys or ceramics with the use of armstrong method and device for their realization
WO2004022800A1 (en) * 2002-09-07 2004-03-18 International Titanium Powder, Llc. Process for separating ti from a ti slurry
US20050284824A1 (en) * 2002-09-07 2005-12-29 International Titanium Powder, Llc Filter cake treatment apparatus and method
WO2004033737A1 (en) * 2002-10-07 2004-04-22 International Titanium Powder, Llc. System and method of producing metals and alloys
BR0204587A (pt) 2002-11-04 2004-06-29 Cbmm Sa Processo de produção de pó de nióbio e/ou de tântalo de elevada área superficial
US6968990B2 (en) * 2003-01-23 2005-11-29 General Electric Company Fabrication and utilization of metallic powder prepared without melting
US20070180951A1 (en) * 2003-09-03 2007-08-09 Armstrong Donn R Separation system, method and apparatus
US7531021B2 (en) 2004-11-12 2009-05-12 General Electric Company Article having a dispersion of ultrafine titanium boride particles in a titanium-base matrix
WO2006098055A1 (ja) * 2005-03-15 2006-09-21 Sumitomo Titanium Corporation 高融点金属の分離回収方法
US20070017319A1 (en) * 2005-07-21 2007-01-25 International Titanium Powder, Llc. Titanium alloy
JP2009511739A (ja) 2005-10-06 2009-03-19 インターナショナル・タイテイニアム・パウダー・リミテッド・ライアビリティ・カンパニー ホウ化チタン
US20080031766A1 (en) * 2006-06-16 2008-02-07 International Titanium Powder, Llc Attrited titanium powder
US20100288649A1 (en) * 2006-10-11 2010-11-18 Pal Uday B Magnesiothermic som process for production of metals
US7753989B2 (en) * 2006-12-22 2010-07-13 Cristal Us, Inc. Direct passivation of metal powder
US9127333B2 (en) * 2007-04-25 2015-09-08 Lance Jacobsen Liquid injection of VCL4 into superheated TiCL4 for the production of Ti-V alloy powder
CN102470443B (zh) * 2009-07-17 2014-10-15 波士顿电子材料有限公司 金属粉末和合金的制造和应用
RU2466198C1 (ru) * 2011-06-14 2012-11-10 Открытое Акционерное Общество "Корпорация Всмпо-Ависма" Способ получения губчатого титана
JP6228550B2 (ja) 2011-12-22 2017-11-08 ユニヴァーサル テクニカル リソース サービシーズ インコーポレイテッド チタンの抽出および精錬のための装置および方法
CN103305876B (zh) * 2013-06-05 2015-08-12 哈尔滨工程大学 熔盐电解和还原萃取连用提取镨并制得铝锂镨合金的方法
RU2559075C2 (ru) * 2013-11-26 2015-08-10 ООО "Современные химические и металлургические технологии" (ООО "СХИМТ") Способ алюмотермического получения титана
WO2014209173A1 (ru) * 2013-06-28 2014-12-31 Общество с ограниченной ответственностью "Современные химические и металлургические технологии" Способ получения титана восстановлением из тетрахлорида титана
RU2549795C2 (ru) * 2013-06-28 2015-04-27 Общество с ограниченной ответственностью "Современные химические и металлургические технологии" (ООО "СХИМТ") Способ получения титана и устройство для его осуществления
US10245642B2 (en) * 2015-02-23 2019-04-02 Nanoscale Powders LLC Methods for producing metal powders
EP3512970B1 (en) 2016-09-14 2021-05-12 Universal Achemetal Titanium, LLC A method for producing titanium-aluminum-vanadium alloy
AU2018249909B2 (en) 2017-01-13 2023-04-06 Universal Achemetal Titanium, Llc Titanium master alloy for titanium-aluminum based alloys
CN113500204A (zh) * 2021-07-08 2021-10-15 安徽理工大学 一种氯化钙熔盐中钙热还原氯化铌制备细微铌粉的方法

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2839385A (en) * 1954-12-08 1958-06-17 Du Pont Method of producing titanium metal
US2913332A (en) * 1957-04-05 1959-11-17 Dow Chemical Co Production of titanium metal
US4105440A (en) * 1969-09-05 1978-08-08 Battelle Memorial Institute Process for reducing metal halides by reaction with calcium carbide
US3966458A (en) * 1974-09-06 1976-06-29 Amax Speciality Metal Corporation Separation of zirconium and hafnium
US4032328A (en) * 1975-10-23 1977-06-28 University Of Minnesota, Inc. Metal reduction process
US4149876A (en) * 1978-06-06 1979-04-17 Fansteel Inc. Process for producing tantalum and columbium powder
FR2432553A1 (fr) * 1978-07-31 1980-02-29 Pechiney Aluminium Procede et dispositif de traitement d'un metal ou alliage liquide au moyen de flux liquide et solide
US4252564A (en) * 1979-08-21 1981-02-24 The United States Of America As Represented By The United States Department Of Energy Method for cleaning bomb-reduced uranium derbies
US4468248A (en) * 1980-12-22 1984-08-28 Occidental Research Corporation Process for making titanium metal from titanium ore
US4519837A (en) * 1981-10-08 1985-05-28 Westinghouse Electric Corp. Metal powders and processes for production from oxides
US4556420A (en) * 1982-04-30 1985-12-03 Westinghouse Electric Corp. Process for combination metal reduction and distillation
US4578242A (en) * 1984-07-03 1986-03-25 General Motors Corporation Metallothermic reduction of rare earth oxides
US4602947A (en) * 1984-11-01 1986-07-29 Alti Corporation Process for producing titanium metal and titanium metal alloys
FR2582019B1 (fr) * 1985-05-17 1987-06-26 Extramet Sa Procede pour la production de metaux par reduction de sels metalliques, metaux ainsi obtenus et dispositif pour sa mise en oeuvre
US4668287A (en) * 1985-09-26 1987-05-26 Westinghouse Electric Corp. Process for producing high purity zirconium and hafnium
US4680055A (en) * 1986-03-18 1987-07-14 General Motors Corporation Metallothermic reduction of rare earth chlorides

Also Published As

Publication number Publication date
JPS6365723B2 (ko) 1988-12-16
KR910006946B1 (ko) 1991-09-14
FR2595101A1 (fr) 1987-09-04
DE3770834D1 (de) 1991-07-25
ATE64627T1 (de) 1991-07-15
EP0236221A1 (fr) 1987-09-09
US4725312A (en) 1988-02-16
EP0236221B1 (fr) 1991-06-19
JPS62240704A (ja) 1987-10-21
CA1286507C (fr) 1991-07-23

Similar Documents

Publication Publication Date Title
KR870007743A (ko) 리티오써미아 방법에 의한 금속분말의 제조방법
KR900004967A (ko) 염화 지르코늄, 하프늄 또는 티타늄을 금속 생성물로 환원시키는 방법
BR8701216A (pt) Processo metalotermica para reduzir carga de alimentacao de terra rara em metal de terra rara
GB1351950A (en) Method of removing mercury vapour from gases
BR8503141A (pt) Processo metalotermico nao eletrolitico,de reducao de oxido de terra rara em metal de terra rara
KR880000328A (ko) 할라이드 유리된 금속산화물의 제조방법
KR850003284A (ko) 산화마그네슘의 불용성화합물을 이용한 수성방사능 폐기물의 고체화 방법
DE3688274D1 (de) Verfahren zur synthese aus schmelzloesungen von ktiop04-typ-kristallen oder monophosphaten von kalium und titanyl.
KR850000045A (ko) 알루미늄 전해환원조 라이닝
KR860002446A (ko) 2,4-디클로로-5-플루오로-벤조산의 제조방법
FR2393761A1 (fr) Procede pour produire du peroxyde de chlore
GB1519291A (en) Water treatment
KR870001333A (ko) 규소, 티타늄, 지르코니움 혹은 우라늄의 불화물 환원공정
GB1339784A (en) Production of mixed oxides containing aluminium oxide
ES2019006A6 (es) Un procedimiento para reducir el contenido de perclorato en electrolitos destinados a la produccion de clorato.
GB1486759A (en) Chemical process
GB1466234A (en) Process for the halogenation of copper phthalocyanine
GB1504807A (en) Method of and salt baths for nitriding metals
SE7512932L (sv) Elektrolytisk utfellningsforfarande
SU419576A1 (ru) Состав ванны для сульфоцианирования
SU663711A1 (ru) Способ химической обработки буровых растворов
GB1464356A (en) Process for the purification of vinylidene chloride
SU512993A1 (ru) Способ растворени фторидов щелочноземельных металлов
SU539983A1 (ru) Водный раствор дл химического оксидировани алюмини и его сплавов
SU770220A1 (ru) Способ переработки материала, содержащего благородные металлы, хлорированием

Legal Events

Date Code Title Description
A201 Request for examination
G160 Decision to publish patent application
E701 Decision to grant or registration of patent right
NORF Unpaid initial registration fee