ES2643517T3 - Procedimiento para la preparación de polioletercarbonatos - Google Patents
Procedimiento para la preparación de polioletercarbonatos Download PDFInfo
- Publication number
- ES2643517T3 ES2643517T3 ES14786870.7T ES14786870T ES2643517T3 ES 2643517 T3 ES2643517 T3 ES 2643517T3 ES 14786870 T ES14786870 T ES 14786870T ES 2643517 T3 ES2643517 T3 ES 2643517T3
- Authority
- ES
- Spain
- Prior art keywords
- acid
- functionality
- ester
- phosphoric acid
- reactor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/32—General preparatory processes using carbon dioxide
- C08G64/34—General preparatory processes using carbon dioxide and cyclic ethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/20—General preparatory processes
- C08G64/32—General preparatory processes using carbon dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
- C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
- C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2663—Metal cyanide catalysts, i.e. DMC's
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2669—Non-metals or compounds thereof
- C08G65/2675—Phosphorus or compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/269—Mixed catalyst systems, i.e. containing more than one reactive component or catalysts formed in-situ
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Toxicology (AREA)
- Polyesters Or Polycarbonates (AREA)
- Polyethers (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP20130189805 EP2865700A1 (de) | 2013-10-23 | 2013-10-23 | Verfahren zur Herstellung von Polyethercarbonatpolyolen |
| EP13189805 | 2013-10-23 | ||
| PCT/EP2014/072389 WO2015059068A1 (de) | 2013-10-23 | 2014-10-20 | Verfahren zur herstellung von polyethercarbonatpolyolen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2643517T3 true ES2643517T3 (es) | 2017-11-23 |
Family
ID=49484147
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES14786870.7T Active ES2643517T3 (es) | 2013-10-23 | 2014-10-20 | Procedimiento para la preparación de polioletercarbonatos |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US10125217B2 (https=) |
| EP (2) | EP2865700A1 (https=) |
| JP (1) | JP6434010B2 (https=) |
| KR (1) | KR102294179B1 (https=) |
| CN (1) | CN105637014B (https=) |
| ES (1) | ES2643517T3 (https=) |
| SA (1) | SA516370995B1 (https=) |
| SG (1) | SG11201602854RA (https=) |
| WO (1) | WO2015059068A1 (https=) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2845871A1 (de) * | 2013-09-05 | 2015-03-11 | Bayer MaterialScience AG | Vernetzung von Doppelbindungen enthaltenden Polyethercarbonatpolyolen durch Addition von Mercaptanen |
| EP3050907A1 (de) * | 2015-01-28 | 2016-08-03 | Covestro Deutschland AG | Verfahren zur Herstellung von Polyethercarbonatpolyolen |
| EP3219741A1 (de) * | 2016-03-18 | 2017-09-20 | Covestro Deutschland AG | Verfahren zur herstellung von polyethercarbonatpolyolen |
| EP3260483A1 (de) * | 2016-06-22 | 2017-12-27 | Covestro Deutschland AG | Verfahren zur herstellung von polyethercarbonatpolyolen |
| EP3538588B1 (en) * | 2016-11-11 | 2023-01-25 | Dow Global Technologies LLC | Polycarbonate based polyols |
| EP3385295A1 (de) * | 2017-04-05 | 2018-10-10 | Covestro Deutschland AG | Flammgeschützte phosphorfunktionelle polyethercarbonatpolyole und verfahren zu deren herstellung |
| WO2019076862A1 (de) * | 2017-10-18 | 2019-04-25 | Covestro Deutschland Ag | Diblockcopolymere und deren verwendung als tenside |
| EP3527606A1 (de) | 2018-02-16 | 2019-08-21 | Covestro Deutschland AG | Verfahren zur herstellung von polyethercarbonatpolyolen |
| GB201906214D0 (en) | 2019-05-02 | 2019-06-19 | Econic Tech Ltd | A polyol block copolymer, compositions and processes therefor |
| GB201906210D0 (en) | 2019-05-02 | 2019-06-19 | Econic Tech Limited | A polyol block copolymer, compositions and processes therefor |
| WO2021032553A1 (de) * | 2019-08-19 | 2021-02-25 | Covestro Intellectual Property Gmbh & Co. Kg | Verfahren zur herstellung von polyethercarbonatalkoholen |
| KR20220111266A (ko) * | 2019-12-04 | 2022-08-09 | 코베스트로 인텔렉쳐 프로퍼티 게엠베하 운트 콤파니 카게 | 폴리에테르 카르보네이트 폴리올을 제조하는 방법 |
| GB202003002D0 (en) | 2020-03-02 | 2020-04-15 | Crane Ltd | Method of preparation of a polyol block copolymer |
| GB202003003D0 (en) | 2020-03-02 | 2020-04-15 | Econic Tech Ltd | A polyol block copolymer |
| JP7845040B2 (ja) * | 2021-05-27 | 2026-04-14 | Ａｇｃ株式会社 | ポリオキシアルキレンポリカーボネートジオール及びその製造方法、ポリウレタン樹脂前駆体、ポリウレタン樹脂、ポリウレタン樹脂組成物、並びに物品 |
| EP4384316A1 (en) * | 2021-08-11 | 2024-06-19 | Econic Technologies Ltd | Method for preparing surfactants by copolymerisation of epoxides and co2 using a mixture of a macrocyclic bimetal catalyst and a double metal cyanide catalyst |
| CN113980264B (zh) * | 2021-11-30 | 2023-02-28 | 江苏钟山新材料有限公司 | 一种阻燃聚醚多元醇的制备方法及其应用 |
| CN114409960B (zh) * | 2022-01-21 | 2023-05-09 | 深圳市那鸿科技有限公司 | 一种阻燃/抗氧协同助剂及其合成方法和在回收pet中的应用 |
Family Cites Families (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1063525A (en) | 1963-02-14 | 1967-03-30 | Gen Tire & Rubber Co | Organic cyclic oxide polymers, their preparation and tires prepared therefrom |
| US3829505A (en) | 1970-02-24 | 1974-08-13 | Gen Tire & Rubber Co | Polyethers and method for making the same |
| US3941849A (en) | 1972-07-07 | 1976-03-02 | The General Tire & Rubber Company | Polyethers and method for making the same |
| US4145525A (en) * | 1977-10-03 | 1979-03-20 | Air Products And Chemicals, Inc. | End capped polyalkylene carbonates |
| AU552988B2 (en) * | 1982-03-31 | 1986-06-26 | Shell Internationale Research Maatschappij B.V. | Polymerizing epoxides and catalyst suspensions for this |
| GB8528071D0 (en) | 1985-11-14 | 1985-12-18 | Shell Int Research | Polycarbonates |
| JP2653236B2 (ja) | 1990-10-05 | 1997-09-17 | 旭硝子株式会社 | ポリエーテル化合物の製造方法 |
| US5158922A (en) | 1992-02-04 | 1992-10-27 | Arco Chemical Technology, L.P. | Process for preparing metal cyanide complex catalyst |
| US5712216A (en) | 1995-05-15 | 1998-01-27 | Arco Chemical Technology, L.P. | Highly active double metal cyanide complex catalysts |
| US5470813A (en) | 1993-11-23 | 1995-11-28 | Arco Chemical Technology, L.P. | Double metal cyanide complex catalysts |
| US5482908A (en) | 1994-09-08 | 1996-01-09 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
| US5545601A (en) | 1995-08-22 | 1996-08-13 | Arco Chemical Technology, L.P. | Polyether-containing double metal cyanide catalysts |
| US5777177A (en) * | 1996-02-07 | 1998-07-07 | Arco Chemical Technology, L.P. | Preparation of double metal cyanide-catalyzed polyols by continuous addition of starter |
| US5627120A (en) | 1996-04-19 | 1997-05-06 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
| US5714428A (en) | 1996-10-16 | 1998-02-03 | Arco Chemical Technology, L.P. | Double metal cyanide catalysts containing functionalized polymers |
| DE19905611A1 (de) | 1999-02-11 | 2000-08-17 | Bayer Ag | Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen |
| DE19958355A1 (de) | 1999-12-03 | 2001-06-07 | Bayer Ag | Verfahren zur Herstellung von DMC-Katalysatoren |
| AU2001260217A1 (en) | 2000-04-20 | 2001-11-07 | Bayer Aktiengesellschaft | Method for producing double metal cyanide (dmc) catalysts |
| DE10147712A1 (de) | 2001-09-27 | 2003-04-17 | Basf Ag | Verfahren zur Herstellung aliphatischer Polycarbonate |
| DE10219028A1 (de) | 2002-04-29 | 2003-11-06 | Bayer Ag | Herstellung und Verwendung von hochmolekularen aliphatischen Polycarbonaten |
| JP4145123B2 (ja) | 2002-11-18 | 2008-09-03 | 株式会社オンダ製作所 | 継手 |
| US20050209438A1 (en) | 2004-03-19 | 2005-09-22 | Browne Edward P | Starter feed stream acidification in DMC-catalyzed process |
| US7304172B2 (en) | 2004-10-08 | 2007-12-04 | Cornell Research Foundation, Inc. | Polycarbonates made using highly selective catalysts |
| US7671228B2 (en) * | 2005-03-29 | 2010-03-02 | Basf Corporation | Method of forming a polyethercarbonate polyol using a CO2-philic compound or substituent |
| DE102006024025A1 (de) * | 2006-05-23 | 2007-11-29 | Bayer Materialscience Ag | Verfahren zur Herstellung von Polyetherpolyolen |
| KR101455878B1 (ko) | 2006-11-15 | 2014-11-03 | 바스프 에스이 | 연질 폴리우레탄 발포체의 제조 방법 |
| CN101611074B (zh) | 2007-01-30 | 2012-07-25 | 巴斯夫欧洲公司 | 制备聚醚碳酸酯多元醇的方法 |
| CA2727959A1 (en) | 2008-07-30 | 2010-02-04 | Sk Energy, Co., Ltd. | Novel coordination complexes and process of producing polycarbonate by copolymerization of carbon dioxide and epoxide using the same as catalyst |
| DE102010040517A1 (de) * | 2010-09-09 | 2012-03-15 | Bayer Materialscience Aktiengesellschaft | Verfahren zur Herstellung von Polyetherpolyolen |
| KR101415574B1 (ko) * | 2011-02-10 | 2014-07-04 | 아주대학교산학협력단 | 난연 이산화탄소/에폭사이드 공중합체 및 이의 제조 방법 |
| EP2548906A1 (de) * | 2011-07-18 | 2013-01-23 | Bayer MaterialScience AG | Verfahren zur Aktivierung von Doppelmetallcyanidkatalysatoren zur Herstellung von Polyetherpolyolen |
| EP2703426A1 (de) | 2012-08-27 | 2014-03-05 | Bayer MaterialScience AG | Verfahren zur Herstellung von Polyethercarbonatpolyolen |
| EP2703425A1 (de) | 2012-08-27 | 2014-03-05 | Bayer MaterialScience AG | Verfahren zur Herstellung von Polyethercarbonatpolyolen |
| SG11201600626YA (en) * | 2013-08-02 | 2016-03-30 | Covestro Deutschland Ag | Method for producing polyether carbonate polyols |
| KR102333890B1 (ko) * | 2014-07-03 | 2021-12-02 | 코베스트로 도이칠란트 아게 | 폴리에테르 카르보네이트 폴리올의 제조 방법 |
-
2013
- 2013-10-23 EP EP20130189805 patent/EP2865700A1/de not_active Withdrawn
-
2014
- 2014-10-20 SG SG11201602854RA patent/SG11201602854RA/en unknown
- 2014-10-20 WO PCT/EP2014/072389 patent/WO2015059068A1/de not_active Ceased
- 2014-10-20 US US15/030,523 patent/US10125217B2/en active Active
- 2014-10-20 ES ES14786870.7T patent/ES2643517T3/es active Active
- 2014-10-20 KR KR1020167013069A patent/KR102294179B1/ko not_active Expired - Fee Related
- 2014-10-20 JP JP2016525883A patent/JP6434010B2/ja not_active Expired - Fee Related
- 2014-10-20 EP EP14786870.7A patent/EP3060596B1/de not_active Not-in-force
- 2014-10-20 CN CN201480058165.2A patent/CN105637014B/zh not_active Expired - Fee Related
-
2016
- 2016-04-21 SA SA516370995A patent/SA516370995B1/ar unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP3060596B1 (de) | 2017-09-20 |
| EP3060596A1 (de) | 2016-08-31 |
| CN105637014A (zh) | 2016-06-01 |
| WO2015059068A1 (de) | 2015-04-30 |
| US20160264727A1 (en) | 2016-09-15 |
| SG11201602854RA (en) | 2016-05-30 |
| SA516370995B1 (ar) | 2018-03-05 |
| US10125217B2 (en) | 2018-11-13 |
| EP2865700A1 (de) | 2015-04-29 |
| JP6434010B2 (ja) | 2018-12-05 |
| JP2016538371A (ja) | 2016-12-08 |
| KR102294179B1 (ko) | 2021-09-01 |
| KR20160079817A (ko) | 2016-07-06 |
| CN105637014B (zh) | 2018-09-14 |
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