KR100611549B1 - 카르보닐화 방법 - Google Patents

카르보닐화 방법 Download PDF

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Publication number
KR100611549B1
KR100611549B1 KR1019990037682A KR19990037682A KR100611549B1 KR 100611549 B1 KR100611549 B1 KR 100611549B1 KR 1019990037682 A KR1019990037682 A KR 1019990037682A KR 19990037682 A KR19990037682 A KR 19990037682A KR 100611549 B1 KR100611549 B1 KR 100611549B1
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KR
South Korea
Prior art keywords
water
acetic acid
iodide
column
propionic acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
KR1019990037682A
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English (en)
Korean (ko)
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KR20000022935A (ko
Inventor
클로드커스텐에버랠드
와트슨데릭존
Original Assignee
비피 케미칼즈 리미티드
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Application filed by 비피 케미칼즈 리미티드 filed Critical 비피 케미칼즈 리미티드
Publication of KR20000022935A publication Critical patent/KR20000022935A/ko
Application granted granted Critical
Publication of KR100611549B1 publication Critical patent/KR100611549B1/ko
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C07C51/46—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation by azeotropic distillation

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
KR1019990037682A 1998-09-08 1999-09-06 카르보닐화 방법 Expired - Fee Related KR100611549B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GBGB9819606.6A GB9819606D0 (en) 1998-09-08 1998-09-08 Carbonylation process
GB9819606.6 1998-09-08

Publications (2)

Publication Number Publication Date
KR20000022935A KR20000022935A (ko) 2000-04-25
KR100611549B1 true KR100611549B1 (ko) 2006-08-10

Family

ID=10838548

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019990037682A Expired - Fee Related KR100611549B1 (ko) 1998-09-08 1999-09-06 카르보닐화 방법

Country Status (16)

Country Link
US (1) US6326515B1 (enExample)
EP (1) EP0985653B1 (enExample)
JP (2) JP5009454B2 (enExample)
KR (1) KR100611549B1 (enExample)
CN (1) CN1138747C (enExample)
CA (1) CA2281379C (enExample)
DE (1) DE69906203T2 (enExample)
GB (1) GB9819606D0 (enExample)
ID (1) ID26007A (enExample)
MY (1) MY117513A (enExample)
RS (1) RS49603B (enExample)
RU (1) RU2213726C2 (enExample)
SA (1) SA99200739B1 (enExample)
SG (1) SG87823A1 (enExample)
TW (1) TWI244478B (enExample)
UA (1) UA65560C2 (enExample)

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GB9819606D0 (en) * 1998-09-08 1998-11-04 Bp Chem Int Ltd Carbonylation process
US6552221B1 (en) 1998-12-18 2003-04-22 Millenium Petrochemicals, Inc. Process control for acetic acid manufacture
GB0213485D0 (en) 2002-06-12 2002-07-24 Bp Chem Int Ltd Process
CN100443173C (zh) * 2004-11-22 2008-12-17 中国科学院化学研究所 甲醇合成乙酸或乙酸甲酯合成乙酐的催化剂体系及应用
GB0601865D0 (en) * 2006-01-30 2006-03-08 Bp Chem Int Ltd Process
US7619113B2 (en) * 2007-09-27 2009-11-17 Celanese International Corporation Method and apparatus for making acetic acid with improved purification
US7902397B2 (en) * 2007-10-11 2011-03-08 Celanese International Corporation Method and apparatus for making acetic acid with improved productivity
US8932372B2 (en) 2010-02-02 2015-01-13 Celanese International Corporation Integrated process for producing alcohols from a mixed acid feed
US8222466B2 (en) 2010-02-02 2012-07-17 Celanese International Corporation Process for producing a water stream from ethanol production
US8575403B2 (en) 2010-05-07 2013-11-05 Celanese International Corporation Hydrolysis of ethyl acetate in ethanol separation process
US8704010B2 (en) 2010-05-07 2014-04-22 Celanese International Corporation Alcohol production process with impurity removal
US8569551B2 (en) 2010-05-07 2013-10-29 Celanese International Corporation Alcohol production process integrating acetic acid feed stream comprising water from carbonylation process
US8664454B2 (en) 2010-07-09 2014-03-04 Celanese International Corporation Process for production of ethanol using a mixed feed using copper containing catalyst
US9272970B2 (en) 2010-07-09 2016-03-01 Celanese International Corporation Hydrogenolysis of ethyl acetate in alcohol separation processes
US8710279B2 (en) 2010-07-09 2014-04-29 Celanese International Corporation Hydrogenolysis of ethyl acetate in alcohol separation processes
WO2012148509A1 (en) 2011-04-26 2012-11-01 Celanese International Corporation Process for producing ethanol using a stacked bed reactor
US8846988B2 (en) 2010-07-09 2014-09-30 Celanese International Corporation Liquid esterification for the production of alcohols
US8927788B2 (en) 2011-04-26 2015-01-06 Celanese International Corporation Process to recover alcohol with reduced water from overhead of acid column
US8686200B2 (en) 2011-04-26 2014-04-01 Celanese International Corporation Process to recover alcohol from an acidic residue stream
US9073816B2 (en) 2011-04-26 2015-07-07 Celanese International Corporation Reducing ethyl acetate concentration in recycle streams for ethanol production processes
US9000233B2 (en) 2011-04-26 2015-04-07 Celanese International Corporation Process to recover alcohol with secondary reactors for hydrolysis of acetal
US9024085B2 (en) 2011-04-26 2015-05-05 Celanese International Corporation Process to reduce ethanol recycled to hydrogenation reactor
US8592635B2 (en) 2011-04-26 2013-11-26 Celanese International Corporation Integrated ethanol production by extracting halides from acetic acid
US8927784B2 (en) 2011-04-26 2015-01-06 Celanese International Corporation Process to recover alcohol from an ethyl acetate residue stream
US8927787B2 (en) 2011-04-26 2015-01-06 Celanese International Corporation Process for controlling a reboiler during alcohol recovery and reduced ester formation
US8933278B2 (en) 2011-04-26 2015-01-13 Celanese International Corporation Process for producing ethanol and reducing acetic acid concentration
US9000232B2 (en) 2011-04-26 2015-04-07 Celanese International Corporation Extractive distillation of crude alcohol product
US8686199B2 (en) 2011-04-26 2014-04-01 Celanese International Corporation Process for reducing the concentration of acetic acid in a crude alcohol product
US9024084B2 (en) 2011-04-26 2015-05-05 Celanese International Corporation Reduced energy alcohol separation process having controlled pressure
US8907141B2 (en) 2011-04-26 2014-12-09 Celanese International Corporation Process to recover alcohol with secondary reactors for esterification of acid
US9024082B2 (en) 2011-04-26 2015-05-05 Celanese International Corporation Using a dilute acid stream as an extractive agent
TW201302684A (zh) 2011-04-26 2013-01-16 Celanese Int Corp 由醋酸進料及再循環醋酸乙酯進料生產乙醇之製程
US8884081B2 (en) 2011-04-26 2014-11-11 Celanese International Corporation Integrated process for producing acetic acid and alcohol
US8754268B2 (en) 2011-04-26 2014-06-17 Celanese International Corporation Process for removing water from alcohol mixtures
US8895786B2 (en) 2011-08-03 2014-11-25 Celanese International Corporation Processes for increasing alcohol production
US8853467B2 (en) 2011-08-19 2014-10-07 Celanese International Corporation Integrated process for producing ethanol
US8829253B2 (en) 2011-08-19 2014-09-09 Celanese International Corporation Integrated process for producing ethanol from methanol
US8853466B2 (en) 2011-08-19 2014-10-07 Celanese International Corporation Integrated process for producing ethanol from methanol
US8704013B2 (en) 2011-11-09 2014-04-22 Celanese International Corporation Integrated process for producing ethanol
US8614359B2 (en) 2011-11-09 2013-12-24 Celanese International Corporation Integrated acid and alcohol production process
US8809599B2 (en) 2011-11-09 2014-08-19 Celanese International Corporation Integrated process for producing ethanol and water balance control
US8686201B2 (en) 2011-11-09 2014-04-01 Celanese International Corporation Integrated acid and alcohol production process having flashing to recover acid production catalyst
US8809598B2 (en) 2011-11-09 2014-08-19 Celanese International Corporation Producing ethanol using two different streams from acetic acid carbonylation process
US8802902B2 (en) 2011-12-30 2014-08-12 Celanese International Corporation Pressure driven distillation for ethanol production and recovery from hydrogenation process
US9353034B2 (en) 2012-02-07 2016-05-31 Celanese International Corporation Hydrogenation process with reduced residence time for vapor phase reactants
KR200483189Y1 (ko) 2015-11-05 2017-04-14 주식회사 엔젤악기 소금용 마우스피스 캡 및 그를 구비하는 소금
BR112018074026A2 (pt) * 2016-07-07 2019-02-26 Daicel Corporation processos para separação ou remoção de compostos redutores de permanganato (prc?s) de uma primeira mistura e para produção de ácido acético
CN111847716B (zh) * 2020-07-21 2023-08-18 河南城建学院 一种醋酸废液的净化装置
CN111762920B (zh) * 2020-07-21 2023-04-18 河南城建学院 一种降低醋酸废液中钾离子浓度的方法
CN114133324B (zh) * 2021-12-06 2023-10-03 上海簇睿低碳能源技术有限公司 一种甲醇羰基化连续制备乙酸的方法和系统

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SE364255B (enExample) 1967-04-05 1974-02-18 Monsanto Co
SE364254B (enExample) 1967-04-05 1974-02-18 Monsanto Co
US3772380A (en) 1970-03-12 1973-11-13 Monsanto Co Production of carboxylic acids and esters
US3791935A (en) * 1971-11-10 1974-02-12 Monsanto Co Purification of carboxylic acids
US3769177A (en) * 1971-11-10 1973-10-30 Monsanto Co Purification of carboxylic acids by plural stage distillation with side stream draw-offs
US4008131A (en) 1975-12-11 1977-02-15 Monsanto Company Purification of acetic acid
GB8904125D0 (en) 1989-02-23 1989-04-05 British Petroleum Co Plc Process for preparing carboxylic acids
JP2839367B2 (ja) 1989-04-06 1998-12-16 ビーピー ケミカルズ リミテッド カルボン酸類の製造方法
AU639630B2 (en) * 1991-01-28 1993-07-29 Celanese International Corporation Removal of carbonyl impurities from carbonylation process stream
GB9120902D0 (en) * 1991-10-02 1991-11-13 Bp Chem Int Ltd Purification process
GB9211671D0 (en) 1992-06-02 1992-07-15 Bp Chem Int Ltd Process
GB9306409D0 (en) 1993-03-26 1993-05-19 Bp Chem Int Ltd Process
DE69407846T2 (de) 1993-03-31 1998-08-20 Acetex Chimie Verfahren zur Herstellung von Carbonsäuren oder ihrer Ester in gegenwart des auf Iridium basierten Katalysators
FR2703351A1 (fr) 1993-03-31 1994-10-07 Rhone Poulenc Chimie Procédé de préparation d'acides carboxyliques ou des esters correspondants en présence d'un catalyseur à base de rhodium et d'iridium.
FR2713620B1 (fr) 1993-12-10 1996-03-01 Rhone Poulenc Chimie Procédé de préparation d'une solution à base d'iridium, solution obtenue et utilisation de celle-ci en tant que catalyseur.
WO1995031426A1 (fr) 1994-05-13 1995-11-23 Pardies Acetiques Procede de preparation d'acides carboxyliques ou des esters correspondants en presence d'un catalyseur a base d'iridium et d'iodures sous forme soluble
DE69609796T2 (de) * 1995-04-27 2000-12-28 Daicel Chem Verfahren zur herstellung von essigsäure
IN192600B (enExample) * 1996-10-18 2004-05-08 Hoechst Celanese Corp
GB9626324D0 (en) * 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
GB9819606D0 (en) * 1998-09-08 1998-11-04 Bp Chem Int Ltd Carbonylation process

Also Published As

Publication number Publication date
CN1247183A (zh) 2000-03-15
CA2281379C (en) 2008-04-08
US6326515B1 (en) 2001-12-04
JP2000086573A (ja) 2000-03-28
DE69906203D1 (de) 2003-04-30
RU2213726C2 (ru) 2003-10-10
EP0985653B1 (en) 2003-03-26
GB9819606D0 (en) 1998-11-04
CN1138747C (zh) 2004-02-18
DE69906203T2 (de) 2004-01-08
KR20000022935A (ko) 2000-04-25
UA65560C2 (uk) 2004-04-15
SA99200739B1 (ar) 2006-10-08
CA2281379A1 (en) 2000-03-08
TWI244478B (en) 2005-12-01
YU43899A (sh) 2002-06-19
EP0985653A1 (en) 2000-03-15
ID26007A (id) 2000-11-16
RS49603B (sr) 2007-06-04
JP5009454B2 (ja) 2012-08-22
JP2010248274A (ja) 2010-11-04
SG87823A1 (en) 2002-04-16
MY117513A (en) 2004-07-31

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