JPWO2018199314A1 - 油性化粧料 - Google Patents
油性化粧料 Download PDFInfo
- Publication number
- JPWO2018199314A1 JPWO2018199314A1 JP2019514672A JP2019514672A JPWO2018199314A1 JP WO2018199314 A1 JPWO2018199314 A1 JP WO2018199314A1 JP 2019514672 A JP2019514672 A JP 2019514672A JP 2019514672 A JP2019514672 A JP 2019514672A JP WO2018199314 A1 JPWO2018199314 A1 JP WO2018199314A1
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- JP
- Japan
- Prior art keywords
- oil
- cosmetic
- component
- red
- color
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 229920001577 copolymer Polymers 0.000 claims abstract description 32
- 239000004711 α-olefin Substances 0.000 claims abstract description 22
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- DBZJJPROPLPMSN-UHFFFAOYSA-N bromoeosin Chemical compound O1C(=O)C2=CC=CC=C2C21C1=CC(Br)=C(O)C(Br)=C1OC1=C(Br)C(O)=C(Br)C=C21 DBZJJPROPLPMSN-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000011161 development Methods 0.000 claims description 24
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
- A61K8/8182—Copolymers of vinyl-pyrrolidones. Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/08—Preparations containing skin colorants, e.g. pigments for cheeks, e.g. rouge
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q3/00—Manicure or pedicure preparations
- A61Q3/02—Nail coatings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
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Abstract
Description
(1)次の成分(A)及び(B);
(A)赤色218号、及び赤色223号から選ばれる1種又は2種
(B)α−オレフィン・ビニルピロリドン共重合体
を含有し、成分(B)に対する成分(A)の含有質量割合(A)/(B)が2以下である油性化粧料に関するものである。
(A)赤色218号、赤色223号から選ばれる1種又は2種
(B)α−オレフィン・ビニルピロリドン共重合体
を含有し、成分(B)に対する成分(A)の含有質量割合(含有質量比)(A)/(B)が2以下である油性化粧料である。本発明の油性化粧料は、鮮やかな外観色を有しながらも、高温安定性及びツヤに優れたものである。
実施例1〜5、比較例1、2
表1に示す組成の混合物に関して、発色の程度を下記評価基準により評価した。その結果を表1に示す。なお、成分(1)〜(4)を3本ローラーで均一混合し、油性化粧料を得た。
実施例1〜5、比較例1、2で得られたものを、透明セルを用い、25℃環境下において、色差計Sectro Color Meter SE7700(島津製作所)にて測定し、得られたa値およびb値より、下記評価基準にて評価を行った。結果を表1に示す。
(評価基準) :(判定)
30≦(a2+b2)(1/2) :◎
10<(a2+b2)(1/2)<30 :○
(a2+b2)(1/2)≦10 :×
また、「高温安定性」および「ツヤ」について、下記評価方法により行った。その結果も併せて表1に示す。
実施例6〜11、比較例3〜8
表2に示す組成の油性口唇用化粧料(半固形状グロス)を下記製造方法に従って調製した。得られた油性口唇用化粧料について、「発色」の程度、加熱した際の色の「高温安定性」、肌や皮膚に塗布した化粧料を除去した際の「染着しにくさ」、化粧料の外観の「透明度」及び塗布後の化粧膜の「ツヤ」の評価を下記評価方法により行った。その結果も併せて表2に示す。なお、「発色」に関しては、表1で用いた方法を用いた。
A.成分(1)〜(8)を均一混合する。
B.Aと成分(9)〜(15)を三本ローラーにて均一混合する。
C.Bを90℃まで加熱し、容器に充填し、油性口唇用化粧料を得た。
(高温安定性)
実施例6〜11、比較例3〜8で得られた油性口唇用化粧料を、110℃に加熱した後、透明セルを用い、25℃環境下において、Sectro Color Meter SE7700(島津製作所)にて測定し、得られたa値およびb値より、下記評価基準にて評価を行った。
(評価基準) :(判定)
30≦(a2+b2)(1/2) :◎
10<(a2+b2)(1/2)<30 :○
(a2+b2)(1/2)≦10 :×
(染着しにくさ)
実施例6〜11、比較例3〜8で得られた油性口唇用化粧料を、肌に塗布し、市販のティッシュペーパーで化粧料を除去した後の染着度合を、下記評価基準にて専門パネルによる評価を行った。
(評価基準) :(判定)
ティッシュペーパーで化粧料を除去した後、染着していない :◎
ティッシュペーパーで化粧料を除去した後、多少染着している :○
ティッシュペーパーで化粧料を除去した後、明らかに染着している:×
(透明度)
実施例6〜11、比較例3〜8で得られた油性口唇用化粧料を、光路長1cmの透明セルを用い、25℃環境下において、650nmの吸光度を島津製作所社製の吸光光度計UV−2500PCにて測定し、650nmの波長領域における吸光度から、下記評価基準にて評価を行った。
(評価基準) :(判定)
95≦(吸光度) :◎
50<(吸光度)<95 :○
(吸光度)≦50 :×
(ツヤ)
実施例6〜11、比較例3〜8で得られた油性口唇用化粧料について、専門パネル20名による使用テストを行い、パネル各人が下記絶対評価にて5段階に評価し、パネル全員の評点合計からその平均値を算出し、下記判定基準により3段階で判定した。具体的には、各試料の塗布直後の化粧膜の状態を観察し、ツヤ高い質感の感じ方について評価した。
<絶対評価基準>
(評点):(評価)
4 :非常に優れていると感じる
3 :優れていると感じる
2 :普通
1 :やや劣っていると感じる
0 :劣っていると感じる
<判定基準>
(評点平均値) :(判定)
3.5点を超える : ◎
2.5点以上3.5未満: ○
2.5点未満 : ×
表2および図1の結果から明らかなように、本発明の実施品である実施例6〜11は、外観が鮮やかに発色し、高温安定性や染着しにくさ、透明度、ツヤに優れた油性化粧料であった。
表3に示す組成の油性口唇用化粧料(固形状)を下記製造方法に従って調製した。得られた油性口唇用化粧料について、表1及び表2で用いた評価方法により、「発色」の程度、加熱した際の色の「高温安定性」、肌や皮膚に塗布した後に化粧料を除去した際の「染着しにくさ」及び塗布後の化粧膜の「ツヤ」の評価を行った。また、下記評価方法により、化粧料の外観の「クリア感」の評価を行った。その結果も併せて表3に示す。
A.成分(1)〜(9)を均一混合する。
B.Aと成分(10)〜(16)を三本ローラーにて均一混合する。
C.Bを110℃まで加熱し、容器に充填し、油性口唇用化粧料を得た。
(クリア感)
実施例12〜17、比較例9〜14で得られた油性口唇用化粧料について、専門パネル20名による使用テストを行い、パネル各人が下記絶対評価にて5段階に評価し、パネル全員の評点合計からその平均値を算出し、下記判定基準により3段階で判定した。具体的には、各試料の外観の状態を観察し、クリアな質感(クリア感)の感じ方について評価した。
<絶対評価基準>
(評点):(評価)
4 :非常にクリア感がある
3 :クリア感がある
2 :普通
1 :ややクリア感が劣っている
0 :クリア感が劣っている(隠ぺい感が強い)と感じる
<判定基準>
(評点平均値) :(判定)
3.5点を超える : ◎
2.5点以上3.5未満: ○
2.5点未満 : ×
表3の結果から明らかなように、本発明の実施品である実施例12〜17は、外観が鮮やかに発色し、高温安定性や染着しにくさ、クリア感、ツヤに優れた油性化粧料であった。
(成分) (%)
1.アボカド油 ※17 50
2.トリエチルヘキサノイン(トリ2−エチルヘキサン酸グリセリル)残量
3.(ビニルピロリドン/ヘキサデセン)コポリマー ※4 15
4.赤色218号 ※2 0.1
5.2,6−ジ−ターシャリ−ブチル−パラ−クレゾール ※18 0.01
6.ジメチルシリル化シリカ ※19 10
7.酸化チタン被覆ガラス末 ※20 0.01
※17:NIKKOL精製アボカド油
※18:2−6−DI−TERT−BUTYL−CRESOL(東京化成品社製)
※19:AEROSIL R976S(日本アエロジル社製、平均粒子径7nm)
※20:マイクログラス メタシャイン 1080RS(日本板硝子社製、平均粒子径85μm)。
A.成分(1)〜(7)を25℃にて均一に溶解する。
B.Aをマニキュア容器に直接流し込み、ネイルオイルを得た。
実施例19:固形状ほほ紅
(成分) (%)
1.マイクロクリスタリンワックス ※21 4
2.キャンデリラロウ ※22 7
3.トリエチルヘキサノイン(トリ2−エチルヘキサン酸グリセリル)残量
4.トリイソステアリン酸ポリグリセリル−2 ※8 15
5.オクチルドデカノール ※23 10
6.(ビニルピロリドン/ヘキサデセン)コポリマー ※4 15
7.赤色218号 ※2 0.1
8.ジメチルシリル化シリカ ※10 5
9.無水ケイ酸 ※24 8
10.酸化チタン被覆合成金雲母 ※25 0.5
11.フェノキシエタノール ※11 0.3
※21:MULTIWAX W445(SONNEBORN社製)
※22:精製キャンデリラワックスSR−3(日本ナチュラルプロダクツ社製)
※23:リソノール20SP(高級アルコール工業社製)
※24:SILICA MICRO BEAD BA−1(日揮触媒化成株式会社製、平均粒子径18μm)
※25:HELIOS R300S(トピー工業社製、平均粒子径210μm)。
A.成分(1)〜(8)を均一に100℃にて溶解する。
B.Aを三本ローラーにて均一混合する。
C.Bに成分(9)〜(10)を加え、均一に混合する。
D.Cを樹脂皿に90℃にて溶解充填して冷却固化し固形状ほほ紅を得た。
(成分) (%)
1.N−ラウロイル−L−グルタミン酸ジブチルアミド※26 5
2.N−エチルヘキサノイル−L−グルタミン酸ジブチルアミド※27 3
3.トリメリト酸トリトリデシル ※9 30
4.(ビニルピロリドン/ヘキサデセン)コポリマー※4 15
5.(ビニルピロリドン/エイコセン)コポリマー※4’ 1
6.赤色218号 ※2 0.1
7.赤色223号 ※3 0.1
8.リンゴ酸ジイソステアリル ※1 残量
9.水添ポリデセン ※28 10
10.ナイロンパウダー ※29 2
11.ポリウレタンパウダー ※30 3
12.ジプロピレングリコール 0.3
13.1,2−ペンタンジオール 0.3
14.2,6−ジ−ターシャリーブチル−パラ−クレゾール 0.01
15.アスタキサンチン 0.0001
16.パルミチン酸アスコルビル 0.0001
17.ニコチン酸アミド 1
※26:アミノ酸系油ゲル化剤GP−1(味の素株式会社製)
※27:アミノ酸系油ゲル化剤EB−21(味の素株式会社製)
※28:ノムコートHP−30(日清オイリオグループ株式会社製)
※29:オルガソール2002D(アトフィナ・ジャパン社製、平均粒径22μm)
※30:平均粒子径7μm。
A.成分(1)〜(11)を均一に150℃にて溶解する。
B.Aを三本ローラーにて均一混合する。
C.Bに成分(12)〜(17)を加え、均一に混合する
D.Cを金型に溶融充填して冷却し固形状口紅を得た。
Claims (6)
- 次の成分(A)及び(B);
(A)赤色218号、及び赤色223号から選ばれる1種又は2種
(B)α−オレフィン・ビニルピロリドン共重合体
を含有し、成分(B)に対する成分(A)の含有質量割合(A)/(B)が2以下である油性化粧料。 - 前記成分(B)におけるα−オレフィンが、炭素数12〜24である、請求項1記載の油性化粧料。
- 前記成分(B)が、ヘキサデセン・ビニルピロリドン共重合体である請求項1または2記載の油性化粧料。
- 前記(A)/(B)が0.0001以上2以下である請求項1〜3のいずれか1項に記載の油性化粧料。
- 前記成分(A)の含有量が化粧料に対して0.1〜1質量%である、請求項1〜4のいずれか1項に記載の油性化粧料。
- α−オレフィン・ビニルピロリドン共重合体を含有する、染料を含む油性材料の発色向上剤であって、前記染料は、赤色218号、及び赤色223号から選ばれる1種又は2種である、発色向上剤。
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WO2018088565A1 (ja) * | 2016-11-14 | 2018-05-17 | 株式会社コーセー | 油性メーキャップ化粧料 |
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TW201842898A (zh) | 2018-12-16 |
JP7288849B2 (ja) | 2023-06-08 |
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