KR101839585B1 - 디오가노디할로실란의 제조 방법 - Google Patents

디오가노디할로실란의 제조 방법 Download PDF

Info

Publication number
KR101839585B1
KR101839585B1 KR1020127027347A KR20127027347A KR101839585B1 KR 101839585 B1 KR101839585 B1 KR 101839585B1 KR 1020127027347 A KR1020127027347 A KR 1020127027347A KR 20127027347 A KR20127027347 A KR 20127027347A KR 101839585 B1 KR101839585 B1 KR 101839585B1
Authority
KR
South Korea
Prior art keywords
silicon
copper catalyst
catalyst
containing copper
organohalide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020127027347A
Other languages
English (en)
Korean (ko)
Other versions
KR20130079349A (ko
Inventor
디미트리스 카트솔리스
로버트 토마스 라르센
Original Assignee
다우 코닝 코포레이션
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 다우 코닝 코포레이션 filed Critical 다우 코닝 코포레이션
Publication of KR20130079349A publication Critical patent/KR20130079349A/ko
Application granted granted Critical
Publication of KR101839585B1 publication Critical patent/KR101839585B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C07F7/121—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/125—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving both Si-C and Si-halogen linkages, the Si-C and Si-halogen linkages can be to the same or to different Si atoms, e.g. redistribution reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/72—Copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/12—Organo silicon halides
    • C07F7/121—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20
    • C07F7/122—Preparation or treatment not provided for in C07F7/14, C07F7/16 or C07F7/20 by reactions involving the formation of Si-C linkages

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020127027347A 2010-05-28 2011-03-31 디오가노디할로실란의 제조 방법 Active KR101839585B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US34924210P 2010-05-28 2010-05-28
US61/349,242 2010-05-28
PCT/US2011/030683 WO2011149588A1 (en) 2010-05-28 2011-03-31 A method for preparing a diorganodihalosilane

Publications (2)

Publication Number Publication Date
KR20130079349A KR20130079349A (ko) 2013-07-10
KR101839585B1 true KR101839585B1 (ko) 2018-03-16

Family

ID=44065690

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020127027347A Active KR101839585B1 (ko) 2010-05-28 2011-03-31 디오가노디할로실란의 제조 방법

Country Status (6)

Country Link
US (2) US8772525B2 (https=)
EP (1) EP2576573B1 (https=)
JP (1) JP5726294B2 (https=)
KR (1) KR101839585B1 (https=)
CN (1) CN102844322B (https=)
WO (1) WO2011149588A1 (https=)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011094140A2 (en) 2010-01-26 2011-08-04 Dow Corning Corporation Method of preparing an organohalosilane
JP5726294B2 (ja) * 2010-05-28 2015-05-27 ダウ コーニング コーポレーションＤｏｗ Ｃｏｒｎｉｎｇ Ｃｏｒｐｏｒａｔｉｏｎ ジオルガノジハロシランの調製方法
US20130039831A1 (en) * 2011-01-25 2013-02-14 Aswini Dash Method of preparing a hydridohalosilane compound
CN103930430B (zh) * 2011-11-17 2016-03-16 道康宁公司 制备二有机二卤代硅烷的方法
US20150045571A1 (en) * 2012-04-05 2015-02-12 Dow Corning Corporation Method for Preparing an Organofunctional Compound
EP2838845A1 (en) 2012-04-16 2015-02-25 Dow Corning Corporation Processes for the preparation of silicon containing intermetallic compounds and intermetallic compounds prepared thereby
US8865850B2 (en) 2012-06-14 2014-10-21 Dow Corning Corporation Method of selectively forming a reaction product in the presence of a metal silicide
CN104736547A (zh) * 2012-08-13 2015-06-24 道康宁公司 通过使氢、卤硅烷和有机卤化物在铜催化剂上以两步法反应制备有机卤硅烷的方法
EP2909217B1 (en) 2012-10-16 2016-10-26 Dow Corning Corporation Method of preparing halogenated silahydrocarbylenes
WO2014099125A1 (en) * 2012-12-19 2014-06-26 Dow Corning Corporation Method for preparing a diorganodihalosilane
WO2014149224A1 (en) * 2013-03-15 2014-09-25 Dow Corning Corporation Method for preparing a halosilane using copper silicides as catalysts
KR102299593B1 (ko) 2013-11-12 2021-09-09 다우 실리콘즈 코포레이션 할로실란의 제조 방법
WO2015100075A1 (en) * 2013-12-23 2015-07-02 Dow Corning Corporation Solid binary copper-silicon material catalysts for emissions control
JP6725510B2 (ja) 2014-12-18 2020-07-22 ダウ シリコーンズ コーポレーション アリール官能性シランの製造方法

Family Cites Families (32)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2380996A (en) * 1941-09-26 1945-08-07 Gen Electric Preparation of organosilicon halides
BE473151A (https=) 1945-03-15
US2888476A (en) 1956-08-01 1959-05-26 Du Pont Preparation of long-chain alkylhalosilanes
US3057686A (en) 1957-08-01 1962-10-09 Du Pont Process for preparing silanes
JPS5747917B2 (https=) 1974-08-20 1982-10-13
US4314908A (en) * 1979-10-24 1982-02-09 Union Carbide Corporation Preparation of reaction mass for the production of methylchlorosilane
DE3024319C2 (de) 1980-06-27 1983-07-21 Wacker-Chemitronic Gesellschaft für Elektronik-Grundstoffe mbH, 8263 Burghausen Kontinuierliches Verfahren zur Herstellung von Trichlorsilan
FR2530638A1 (fr) 1982-07-26 1984-01-27 Rhone Poulenc Spec Chim Procede de preparation d'un melange a base de trichlorosilane utilisable pour la preparation de silicium de haute purete
US4526769A (en) 1983-07-18 1985-07-02 Motorola, Inc. Trichlorosilane production process
JPS63118069A (ja) * 1986-11-07 1988-05-23 Sumitomo Electric Ind Ltd 耐食性・耐摩耗性部材
US4973725A (en) * 1988-06-28 1990-11-27 Union Carbide Chemicals And Plastics Company Inc. Direct synthesis process for organohalohydrosilanes
US4946980A (en) 1988-10-17 1990-08-07 Dow Corning Corporation Preparation of organosilanes
US4888435A (en) 1989-06-22 1989-12-19 Dow Corning Corporation Integrated process for alkylation and redistribution of halosilanes
DE4041644A1 (de) 1990-12-22 1992-06-25 Nuenchritz Chemie Gmbh Verfahren zur reduktiven umwandlung von siliciumtetrachlorid in trichlorsilan
TW232751B (en) 1992-10-09 1994-10-21 Semiconductor Energy Res Co Ltd Semiconductor device and method for forming the same
DE19654154A1 (de) 1995-12-25 1997-06-26 Tokuyama Corp Verfahren zur Herstellung von Trichlorsilan
US7223879B2 (en) 1998-07-10 2007-05-29 Massachusetts Institute Of Technology Ligands for metals and improved metal-catalyzed processes based thereon
US6156380A (en) 1998-10-05 2000-12-05 Shin-Etsu Chemical Co., Ltd. Method for preparing contact mass for organohalosilane synthesis
US6528674B1 (en) * 2000-04-20 2003-03-04 General Electric Company Method for preparing a contact mass
DE10044796A1 (de) 2000-09-11 2002-04-04 Bayer Ag Verfahren zur Herstellung von Chlorsilanen
DE10061682A1 (de) 2000-12-11 2002-07-04 Solarworld Ag Verfahren zur Herstellung von Reinstsilicium
ES2300652T3 (es) 2002-08-06 2008-06-16 Loma Linda University Sustancias para prevenir y tratar enfermedades autoinmunes.
US7716590B1 (en) 2002-10-28 2010-05-11 Oracle International Corporation Method and apparatus for dynamically updating a secondary form element based on a selection in a primary form element
US7559969B2 (en) 2003-09-19 2009-07-14 Sri International Methods and apparatuses for producing metallic compositions via reduction of metal halides
JP4841954B2 (ja) 2003-11-28 2011-12-21 北興化学工業株式会社 ホスホニウムボレート化合物の製造方法、新規なホスホニウムボレート化合物およびその使用方法
JP2005292324A (ja) 2004-03-31 2005-10-20 Canon Inc 画像形成装置のクリーニング装置
WO2006081384A2 (en) * 2005-01-26 2006-08-03 The Regents Of The University Of California Heterogeneous copper catalysts
DE102005046703A1 (de) 2005-09-29 2007-04-05 Wacker Chemie Ag Verfahren und Vorrichtung zur Hydrierung von Chlorsilanen
EP2039669A1 (en) 2007-09-19 2009-03-25 Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V. Use of a mixture of an ordered intermetallic compound and an inert material as a catalyst and corresponding hydrogenation processes
JP2009111202A (ja) 2007-10-31 2009-05-21 Panasonic Corp 半導体装置及びその製造方法
JP5726294B2 (ja) * 2010-05-28 2015-05-27 ダウ コーニング コーポレーションＤｏｗ Ｃｏｒｎｉｎｇ Ｃｏｒｐｏｒａｔｉｏｎ ジオルガノジハロシランの調製方法
DE102011005647A1 (de) 2011-03-16 2012-10-04 Evonik Degussa Gmbh Verbundverfahren zur Umstetzung von STC-haltigen und OCS-haltigen Nebenströmen zu wasserstoffhaltigen Chlorsilanen

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Zhurnal Obshchei Khimii, Vol. 48(11), pp. 2534-2541, 1978

Also Published As

Publication number Publication date
CN102844322A (zh) 2012-12-26
JP2013528187A (ja) 2013-07-08
WO2011149588A1 (en) 2011-12-01
CN102844322B (zh) 2015-09-23
US20130066096A1 (en) 2013-03-14
JP5726294B2 (ja) 2015-05-27
US8772525B2 (en) 2014-07-08
US20140256975A1 (en) 2014-09-11
EP2576573B1 (en) 2015-06-24
KR20130079349A (ko) 2013-07-10
EP2576573A1 (en) 2013-04-10

Similar Documents

Publication Publication Date Title
KR101839585B1 (ko) 디오가노디할로실란의 제조 방법
US9296765B2 (en) Method of preparing an organohalosilane
US8765090B2 (en) Method for preparing a trihalosilane
EP2909217B1 (en) Method of preparing halogenated silahydrocarbylenes
KR20130132920A (ko) 트라이할로실란의 제조 방법
US8865927B2 (en) Method for preparing a diorganodihalosilane
US8722915B2 (en) Preparation of organohalosilanes

Legal Events

Date Code Title Description
PA0105 International application

St.27 status event code: A-0-1-A10-A15-nap-PA0105

E13-X000 Pre-grant limitation requested

St.27 status event code: A-2-3-E10-E13-lim-X000

P11-X000 Amendment of application requested

St.27 status event code: A-2-2-P10-P11-nap-X000

P13-X000 Application amended

St.27 status event code: A-2-2-P10-P13-nap-X000

R17-X000 Change to representative recorded

St.27 status event code: A-3-3-R10-R17-oth-X000

PG1501 Laying open of application

St.27 status event code: A-1-1-Q10-Q12-nap-PG1501

A201 Request for examination
PA0201 Request for examination

St.27 status event code: A-1-2-D10-D11-exm-PA0201

P22-X000 Classification modified

St.27 status event code: A-2-2-P10-P22-nap-X000

P22-X000 Classification modified

St.27 status event code: A-2-2-P10-P22-nap-X000

D13-X000 Search requested

St.27 status event code: A-1-2-D10-D13-srh-X000

D14-X000 Search report completed

St.27 status event code: A-1-2-D10-D14-srh-X000

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

St.27 status event code: A-1-2-D10-D21-exm-PE0902

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

St.27 status event code: A-1-2-D10-D22-exm-PE0701

GRNT Written decision to grant
PR0701 Registration of establishment

St.27 status event code: A-2-4-F10-F11-exm-PR0701

PR1002 Payment of registration fee

St.27 status event code: A-2-2-U10-U12-oth-PR1002

Fee payment year number: 1

PG1601 Publication of registration

St.27 status event code: A-4-4-Q10-Q13-nap-PG1601

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 4

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 5

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 6

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 7

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 8

PR1001 Payment of annual fee

St.27 status event code: A-4-4-U10-U11-oth-PR1001

Fee payment year number: 9

U11 Full renewal or maintenance fee paid

Free format text: ST27 STATUS EVENT CODE: A-4-4-U10-U11-OTH-PR1001 (AS PROVIDED BY THE NATIONAL OFFICE)

Year of fee payment: 9

R18 Changes to party contact information recorded

Free format text: ST27 STATUS EVENT CODE: A-5-5-R10-R18-OTH-X000 (AS PROVIDED BY THE NATIONAL OFFICE)

R18-X000 Changes to party contact information recorded

St.27 status event code: A-5-5-R10-R18-oth-X000