JPWO2018074149A1 - 洗浄剤組成物 - Google Patents
洗浄剤組成物 Download PDFInfo
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- JPWO2018074149A1 JPWO2018074149A1 JP2018546209A JP2018546209A JPWO2018074149A1 JP WO2018074149 A1 JPWO2018074149 A1 JP WO2018074149A1 JP 2018546209 A JP2018546209 A JP 2018546209A JP 2018546209 A JP2018546209 A JP 2018546209A JP WO2018074149 A1 JPWO2018074149 A1 JP WO2018074149A1
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Abstract
Description
成分(A)、成分(B)、成分(C)及び成分(D)の合計質量に対する成分(A)及び成分(B)の合計質量の比が0.35〜0.9である。
アニオン性界面活性剤としては、例えば、脂肪酸セッケン(例えば、ラウリン酸ナトリウム、パルミチン酸ナトリウム等);高級アルキル硫酸エステル塩(例えば、ラウリル硫酸ナトリウム、ラウリル硫酸カリウム等);アルキルエーテル硫酸エステル塩(例えば、POE−ラウリル硫酸トリエタノールアミン、POE−ラウリル硫酸ナトリウム等);N−アシルサルコシン酸(例えば、ラウロイルサルコシンナトリウム等);高級脂肪酸アミドスルホン酸塩(例えば、N‐ステアロイル‐N‐メチルタウリンナトリウム、N−ミリストイル−N−メチルタウリンナトリウム、ヤシ油脂肪酸メチルタウリッドナトリウム、ラウリルメチルタウリッドナトリウム等);リン酸エステル塩(POE−オレイルエーテルリン酸ナトリウム、POE−ステアリルエーテルリン酸等);スルホコハク酸塩(例えば、ジ−2−エチルヘキシルスルホコハク酸ナトリウム、モノラウロイルモノエタノールアミドポリオキシエチレンスルホコハク酸ナトリウム、ラウリルポリプロピレングリコールスルホコハク酸ナトリウム等);アルキルベンゼンスルホン酸塩(例えば、リニアドデシルベンゼンスルホン酸ナトリウム、リニアドデシルベンゼンスルホン酸トリエタノールアミン、リニアドデシルベンゼンスルホン酸等);高級脂肪酸エステル硫酸エステル塩(例えば、硬化ヤシ油脂肪酸グリセリン硫酸ナトリウム等);N−アシルグルタミン酸塩(例えば、N−ラウロイルグルタミン酸モノナトリウム、N−ステアロイルグルタミン酸ジナトリウム、N−ミリストイル−L−グルタミン酸モノナトリウム等);硫酸化油(例えば、ロート油等);POE−アルキルエーテルカルボン酸;POE−アルキルアリルエーテルカルボン酸塩;α-オレフィンスルホン酸塩;高級脂肪酸エステルスルホン酸塩;二級アルコール硫酸エステル塩;高級脂肪酸アルキロールアミド硫酸エステル塩;ラウロイルモノエタノールアミドコハク酸ナトリウム;N−パルミトイルアスパラギン酸ジトリエタノールアミン;カゼインナトリウム等を使用することができる。
両性界面活性剤としては、例えば、イミダゾリン系両性界面活性剤(例えば、2−ウンデシル−N,N,N−(ヒドロキシエチルカルボキシメチル)−2−イミダゾリンナトリウム、2−ココイル−2−イミダゾリニウムヒドロキサイド−1−カルボキシエチロキシ2ナトリウム塩等);ベタイン系界面活性剤(例えば、2−ヘプタデシル−N−カルボキシメチル−N−ヒドロキシエチルイミダゾリニウムベタイン、ラウリルジメチルアミノ酢酸ベタイン、アルキルベタイン、アミドベタイン、スルホベタイン等)等が挙げられる。
非イオン性界面活性剤は、例えば、ポリオキシアルキレン脂肪酸グリセリルを含むことができる。
油性成分としては、例えば、液体油脂、固体油脂、ロウ、炭化水素、高級脂肪酸、高級アルコール、合成エステル油、シリコーン油等を使用することができる。
本開示の洗浄剤組成物は、上述の成分に加えて、さらに起泡剤(増泡剤、コサーファクタント)を含有することができる。起泡剤とは、本開示の洗浄剤組成物の泡立ちを改善するものである。起泡剤としては、例えば、水溶性多価アルコール及び/又はその誘導体を使用することができる。起泡剤の例としては、オクトキシグリセリン、イソオクタン酸グリセリル、ラウリン酸ポリグリセリル−2、モノオクタン酸グリセリル等を挙げることができる。
本開示の洗浄剤組成物は、上述の成分に加えて、さらに水を含有することができる。水としては、化粧料、医薬部外品等に使用される水を使用することができ、例えば、精製水、イオン交換水、水道水等を使用することができる。水相は、目的に応じて、水溶性アルコールをさらに含有することができる。
本開示の洗浄剤組成物は、本開示の効果を阻害しない範囲において、他の成分、例えば、水性溶媒、カチオン界面活性剤、親油性非イオン性界面活性剤、粉体、保湿剤、水溶性高分子、増粘剤、皮膜剤、紫外線吸収剤、金属イオン封鎖剤、アミノ酸、有機アミン、高分子エマルジョン、pH調整剤、皮膚栄養剤、ビタミン、酸化防止剤、酸化防止助剤、香料等を必要に応じて適宜含有することができる。
各組成物について、洗浄性及び泡立ちの良さについて評価した。また、追加的に、各組成物について、外観上の安定性及びポンプフォーマによる泡吐出性についても評価した。各評価項目の評価基準は以下の通りである。試験例1〜32に係る組成物の組成及び評価を表2〜9に示す。
専門パネル7名の顔に、ウォータプルーフタイプの油性ファンデーション及び口紅でもって化粧をした。化粧してから1時間経過後、洗浄剤組成物を2g採り、顔上のファンデーション及び口紅になじませた。そして、水道水を使用して洗浄剤組成物と共にファンデーション及び口紅を洗い流した。このとき、専門パネル7名中、何名が十分にファンデーション及び口紅が落ちたかと感じたかによって洗浄剤組成物の洗浄性を評価した。以下に評価基準を示す。
A:6〜7名が、十分に化粧が落ちたと評価した。
B:4〜5名が、十分に化粧が落ちたと評価した。
C:2〜3名が、十分に化粧が落ちたと評価した。
D:1名以下が、十分に化粧が落ちたと評価した。
専門パネル7名の顔に、ウォータプルーフタイプの油性ファンデーションでもって化粧をした。化粧してから1時間経過後、洗浄剤組成物を2g採り、顔上のファンデーションになじませた。そして、水道水を使用して洗浄剤組成物と共にファンデーションを洗い流す時の泡立ちを評価した。このとき、専門パネル7名中、何名が十分に泡立ったと感じたかによって洗浄剤組成物の起泡性を評価した。以下に評価基準を示す。
A:6〜7名が、十分に泡立っていると評価した。
B:4〜5名が、十分に泡立っていると評価した。
C:2〜3名が、十分に泡立っていると評価した。
D:1名以下が、十分に泡立っていると評価した。
洗浄剤組成物の外観を観察して、以下の評価基準で洗浄剤組成物の外観安定性を評価した。
A:洗浄剤組成物は透明である。
B及びC:評価不使用
D:洗浄剤組成物は半透明であるか、白濁している。
洗浄剤組成物を泡立てた状態で吐出するポンプフォーマを用いてポンプフォーマから洗浄剤組成物を吐出させた。この時、ポンプフォーマから吐出され泡がきめ細かく、かつ体積が十分にあると専門パネル7名のうち何名が評価したかによって洗浄剤組成物の泡吐出性を評価した。使用したポンプフォーマは、市販のハンドソープ等に用いられている、手で可動式ノズルを上から容器に押し込んで泡を吐出させるタイプである。
A:6〜7名が、吐出された泡がきめ細かく、かつ体積が十分にあると評価した。
B:4〜5名が、吐出された泡がきめ細かく、かつ体積が十分にあると評価した。
C:2〜3名が、吐出された泡がきめ細かく、かつ体積が十分にあると評価した。
D:1名以下が、吐出された泡がきめ細かく、かつ体積が十分にあると評価した。
試験例1〜3に係る組成物の組成及び評価を表2に示す。試験例1〜3においては、(A)アニオン性界面活性剤及び(B)両性界面活性剤の含有率を変化させた。ただし、アニオン性比は一定になるようにした。
試験例4〜5に係る組成物の組成及び評価を表3に示す。試験例4においては、試験例1〜3とは異なる(A)アニオン性界面活性剤を使用した。試験例5においては、試験例1〜3とは異なる(B)両性界面活性剤を使用した。
試験例6〜7に係る組成物の組成及び評価を表4に示す。試験例6〜7においては、上記試験例から(C)非イオン性界面活性剤の含有率を変化させた。
試験例8〜15に係る組成物の組成及び評価を表5に示す。試験例8〜15においては、上記試験例から(C)非イオン性界面活性剤の親水性(HLB)が変化するように、非イオン性界面活性剤の種類を変化させた。
試験例16〜19に係る組成物の組成及び評価を表6に示す。試験例16〜19においては、上記試験例から(D)油性成分の含有率を変化させた。
試験例20〜26に係る組成物の組成及び評価を表7に示す。試験例20〜26においては、上記試験例から(D)油性成分の種類を変更した。
試験例27〜29に係る組成物の組成及び評価を表8に示す。試験例27〜29においては、上記試験例から(E)起泡剤の含有率を変化させた。
試験例30〜32に係る組成物の組成及び評価を表9に示す。試験例30〜32においては、上記試験例から(E)起泡剤の種類を変更した。
試験例1〜32と同様の試験を行った。試験方法については、試験例1〜32と同様である。評価方法については、専門パネルを5名とし、以下の評価基準を用いた以外は、試験例1〜32と同様である。
A:4〜5名が、十分に化粧が落ちたと評価した。
B:評価不使用
C:2〜3名が、十分に化粧が落ちたと評価した。
D:1名以下が、十分に化粧が落ちたと評価した。
A:4〜5名が、十分に泡立っていると評価した。
B:評価不使用
C:2〜3名が、十分に泡立っていると評価した。
D:1名以下が、十分に泡立っていると評価した。
洗浄剤組成物の外観を観察して、以下の評価基準で洗浄剤組成物の外観安定性を評価した。
A:洗浄剤組成物は透明である。
B及びC:評価不使用
D:洗浄剤組成物は半透明であるか、白濁している。
A:4〜5名が、吐出された泡がきめ細かく、かつ体積が十分にあると評価した。
B:評価不使用
C:2〜3名が、吐出された泡がきめ細かく、かつ体積が十分にあると評価した。
D:1名以下が、吐出された泡がきめ細かく、かつ体積が十分にあると評価した。
試験例33〜42に係る組成物の組成及び評価を表10及び11に示す。試験例33〜42においてはイオン性比が変動するように成分(A)〜(D)の含有率を変化させた。アニオン性比は一定になるようにした。
試験例43〜52に係る組成物の組成及び評価を表12及び13に示す。試験例43〜52においてはアニオン性比が変動するように(A)アニオン性界面活性剤及び(B)両性界面活性剤の含有率を変化させた。イオン性比はほぼ一定になるようにした。
試験例53〜56に係る組成物の組成及び評価を表14に示す。評価基準は試験例1〜32と同じである。試験例53〜56においては、(E)起泡剤成分におけるアシル基の炭素数を変化させた。
[付記1]
(A)2質量%〜17質量%のアニオン性界面活性剤と、
(B)2質量%〜17質量%の両性界面活性剤と、
(C)4質量%〜17質量%の非イオン性界面活性剤と、
(D)0.2質量%〜5質量%の油性成分と、
を含有し、
上記化4又は化5に示す化合物を実質量含まない、洗浄剤組成物。
[付記2]
(A)2質量%〜17.5質量%のアニオン性界面活性剤と、
(B)1質量%〜17.5質量%の両性界面活性剤と、
(C)4質量%〜17質量%の非イオン性界面活性剤と、
(D)0.2質量%〜5質量%の油性成分と、
を含有し、
上記化4又は化5に示す化合物を実質量含まない、洗浄剤組成物。
[付記3]
(A)2質量%〜17.5質量%のアニオン性界面活性剤と、
(B)1質量%〜17.5質量%の両性界面活性剤と、
(C)2.5質量%〜17質量%の非イオン性界面活性剤と、
(D)0.2質量%〜5質量%の油性成分と、
を含有し、
前記成分(A)、前記成分(B)、前記成分(C)及び前記成分(D)の合計質量に対する前記成分(A)及び前記成分(B)の合計質量の比が0.8〜0.9であり、
上記化4又は化5に示す化合物を実質量含まない、洗浄剤組成物。
[付記4]
前記成分(A)、前記成分(B)、前記成分(C)及び前記成分(D)の合計質量に対する前記成分(A)及び前記成分(B)の合計質量の比が0.4〜0.9である、付記に記載の洗浄剤組成物。
Claims (13)
- (A)2質量%〜17.5質量%のアニオン性界面活性剤と、
(B)1質量%〜17.5質量%の両性界面活性剤と、
(C)2.5質量%〜17質量%の非イオン性界面活性剤と、
(D)0.2質量%〜5質量%の油性成分と、
を含有し、
下記化1又は化2に示す化合物を実質量含まない、洗浄剤組成物。
- 前記成分(A)及び前記成分(B)の合計質量に対する前記成分(A)の質量の比が0.1〜0.9である、請求項1に記載の洗浄剤組成物。
- 前記成分(A)、前記成分(B)、前記成分(C)及び前記成分(D)の合計質量に対する前記成分(A)及び前記成分(B)の合計質量の比が0.35〜0.9である、請求項1又は2に記載の洗浄剤組成物。
- (E)0.4質量%〜5質量%の起泡剤をさらに含有する、請求項1〜3のいずれか一項に記載の洗浄剤組成物。
- 前記成分(E)が、下記化3に示す化合物のうちの少なくとも1つを含む、請求項4に記載の組成物。
- (F)60質量%〜85質量%の水をさらに含有する、請求項1〜5のいずれか一項に記載の洗浄剤組成物。
- 前記成分(A)がポリオキシエチレンアルキルエーテル硫酸塩及び/又はアシルメチルタウリン塩を含む、請求項1〜6のいずれか一項に記載の洗浄剤組成物。
- 前記成分(B)がベタイン型である、請求項1〜7のいずれか一項に記載の洗浄剤組成物。
- 前記成分(C)のHLBが9〜14である、請求項1〜8のいずれか一項に記載の組成物。
- 前記成分(C)がポリオキシエチレン脂肪酸グリセリルである、請求項1〜9のいずれか一項に記載の洗浄剤組成物。
- バイコンティニュアス相を有しない、請求項1〜10のいずれか一項に記載の洗浄剤組成物。
- 高圧ガスを使用しない泡立てポンプに適用される、請求項1〜11のいずれか一項に記載の洗浄剤組成物。
- 化粧料用洗浄剤として使用される、請求項1〜12のいずれか一項に記載の洗浄剤組成物。
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