JP6434010B2 - ポリエーテルカーボネートポリオールを製造する方法 - Google Patents

ポリエーテルカーボネートポリオールを製造する方法 Download PDF

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Publication number
JP6434010B2
JP6434010B2 JP2016525883A JP2016525883A JP6434010B2 JP 6434010 B2 JP6434010 B2 JP 6434010B2 JP 2016525883 A JP2016525883 A JP 2016525883A JP 2016525883 A JP2016525883 A JP 2016525883A JP 6434010 B2 JP6434010 B2 JP 6434010B2
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Prior art keywords
acid
diol
reactor
mono
esters
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Expired - Fee Related
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JP2016525883A
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Japanese (ja)
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JP2016538371A (ja
JP2016538371A5 (https=
Inventor
イェルク、ホフマン
ハンス−ゲオルク、パークル
カイ、レマーホルト
ハルトムート、ネフツガー
マティアス、ボハク
シュテファニー、ブラウン
クリストフ、ギュルトラー
オーレル、ボルフ
イェンス、ランガンク
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Covestro Deutschland AG
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Covestro Deutschland AG
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/20—General preparatory processes
    • C08G64/32—General preparatory processes using carbon dioxide
    • C08G64/34—General preparatory processes using carbon dioxide and cyclic ethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/20—General preparatory processes
    • C08G64/32—General preparatory processes using carbon dioxide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
    • C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2669—Non-metals or compounds thereof
    • C08G65/2675—Phosphorus or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/269—Mixed catalyst systems, i.e. containing more than one reactive component or catalysts formed in-situ

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Polyethers (AREA)
JP2016525883A 2013-10-23 2014-10-20 ポリエーテルカーボネートポリオールを製造する方法 Expired - Fee Related JP6434010B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP20130189805 EP2865700A1 (de) 2013-10-23 2013-10-23 Verfahren zur Herstellung von Polyethercarbonatpolyolen
EP13189805.8 2013-10-23
PCT/EP2014/072389 WO2015059068A1 (de) 2013-10-23 2014-10-20 Verfahren zur herstellung von polyethercarbonatpolyolen

Publications (3)

Publication Number Publication Date
JP2016538371A JP2016538371A (ja) 2016-12-08
JP2016538371A5 JP2016538371A5 (https=) 2018-10-11
JP6434010B2 true JP6434010B2 (ja) 2018-12-05

Family

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JP2016525883A Expired - Fee Related JP6434010B2 (ja) 2013-10-23 2014-10-20 ポリエーテルカーボネートポリオールを製造する方法

Country Status (9)

Country Link
US (1) US10125217B2 (https=)
EP (2) EP2865700A1 (https=)
JP (1) JP6434010B2 (https=)
KR (1) KR102294179B1 (https=)
CN (1) CN105637014B (https=)
ES (1) ES2643517T3 (https=)
SA (1) SA516370995B1 (https=)
SG (1) SG11201602854RA (https=)
WO (1) WO2015059068A1 (https=)

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EP2845871A1 (de) * 2013-09-05 2015-03-11 Bayer MaterialScience AG Vernetzung von Doppelbindungen enthaltenden Polyethercarbonatpolyolen durch Addition von Mercaptanen
EP3050907A1 (de) * 2015-01-28 2016-08-03 Covestro Deutschland AG Verfahren zur Herstellung von Polyethercarbonatpolyolen
EP3219741A1 (de) * 2016-03-18 2017-09-20 Covestro Deutschland AG Verfahren zur herstellung von polyethercarbonatpolyolen
EP3260483A1 (de) * 2016-06-22 2017-12-27 Covestro Deutschland AG Verfahren zur herstellung von polyethercarbonatpolyolen
EP3538588B1 (en) * 2016-11-11 2023-01-25 Dow Global Technologies LLC Polycarbonate based polyols
EP3385295A1 (de) * 2017-04-05 2018-10-10 Covestro Deutschland AG Flammgeschützte phosphorfunktionelle polyethercarbonatpolyole und verfahren zu deren herstellung
WO2019076862A1 (de) * 2017-10-18 2019-04-25 Covestro Deutschland Ag Diblockcopolymere und deren verwendung als tenside
EP3527606A1 (de) 2018-02-16 2019-08-21 Covestro Deutschland AG Verfahren zur herstellung von polyethercarbonatpolyolen
GB201906214D0 (en) 2019-05-02 2019-06-19 Econic Tech Ltd A polyol block copolymer, compositions and processes therefor
GB201906210D0 (en) 2019-05-02 2019-06-19 Econic Tech Limited A polyol block copolymer, compositions and processes therefor
WO2021032553A1 (de) * 2019-08-19 2021-02-25 Covestro Intellectual Property Gmbh & Co. Kg Verfahren zur herstellung von polyethercarbonatalkoholen
KR20220111266A (ko) * 2019-12-04 2022-08-09 코베스트로 인텔렉쳐 프로퍼티 게엠베하 운트 콤파니 카게 폴리에테르 카르보네이트 폴리올을 제조하는 방법
GB202003002D0 (en) 2020-03-02 2020-04-15 Crane Ltd Method of preparation of a polyol block copolymer
GB202003003D0 (en) 2020-03-02 2020-04-15 Econic Tech Ltd A polyol block copolymer
JP7845040B2 (ja) * 2021-05-27 2026-04-14 Ａｇｃ株式会社 ポリオキシアルキレンポリカーボネートジオール及びその製造方法、ポリウレタン樹脂前駆体、ポリウレタン樹脂、ポリウレタン樹脂組成物、並びに物品
EP4384316A1 (en) * 2021-08-11 2024-06-19 Econic Technologies Ltd Method for preparing surfactants by copolymerisation of epoxides and co2 using a mixture of a macrocyclic bimetal catalyst and a double metal cyanide catalyst
CN113980264B (zh) * 2021-11-30 2023-02-28 江苏钟山新材料有限公司 一种阻燃聚醚多元醇的制备方法及其应用
CN114409960B (zh) * 2022-01-21 2023-05-09 深圳市那鸿科技有限公司 一种阻燃/抗氧协同助剂及其合成方法和在回收pet中的应用

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Also Published As

Publication number Publication date
EP3060596B1 (de) 2017-09-20
EP3060596A1 (de) 2016-08-31
CN105637014A (zh) 2016-06-01
WO2015059068A1 (de) 2015-04-30
US20160264727A1 (en) 2016-09-15
SG11201602854RA (en) 2016-05-30
SA516370995B1 (ar) 2018-03-05
ES2643517T3 (es) 2017-11-23
US10125217B2 (en) 2018-11-13
EP2865700A1 (de) 2015-04-29
JP2016538371A (ja) 2016-12-08
KR102294179B1 (ko) 2021-09-01
KR20160079817A (ko) 2016-07-06
CN105637014B (zh) 2018-09-14

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