KR102294179B1 - 폴리에테르 카르보네이트 폴리올의 제조 방법 - Google Patents

폴리에테르 카르보네이트 폴리올의 제조 방법 Download PDF

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KR102294179B1
KR102294179B1 KR1020167013069A KR20167013069A KR102294179B1 KR 102294179 B1 KR102294179 B1 KR 102294179B1 KR 1020167013069 A KR1020167013069 A KR 1020167013069A KR 20167013069 A KR20167013069 A KR 20167013069A KR 102294179 B1 KR102294179 B1 KR 102294179B1
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acid
diol
reactor
esters
mono
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KR20160079817A (ko
Inventor
외르크 호프만
한스-게오르크 피르클
카이 라엠머르홀트
하르트무트 네프츠거
마티아스 보하크
스테파니에 브라운
크리스토프 귀르틀러
아우렐 볼프
옌스 랑간케
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코베스트로 도이칠란트 아게
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/20—General preparatory processes
    • C08G64/32—General preparatory processes using carbon dioxide
    • C08G64/34—General preparatory processes using carbon dioxide and cyclic ethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/20—General preparatory processes
    • C08G64/32—General preparatory processes using carbon dioxide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
    • C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2669—Non-metals or compounds thereof
    • C08G65/2675—Phosphorus or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/269—Mixed catalyst systems, i.e. containing more than one reactive component or catalysts formed in-situ

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Polyethers (AREA)
KR1020167013069A 2013-10-23 2014-10-20 폴리에테르 카르보네이트 폴리올의 제조 방법 Expired - Fee Related KR102294179B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP20130189805 EP2865700A1 (de) 2013-10-23 2013-10-23 Verfahren zur Herstellung von Polyethercarbonatpolyolen
EP13189805.8 2013-10-23
PCT/EP2014/072389 WO2015059068A1 (de) 2013-10-23 2014-10-20 Verfahren zur herstellung von polyethercarbonatpolyolen

Publications (2)

Publication Number Publication Date
KR20160079817A KR20160079817A (ko) 2016-07-06
KR102294179B1 true KR102294179B1 (ko) 2021-09-01

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Country Status (9)

Country Link
US (1) US10125217B2 (https=)
EP (2) EP2865700A1 (https=)
JP (1) JP6434010B2 (https=)
KR (1) KR102294179B1 (https=)
CN (1) CN105637014B (https=)
ES (1) ES2643517T3 (https=)
SA (1) SA516370995B1 (https=)
SG (1) SG11201602854RA (https=)
WO (1) WO2015059068A1 (https=)

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EP2845871A1 (de) * 2013-09-05 2015-03-11 Bayer MaterialScience AG Vernetzung von Doppelbindungen enthaltenden Polyethercarbonatpolyolen durch Addition von Mercaptanen
EP3050907A1 (de) * 2015-01-28 2016-08-03 Covestro Deutschland AG Verfahren zur Herstellung von Polyethercarbonatpolyolen
EP3219741A1 (de) * 2016-03-18 2017-09-20 Covestro Deutschland AG Verfahren zur herstellung von polyethercarbonatpolyolen
EP3260483A1 (de) * 2016-06-22 2017-12-27 Covestro Deutschland AG Verfahren zur herstellung von polyethercarbonatpolyolen
EP3538588B1 (en) * 2016-11-11 2023-01-25 Dow Global Technologies LLC Polycarbonate based polyols
EP3385295A1 (de) * 2017-04-05 2018-10-10 Covestro Deutschland AG Flammgeschützte phosphorfunktionelle polyethercarbonatpolyole und verfahren zu deren herstellung
WO2019076862A1 (de) * 2017-10-18 2019-04-25 Covestro Deutschland Ag Diblockcopolymere und deren verwendung als tenside
EP3527606A1 (de) 2018-02-16 2019-08-21 Covestro Deutschland AG Verfahren zur herstellung von polyethercarbonatpolyolen
GB201906214D0 (en) 2019-05-02 2019-06-19 Econic Tech Ltd A polyol block copolymer, compositions and processes therefor
GB201906210D0 (en) 2019-05-02 2019-06-19 Econic Tech Limited A polyol block copolymer, compositions and processes therefor
WO2021032553A1 (de) * 2019-08-19 2021-02-25 Covestro Intellectual Property Gmbh & Co. Kg Verfahren zur herstellung von polyethercarbonatalkoholen
KR20220111266A (ko) * 2019-12-04 2022-08-09 코베스트로 인텔렉쳐 프로퍼티 게엠베하 운트 콤파니 카게 폴리에테르 카르보네이트 폴리올을 제조하는 방법
GB202003002D0 (en) 2020-03-02 2020-04-15 Crane Ltd Method of preparation of a polyol block copolymer
GB202003003D0 (en) 2020-03-02 2020-04-15 Econic Tech Ltd A polyol block copolymer
JP7845040B2 (ja) * 2021-05-27 2026-04-14 Ａｇｃ株式会社 ポリオキシアルキレンポリカーボネートジオール及びその製造方法、ポリウレタン樹脂前駆体、ポリウレタン樹脂、ポリウレタン樹脂組成物、並びに物品
EP4384316A1 (en) * 2021-08-11 2024-06-19 Econic Technologies Ltd Method for preparing surfactants by copolymerisation of epoxides and co2 using a mixture of a macrocyclic bimetal catalyst and a double metal cyanide catalyst
CN113980264B (zh) * 2021-11-30 2023-02-28 江苏钟山新材料有限公司 一种阻燃聚醚多元醇的制备方法及其应用
CN114409960B (zh) * 2022-01-21 2023-05-09 深圳市那鸿科技有限公司 一种阻燃/抗氧协同助剂及其合成方法和在回收pet中的应用

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EP3060596B1 (de) 2017-09-20
EP3060596A1 (de) 2016-08-31
CN105637014A (zh) 2016-06-01
WO2015059068A1 (de) 2015-04-30
US20160264727A1 (en) 2016-09-15
SG11201602854RA (en) 2016-05-30
SA516370995B1 (ar) 2018-03-05
ES2643517T3 (es) 2017-11-23
US10125217B2 (en) 2018-11-13
EP2865700A1 (de) 2015-04-29
JP6434010B2 (ja) 2018-12-05
JP2016538371A (ja) 2016-12-08
KR20160079817A (ko) 2016-07-06
CN105637014B (zh) 2018-09-14

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