KR101554409B1 - 시클로헥산올, 시클로헥산올의 제조 방법 및 아디프산의 제조 방법 - Google Patents

시클로헥산올, 시클로헥산올의 제조 방법 및 아디프산의 제조 방법 Download PDF

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KR101554409B1
KR101554409B1 KR1020137031573A KR20137031573A KR101554409B1 KR 101554409 B1 KR101554409 B1 KR 101554409B1 KR 1020137031573 A KR1020137031573 A KR 1020137031573A KR 20137031573 A KR20137031573 A KR 20137031573A KR 101554409 B1 KR101554409 B1 KR 101554409B1
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cyclohexanol
weight
ppm
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methylcyclopentanol
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KR20140004794A (ko
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나오키 나리사와
가츠토시 다나카
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아사히 가세이 케미칼즈 가부시키가이샤
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/03—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by addition of hydroxy groups to unsaturated carbon-to-carbon bonds, e.g. with the aid of H2O2
    • C07C29/04—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by addition of hydroxy groups to unsaturated carbon-to-carbon bonds, e.g. with the aid of H2O2 by hydration of carbon-to-carbon double bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C35/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
    • C07C35/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic
    • C07C35/08—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic containing a six-membered rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/316—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with oxides of nitrogen or nitrogen-containing mineral acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
KR1020137031573A 2011-07-12 2012-06-28 시클로헥산올, 시클로헥산올의 제조 방법 및 아디프산의 제조 방법 Active KR101554409B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JPJP-P-2011-154023 2011-07-12
JP2011154023 2011-07-12
PCT/JP2012/066545 WO2013008637A1 (ja) 2011-07-12 2012-06-28 シクロヘキサノール、シクロヘキサノールの製造方法及びアジピン酸の製造方法

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KR20140004794A KR20140004794A (ko) 2014-01-13
KR101554409B1 true KR101554409B1 (ko) 2015-09-18

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Country Status (9)

Country Link
US (1) US9771313B2 (cg-RX-API-DMAC7.html)
EP (1) EP2733136B1 (cg-RX-API-DMAC7.html)
JP (1) JP5462981B2 (cg-RX-API-DMAC7.html)
KR (1) KR101554409B1 (cg-RX-API-DMAC7.html)
CN (2) CN104761434A (cg-RX-API-DMAC7.html)
IN (1) IN2014DN00083A (cg-RX-API-DMAC7.html)
MY (1) MY157220A (cg-RX-API-DMAC7.html)
TW (2) TWI527789B (cg-RX-API-DMAC7.html)
WO (1) WO2013008637A1 (cg-RX-API-DMAC7.html)

Families Citing this family (4)

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UA121121C2 (uk) 2014-12-22 2020-04-10 Перфоманс Поліамід Сас Каталізатори окиснення циклоалканів і спосіб одержання спиртів та кетонів
KR101973066B1 (ko) 2017-06-16 2019-04-26 경기대학교 산학협력단 소규모 합성에 적합한 아디프산의 제조 방법
CN108440241B (zh) * 2018-04-10 2021-12-07 中国化学赛鼎宁波工程有限公司 一种高纯度环己醇的提纯系统及方法
WO2024124500A1 (zh) * 2022-12-15 2024-06-20 中国科学院大连化学物理研究所 己二酸的生产方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100562810B1 (ko) * 1999-12-28 2006-03-21 아사히 가세이 가부시키가이샤 시클로헥산올의 제조 방법

Family Cites Families (21)

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Publication number Priority date Publication date Assignee Title
US2719172A (en) 1951-09-03 1955-09-27 Basf Ag Nitric acid oxidation to dicarboxylic acids
US3702886A (en) 1969-10-10 1972-11-14 Mobil Oil Corp Crystalline zeolite zsm-5 and method of preparing the same
DE3165950D1 (de) 1980-05-13 1984-10-18 Ici Plc Zeolite nu-3
EP0054364B1 (en) 1980-12-11 1985-04-24 Imperial Chemical Industries Plc Zeolites
EP0054386B1 (en) 1980-12-17 1985-03-27 Imperial Chemical Industries Plc Zeolites
JPS57200218A (en) 1981-05-20 1982-12-08 Ici Ltd Novel synthetic zeolite substance
JPS58110419A (ja) 1981-12-21 1983-07-01 Teijin Yuka Kk 結晶性アルミノシリケ−トゼオライト及びその製造方法
JPS60104028A (ja) 1983-11-09 1985-06-08 Asahi Chem Ind Co Ltd 環状アルコ−ルの製造法
JPS61257940A (ja) * 1985-05-13 1986-11-15 Asahi Chem Ind Co Ltd ジカルボン酸の製造法
FR2630732B1 (fr) * 1988-05-02 1990-07-20 Rhone Poulenc Chimie Procede de preparation du cyclohexanol
JPH0231056A (ja) 1988-07-18 1990-02-01 Nissan Motor Co Ltd トロイダル式無段変速機の動力分配構造
JP2844098B2 (ja) 1989-12-20 1999-01-06 旭化成工業株式会社 Ｚｓｍ―５微粒子体の製造法
JPH0763902B2 (ja) 1990-06-04 1995-07-12 積水化学工業株式会社 密封リング装着装置
EP0614866B1 (en) 1991-10-07 1997-01-02 Asahi Kasei Kogyo Kabushiki Kaisha Method for hydrating a cycloolefin
CN1052468C (zh) * 1992-12-25 2000-05-17 旭化成工业株式会社 环烯烃水合法
JP3032931B2 (ja) * 1993-12-08 2000-04-17 旭化成工業株式会社 シクロヘキサノールの製造方法
KR100231761B1 (ko) * 1997-12-08 1999-11-15 전원중 고순도 카프로락탐의 제조방법
JP4076269B2 (ja) * 1998-04-17 2008-04-16 旭化成ケミカルズ株式会社 環状アルコールの製造方法
TWI238157B (en) 2001-01-25 2005-08-21 Asahi Kasei Corp Process for producing alkanedicarboxylic acid
CN101796001B (zh) 2007-09-05 2013-11-13 旭化成化学株式会社 环己烯的分离和制造方法
FR2946646B1 (fr) 2009-06-16 2012-09-21 Rhodia Operations Procede de production de cristaux d'acide adipique

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100562810B1 (ko) * 1999-12-28 2006-03-21 아사히 가세이 가부시키가이샤 시클로헥산올의 제조 방법

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Publication number Publication date
TWI492922B (zh) 2015-07-21
TW201307264A (zh) 2013-02-16
EP2733136A1 (en) 2014-05-21
EP2733136B1 (en) 2016-05-04
JP5462981B2 (ja) 2014-04-02
US20140256981A1 (en) 2014-09-11
CN104761434A (zh) 2015-07-08
TWI527789B (zh) 2016-04-01
KR20140004794A (ko) 2014-01-13
US9771313B2 (en) 2017-09-26
WO2013008637A1 (ja) 2013-01-17
JPWO2013008637A1 (ja) 2015-02-23
CN103649029A (zh) 2014-03-19
TW201524945A (zh) 2015-07-01
MY157220A (en) 2016-05-13
IN2014DN00083A (cg-RX-API-DMAC7.html) 2015-05-15
EP2733136A4 (en) 2014-11-26
CN103649029B (zh) 2015-10-14

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