KR101501798B1 - Ｔｓ-1 제올라이트의 제조 공정 - Google Patents

Ｔｓ-1 제올라이트의 제조 공정 Download PDF

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KR101501798B1
KR101501798B1 KR1020107014696A KR20107014696A KR101501798B1 KR 101501798 B1 KR101501798 B1 KR 101501798B1 KR 1020107014696 A KR1020107014696 A KR 1020107014696A KR 20107014696 A KR20107014696 A KR 20107014696A KR 101501798 B1 KR101501798 B1 KR 101501798B1
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zeolite
silica
range
hours
sio
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KR20100103545A (ko
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안젤라 카라티
도나텔라 베르티
로베르토 밀리니
프랑코 리베티
마리아 안젤라 만테가차
지안니 지로티
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베르살리스 에스.피.에이.
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B01J35/45—Nanoparticles
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/005—Silicates, i.e. so-called metallosilicalites or metallozeosilites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/08—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the aluminium atoms being wholly replaced
    • C01B39/085—Group IVB- metallosilicates
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pretreatment Of Seeds And Plants (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
KR1020107014696A 2007-12-14 2008-12-03 Ｔｓ-1 제올라이트의 제조 공정 Active KR101501798B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IT002342A ITMI20072342A1 (it) 2007-12-14 2007-12-14 Processo per preparare zeoliti ts-1
ITMI2007A002342 2007-12-14
PCT/EP2008/010290 WO2009077086A1 (en) 2007-12-14 2008-12-03 Process for the preparation of ts-1 zeolites

Publications (2)

Publication Number Publication Date
KR20100103545A KR20100103545A (ko) 2010-09-27
KR101501798B1 true KR101501798B1 (ko) 2015-03-11

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ID=40315583

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KR1020107014696A Active KR101501798B1 (ko) 2007-12-14 2008-12-03 Ｔｓ-1 제올라이트의 제조 공정

Country Status (19)

Country Link
US (1) US9358531B2 (cg-RX-API-DMAC7.html)
EP (1) EP2222601B1 (cg-RX-API-DMAC7.html)
JP (1) JP5619617B2 (cg-RX-API-DMAC7.html)
KR (1) KR101501798B1 (cg-RX-API-DMAC7.html)
CN (1) CN101918315B (cg-RX-API-DMAC7.html)
BR (1) BRPI0820994B1 (cg-RX-API-DMAC7.html)
CA (1) CA2708787C (cg-RX-API-DMAC7.html)
DK (1) DK2222601T3 (cg-RX-API-DMAC7.html)
EA (1) EA022667B1 (cg-RX-API-DMAC7.html)
EG (1) EG25949A (cg-RX-API-DMAC7.html)
ES (1) ES2443030T3 (cg-RX-API-DMAC7.html)
IL (1) IL206285A (cg-RX-API-DMAC7.html)
IT (1) ITMI20072342A1 (cg-RX-API-DMAC7.html)
MX (1) MX2010006545A (cg-RX-API-DMAC7.html)
MY (1) MY155562A (cg-RX-API-DMAC7.html)
TN (1) TN2010000271A1 (cg-RX-API-DMAC7.html)
TW (1) TWI432379B (cg-RX-API-DMAC7.html)
UA (1) UA103757C2 (cg-RX-API-DMAC7.html)
WO (1) WO2009077086A1 (cg-RX-API-DMAC7.html)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TWI399242B (zh) * 2009-12-11 2013-06-21 China Petrochemical Dev Corp Taipei Taiwan Method for preparing large-diameter titanium-silicon molecular sieve and method for producing cyclohexanone oxime using the molecular sieve
TWI426050B (zh) * 2011-04-19 2014-02-11 China Petrochemical Dev Corp Taipei Taiwan A method for preparing titanium-silicon molecular sieve and method for producing cyclohexanone oxime using the molecular sieve
TWI480100B (zh) * 2011-04-27 2015-04-11 China Petrochemical Dev Corp Taipei Taiwan Titanium-silicon molecular sieve and its preparation method and method for producing cyclohexanone oxime using the molecular sieve
TWI508935B (zh) * 2011-08-11 2015-11-21 China Petrochemical Dev Corp Taipei Taiwan Titanium-silicon molecular sieve and its preparation method and method for producing cyclohexanone oxime using the molecular sieve
CN102502690A (zh) 2011-10-31 2012-06-20 大连理工大学 一种基于季铵盐和无机碱混合液的ts-1改性方法
CN103360344B (zh) * 2012-04-01 2016-01-20 中国石油化工股份有限公司 一种催化丙烯环氧化的方法
CN104174341B (zh) * 2013-05-27 2017-09-26 乌鲁木齐益好天成新型节能材料有限公司 一种固相硅凝胶的制备方法
CN104944441B (zh) * 2014-03-31 2017-05-24 中国石油化工股份有限公司 一种合成钛硅分子筛的方法
CN104528760B (zh) * 2014-12-25 2016-12-07 中国天辰工程有限公司 一种纳米级钛硅分子筛的制备方法
CN107986293B (zh) * 2016-10-27 2020-03-24 中国石油化工股份有限公司 一种钛硅分子筛及其合成方法和应用
CN109721070B (zh) * 2017-10-31 2020-12-04 中国石油化工股份有限公司 钛硅分子筛的生产方法以及由该方法生产的钛硅分子筛和氨肟化反应方法
JP7393424B2 (ja) 2018-11-15 2023-12-06 中国科学院大▲連▼化学物理研究所 階層的細孔を有するｔｓ－１分子篩の製造方法
US12384686B2 (en) 2018-11-15 2025-08-12 Dalian Institute Of Chemical Physics, Chinese Academy Of Sciences Method for preparing TS-1 molecular sieve with hierarchical pores
US11655158B2 (en) 2019-10-14 2023-05-23 Totalenergies Onetech Isomorphous substitution of metals during the synthesis of a zeolite framework
JP7739292B2 (ja) * 2019-12-19 2025-09-16 ビーエーエスエフ ソシエタス・ヨーロピア チタノシリケートゼオライト材料の連続合成
CN112624143B (zh) * 2020-12-11 2022-05-03 北京科技大学 一种以MOFs为钛源制备TS-1分子筛催化剂的方法
CN114669287B (zh) * 2022-04-26 2024-09-24 西安科技大学 一种有序介孔钛铝复合氧化物包覆ts-1分子筛材料及其制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070059237A1 (en) * 2005-09-13 2007-03-15 Chevron U.S.A. Inc. Preparation of titanosilicate zeolite TS-1
JP2007145687A (ja) * 2005-10-26 2007-06-14 Tohoku Univ チタノシリケートの製造方法及びチタノシリケート

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IT1127311B (it) 1979-12-21 1986-05-21 Anic Spa Materiale sintetico,cristallino,poroso costituito da ossidi di silicio e titanio,metodo per la sua preparazione e suoi usi
JP3598567B2 (ja) * 1995-01-19 2004-12-08 東ソー株式会社 高結晶性チタノシリケートの製造方法
CN1050584C (zh) * 1996-06-05 2000-03-22 中国石油化工总公司 一种钛硅分子筛(ts-1)的制备方法
JP3174829B2 (ja) * 1997-05-30 2001-06-11 経済産業省産業技術総合研究所長 多孔性チタノシリケート及びその製造方法
IT1295267B1 (it) * 1997-10-03 1999-05-04 Enichem Spa Processo per preparare zeoliti legate
JP2000185912A (ja) * 1998-12-22 2000-07-04 Tosoh Corp 結晶性チタノシリケートゼオライトおよびその製造方法
IT1314001B1 (it) * 1999-11-19 2002-12-03 Enichem Spa Metodo per la rimozione del templante da zeoliti sintetiche
IT1314263B1 (it) * 1999-12-03 2002-12-06 Enichem Spa Processo per la preparazione di catalizzatori zeolitici.
EP1129991A1 (de) * 2000-03-02 2001-09-05 Degussa AG Verfahren zur Herstellung eines titanhaltigen Zeolithen
AU2002356941A1 (en) * 2001-11-15 2003-06-10 Pq Holding, Inc. Method for controlling synthesis conditions during molecular sieve synthesis using combinations of quaternary ammonium hydroxides and halides

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070059237A1 (en) * 2005-09-13 2007-03-15 Chevron U.S.A. Inc. Preparation of titanosilicate zeolite TS-1
JP2007145687A (ja) * 2005-10-26 2007-06-14 Tohoku Univ チタノシリケートの製造方法及びチタノシリケート

Also Published As

Publication number Publication date
UA103757C2 (ru) 2013-11-25
CN101918315B (zh) 2013-04-24
JP2011506241A (ja) 2011-03-03
IL206285A (en) 2014-01-30
CN101918315A (zh) 2010-12-15
DK2222601T3 (da) 2013-12-09
EA022667B1 (ru) 2016-02-29
WO2009077086A8 (en) 2009-10-15
KR20100103545A (ko) 2010-09-27
WO2009077086A1 (en) 2009-06-25
BRPI0820994B1 (pt) 2019-11-05
US9358531B2 (en) 2016-06-07
EP2222601A1 (en) 2010-09-01
MX2010006545A (es) 2010-08-31
EA201000989A1 (ru) 2011-02-28
ES2443030T3 (es) 2014-02-17
ITMI20072342A1 (it) 2009-06-15
HK1142872A1 (en) 2010-12-17
BRPI0820994A2 (pt) 2015-06-16
CA2708787C (en) 2013-07-16
JP5619617B2 (ja) 2014-11-05
MY155562A (en) 2015-10-30
TWI432379B (zh) 2014-04-01
EP2222601B1 (en) 2013-09-25
IL206285A0 (en) 2010-12-30
TW200934728A (en) 2009-08-16
CA2708787A1 (en) 2009-06-25
US20100331576A1 (en) 2010-12-30
EG25949A (en) 2012-11-12
TN2010000271A1 (en) 2011-11-11

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