JPWO2010090192A1 - 一酸化炭素を処理するための方法 - Google Patents
一酸化炭素を処理するための方法 Download PDFInfo
- Publication number
- JPWO2010090192A1 JPWO2010090192A1 JP2010549478A JP2010549478A JPWO2010090192A1 JP WO2010090192 A1 JPWO2010090192 A1 JP WO2010090192A1 JP 2010549478 A JP2010549478 A JP 2010549478A JP 2010549478 A JP2010549478 A JP 2010549478A JP WO2010090192 A1 JPWO2010090192 A1 JP WO2010090192A1
- Authority
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- Japan
- Prior art keywords
- component
- carbon monoxide
- carbon dioxide
- mass
- container
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 title claims abstract description 61
- 229910002091 carbon monoxide Inorganic materials 0.000 title claims abstract description 61
- 238000000034 method Methods 0.000 title claims abstract description 31
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 108
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 54
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 54
- 239000000126 substance Substances 0.000 claims abstract description 21
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 16
- 239000001301 oxygen Substances 0.000 claims abstract description 16
- 230000001590 oxidative effect Effects 0.000 claims abstract description 5
- 239000011342 resin composition Substances 0.000 claims description 30
- 239000003054 catalyst Substances 0.000 claims description 28
- 229920005989 resin Polymers 0.000 claims description 25
- 239000011347 resin Substances 0.000 claims description 25
- 230000003647 oxidation Effects 0.000 claims description 21
- 238000007254 oxidation reaction Methods 0.000 claims description 21
- 238000003860 storage Methods 0.000 claims description 20
- 229920000573 polyethylene Polymers 0.000 claims description 17
- 238000001179 sorption measurement Methods 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 13
- 239000000395 magnesium oxide Substances 0.000 claims description 12
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 12
- 125000000816 ethylene group Chemical group [H]C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 10
- 239000003990 capacitor Substances 0.000 claims description 9
- 239000011255 nonaqueous electrolyte Substances 0.000 claims description 9
- IATRAKWUXMZMIY-UHFFFAOYSA-N strontium oxide Chemical compound [O-2].[Sr+2] IATRAKWUXMZMIY-UHFFFAOYSA-N 0.000 claims description 9
- 239000005977 Ethylene Substances 0.000 claims description 8
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 8
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 7
- 229910000510 noble metal Inorganic materials 0.000 claims description 7
- 239000010457 zeolite Substances 0.000 claims description 7
- 229910021536 Zeolite Inorganic materials 0.000 claims description 6
- 239000011148 porous material Substances 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 3
- 239000007789 gas Substances 0.000 description 24
- 239000002245 particle Substances 0.000 description 14
- -1 Polyethylene Polymers 0.000 description 12
- 238000004898 kneading Methods 0.000 description 12
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 8
- 239000010410 layer Substances 0.000 description 8
- 238000002844 melting Methods 0.000 description 8
- 230000008018 melting Effects 0.000 description 8
- 239000000203 mixture Substances 0.000 description 8
- 239000002808 molecular sieve Substances 0.000 description 8
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 8
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 7
- 238000009826 distribution Methods 0.000 description 7
- 239000000945 filler Substances 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 7
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- 150000001875 compounds Chemical class 0.000 description 6
- 230000005611 electricity Effects 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 238000000465 moulding Methods 0.000 description 6
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 6
- VZCYOOQTPOCHFL-OWOJBTEDSA-N Fumaric acid Chemical compound OC(=O)\C=C\C(O)=O VZCYOOQTPOCHFL-OWOJBTEDSA-N 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 5
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- 150000004706 metal oxides Chemical class 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 5
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 5
- 229920001862 ultra low molecular weight polyethylene Polymers 0.000 description 5
- VXNZUUAINFGPBY-UHFFFAOYSA-N 1-Butene Chemical compound CCC=C VXNZUUAINFGPBY-UHFFFAOYSA-N 0.000 description 4
- LIKMAJRDDDTEIG-UHFFFAOYSA-N 1-hexene Chemical compound CCCCC=C LIKMAJRDDDTEIG-UHFFFAOYSA-N 0.000 description 4
- KWKAKUADMBZCLK-UHFFFAOYSA-N 1-octene Chemical compound CCCCCCC=C KWKAKUADMBZCLK-UHFFFAOYSA-N 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 239000004698 Polyethylene Substances 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 239000002131 composite material Substances 0.000 description 4
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 4
- 229910052737 gold Inorganic materials 0.000 description 4
- 239000010931 gold Substances 0.000 description 4
- 229920000092 linear low density polyethylene Polymers 0.000 description 4
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- 239000012085 test solution Substances 0.000 description 4
- QLZJUIZVJLSNDD-UHFFFAOYSA-N 2-(2-methylidenebutanoyloxy)ethyl 2-methylidenebutanoate Chemical compound CCC(=C)C(=O)OCCOC(=O)C(=C)CC QLZJUIZVJLSNDD-UHFFFAOYSA-N 0.000 description 3
- QPLDLSVMHZLSFG-UHFFFAOYSA-N Copper oxide Chemical compound [Cu]=O QPLDLSVMHZLSFG-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000002250 absorbent Substances 0.000 description 3
- 230000002745 absorbent Effects 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 238000013329 compounding Methods 0.000 description 3
- 235000014113 dietary fatty acids Nutrition 0.000 description 3
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- 239000004615 ingredient Substances 0.000 description 3
- 239000011976 maleic acid Substances 0.000 description 3
- LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 229910052763 palladium Inorganic materials 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 239000005060 rubber Substances 0.000 description 3
- 239000012748 slip agent Substances 0.000 description 3
- 239000004711 α-olefin Substances 0.000 description 3
- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- OIFBSDVPJOWBCH-UHFFFAOYSA-N Diethyl carbonate Chemical compound CCOC(=O)OCC OIFBSDVPJOWBCH-UHFFFAOYSA-N 0.000 description 2
- KMTRUDSVKNLOMY-UHFFFAOYSA-N Ethylene carbonate Chemical compound O=C1OCCO1 KMTRUDSVKNLOMY-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- 239000006096 absorbing agent Substances 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 229920005549 butyl rubber Polymers 0.000 description 2
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 description 2
- 239000008116 calcium stearate Substances 0.000 description 2
- 235000013539 calcium stearate Nutrition 0.000 description 2
- 230000009849 deactivation Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000005038 ethylene vinyl acetate Substances 0.000 description 2
- 229920006244 ethylene-ethyl acrylate Polymers 0.000 description 2
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- 238000001125 extrusion Methods 0.000 description 2
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- 235000011187 glycerol Nutrition 0.000 description 2
- 229920001684 low density polyethylene Polymers 0.000 description 2
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- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 2
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 2
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- TVMXDCGIABBOFY-UHFFFAOYSA-N n-Octanol Natural products CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 125000004430 oxygen atom Chemical group O* 0.000 description 2
- 238000005453 pelletization Methods 0.000 description 2
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 2
- 239000004014 plasticizer Substances 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 231100000572 poisoning Toxicity 0.000 description 2
- 230000000607 poisoning effect Effects 0.000 description 2
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 description 2
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- 229920005604 random copolymer Polymers 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- 229920002725 thermoplastic elastomer Polymers 0.000 description 2
- 239000001993 wax Substances 0.000 description 2
- OFNISBHGPNMTMS-UHFFFAOYSA-N 3-methylideneoxolane-2,5-dione Chemical compound C=C1CC(=O)OC1=O OFNISBHGPNMTMS-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229920000089 Cyclic olefin copolymer Polymers 0.000 description 1
- 229920002943 EPDM rubber Polymers 0.000 description 1
- 229920000181 Ethylene propylene rubber Polymers 0.000 description 1
- 101000596741 Homo sapiens Testis-specific protein TEX28 Proteins 0.000 description 1
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 239000005662 Paraffin oil Substances 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 102100035104 Testis-specific protein TEX28 Human genes 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 229920004482 WACKER® Polymers 0.000 description 1
- GJCXHYNLSNVSQZ-UHFFFAOYSA-L [Cu](Cl)Cl.Cl Chemical compound [Cu](Cl)Cl.Cl GJCXHYNLSNVSQZ-UHFFFAOYSA-L 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 229910000287 alkaline earth metal oxide Inorganic materials 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
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- 125000003118 aryl group Chemical group 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 229910000420 cerium oxide Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
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- 239000003086 colorant Substances 0.000 description 1
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- 238000007334 copolymerization reaction Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- HPDFFVBPXCTEDN-UHFFFAOYSA-N copper manganese Chemical compound [Mn].[Cu] HPDFFVBPXCTEDN-UHFFFAOYSA-N 0.000 description 1
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
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- UAUDZVJPLUQNMU-KTKRTIGZSA-N erucamide Chemical compound CCCCCCCC\C=C/CCCCCCCCCCCC(N)=O UAUDZVJPLUQNMU-KTKRTIGZSA-N 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
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- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- DIOQZVSQGTUSAI-UHFFFAOYSA-N n-butylhexane Natural products CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 description 1
- 229940110728 nitrogen / oxygen Drugs 0.000 description 1
- JCXJVPUVTGWSNB-UHFFFAOYSA-N nitrogen dioxide Inorganic materials O=[N]=O JCXJVPUVTGWSNB-UHFFFAOYSA-N 0.000 description 1
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 1
- 239000002667 nucleating agent Substances 0.000 description 1
- FATBGEAMYMYZAF-KTKRTIGZSA-N oleamide Chemical compound CCCCCCCC\C=C/CCCCCCCC(N)=O FATBGEAMYMYZAF-KTKRTIGZSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 239000011941 photocatalyst Substances 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
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- 230000002265 prevention Effects 0.000 description 1
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- 125000003011 styrenyl group Chemical class [H]\C(*)=C(/[H])C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
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- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 238000003221 volumetric titration Methods 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/62—Carbon oxides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/86—Catalytic processes
- B01D53/864—Removing carbon monoxide or hydrocarbons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
- B01J20/0222—Compounds of Mn, Re
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/0203—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of metals not provided for in B01J20/04
- B01J20/0233—Compounds of Cu, Ag, Au
- B01J20/0237—Compounds of Cu
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
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Abstract
Description
本発明は、非水電解質二次電池や電気二重層キャパシタなどの蓄電デバイスにおける、蓄電要素が封入された容器内において発生する一酸化炭素の処理に適する方法に関する。
(A)樹脂 100質量部、および
(B)一酸化炭素酸化触媒 1〜300質量部
を含む樹脂組成物からなる成形体を提供する。
(A)樹脂100質量部、および
(B)一酸化炭素酸化触媒1〜300質量部
を含む樹脂組成物からなる成形体(1)により行うことができる。
(C)二酸化炭素吸着物質
により行うことができる。上記成分(C)は、上記成分(A)との組成物からなる成形体(2)の形であってもよく、あるいは、上記成分(A)および(B)との組成物からなる成形体(3)の形であってもよい。
(i)DSC融解曲線における最も高い温度側のピークトップ融点(Tm)が110℃以上である、
(ii)DSC融解曲線における融解熱量(ΔH)が90〜180J/gである、
(iii)110℃における結晶化度(Xc110)が10〜60%である、および
(iv)MFR(190℃、21.18N)が0.1g/10分以上10g/10分未満である。
表1に示す配合量(質量部)の成分をドライブレンドし、これを(株)日本製鋼所の二軸押出機TEX28により溶融混練し、樹脂組成物のペレットを得た。二軸押出機出口樹脂温度は240℃であった(真空ベント使用)。得られた樹脂組成物ペレットを、(株)日本製鋼所の二軸押出機を使用し、ギヤポンプを介して、東芝機械株式会社製の単層Tダイへと送って製膜し、膜厚50μmのフィルムを得た。二軸押出機出口樹脂温度は220℃であり(真空ベント使用)、ギヤポンプ出口樹脂温度は220℃であった。また、製膜は、Tダイ出口樹脂温度220℃、チルロール温度40℃、引取速度10m/分の条件で行った。得られたフィルムは、露点温度−50℃以下にしたガス置換型グローブボックス(アズワン株式会社のSG−1000)の中に保管した。得られたフィルムについて、下記(1)〜(3)の評価試験を行った。結果を表1および表2に示す。実施例2、5、6および13については、下記(4)の試験も行った。
テトラバックに1000cm2のフィルムを入れ、255mLの窒素を充填した。ここに45mLの一酸化炭素を注入した(一酸化炭素の計算濃度:15vol%)。これを24時間、常温、常圧で放置した後、一酸化炭素濃度および二酸化炭素濃度をガスクロマトグラフにより測定した。なお、テトラバックからはガスが少しずつ透過して抜けるため、同時にブランク(上記フィルムを使用しない場合)の測定も行ったところ、24時間後の一酸化炭素濃度は14.1vol%であり、二酸化炭素は検出されなかった。
上記(1)の試験おいて、255mLの窒素の代わりに255mLの空気(窒素/酸素=80/20(体積比))を用いた以外は試験(1)と同様に測定を行った。ブランクでの一酸化炭素濃度は14.2vol%であり、二酸化炭素は検出されなかった。
二酸化炭素は透過性が高いため、フィルムによる二酸化炭素の吸着能の測定を行った。上記(1)の試験おいて、45mLの一酸化炭素を注入する代わりに、45mLの二酸化炭素を注入した以外は試験(1)と同様にして、二酸化炭素濃度の測定を行った。ブランクでの二酸化炭素濃度は12.3vol%であった。
ジメチルカーボネート(DMC)/ジエチルカーボネート(DEC)/エチレンカーボネート(EC)=1/1/1(容積比)に水を極少量混合し、試験液とした。この試験液中の水分量をカールフィッシャー容量滴定装置(平沼産業株式会社のAQ−300)により測定したところ982ppmであった。次いで、この試験液30g中に450cm2のフィルムを浸漬して、25℃×48hr後に試験液中の水分量を同様に測定した。以上の操作はアイ・エイ・シー株式会社のエアードライヤーQD20−75により露点温度−50℃以下にしたガス置換型グローブボックス(アズワン株式会社のSG−1000)中で行った。
成分(A)
KF271:日本ポリエチレン(株)製、直鎖状低密度ポリエチレン、MFR(190℃、21.18N)=2.4g/10分、密度913kg/m3、Tm=127℃、ΔH=127J/g、Xc110=26%
KF360:日本ポリエチレン(株)製、超低密度ポリエチレン、MFR(190℃、21.18N)=3.5g/10分、密度898kg/m3、Tm=111℃、ΔH=92J/g、Xc110=5%
F−730NV:プライムポリマー(株)製、プロピレンランダムコポリマー、MFR(190℃、21.18N)=7g/10分
アドマーXE070:三井化学(株)製、無水マレイン酸変性エチレン系重合体、MFR(190℃、21.18N)=3 g/10分
アドマーXM7070:三井化学(株)製、プロピレン系ランダム共重合体、MFR(230℃、21.18N)=7g/10分
ホプカライト:ジーエルサイエンス(株)製の複合金属酸化物触媒(CuMn2O4)、乳鉢で粉砕・分級したもの、D99=12μm、D50=3μm
5%Pd−MgO−01:エヌ・イー・ケムキャット(株)製の酸化マグネシウム担持パラジウム触媒、担持量5質量%、D99=6μm、D50=2μm
ゼオラムA4 LPH:東ソー(株)製、A型ゼオライト(モレキュラーシーブ4A)、D99=20μm、D50=12μm
STO:堺化学工業(株)製、酸化ストロンチウム、粗粉を分級したもの、D99=18μm、D50=5μm
スターマグPSF−150F:神島化学工業(株)製の高BET酸化マグネシウム、BET比表面積=150m2/g 、D99=3μm、D50=1μm
スターマグU:神島化学工業(株)製の高BET酸化マグネシウム、BET比表面積=125m2/g 、D99=6μm、D50=2μm
スターマグP:神島化学工業(株)製の酸化マグネシウム、BET比表面積=10m2/g、D99=9μm、D50=3μm
LBT−77:堺化学工業(株)製、ポリエチレンワックス
ステアリン酸カルシウム
モレキュラーシーブ3Aパウダー:ユニオン昭和(株)製、細孔径0.3mmのA型ゼオライト、粗粉を分級したもの、D99=19μm、D50=9μm
Claims (19)
- 気体状酸素が実質的に存在せずかつ一酸化炭素を発生する物質を収容する密閉容器内において発生する一酸化炭素を該容器内で処理する方法において、一酸化炭素を二酸化炭素に酸化すること、および二酸化炭素を該容器内で吸着することを含む方法。
- 該密閉容器が、蓄電デバイスにおける蓄電要素が封入された容器である、請求項1記載の方法。
- 上記酸化が、該容器内に予め配置された、
(A)樹脂 100質量部、および
(B)一酸化炭素酸化触媒 1〜300質量部
を含む樹脂組成物からなる成形体によって行われる、請求項1または2記載の方法。 - 上記吸着が、該容器内に予め配置された、
(C)二酸化炭素吸着物質
により行われる、請求項1〜3のいずれか1項に記載の方法。 - 成分(C)が、
(A)樹脂 100質量部、および
(C)二酸化炭素吸着物質 1〜300質量部
を含む樹脂組成物からなる成形体である、請求項1〜4のいずれか1項に記載の方法。 - 成分(C)が、
(A)樹脂 100質量部、
(B)一酸化炭素酸化触媒 1〜300質量部、および
(C)二酸化炭素吸着物質 1〜300質量部
を含む樹脂組成物からなる成形体である、請求項1〜5のいずれか1項に記載の方法。 - 成分(B)が、ホプカライトおよび担持貴金属触媒から成る群から選択される少なくとも1を含む、請求項3〜6のいずれか1項に記載の方法。
- 成分(C)が、二酸化炭素の吸着に水を必要としないものである、請求項4〜7のいずれか1項に記載の方法。
- 成分(C)が、酸化ストロンチウム、0.4nm以上の細孔径を有するゼオライト、およびBET比表面積が50m2/g以上である酸化マグネシウムからなる群から選択される少なくとも1を含む、請求項4〜8のいずれか1項に記載の方法。
- 成分(A)が、エチレン系重合体および酸変性エチレン系樹脂を含むエチレン系樹脂組成物である、請求項3〜9のいずれか1項に記載の方法。
- (A)樹脂 100質量部、および
(B)一酸化炭素酸化触媒 1〜300質量部
を含む樹脂組成物からなる成形体。 - 樹脂組成物が
(C)二酸化炭素吸着物質 1〜300質量部
をさらに含む、請求項11に記載の成形体。 - 成分(B)が、ホプカライトおよび担持貴金属触媒から成る群から選択される少なくとも1を含む、
請求項11または12に記載の成形体。 - 成分(C)が、二酸化炭素の吸着に水を必要としないものである、請求項12または13に記載の成形体。
- 成分(C)が、酸化ストロンチウム、0.4nm以上の細孔径を有するゼオライト、およびBET比表面積が50m2/g以上である酸化マグネシウムからなる群から選択される少なくとも1を含む、請求項12〜14のいずれか1項に記載の成形体。
- 成分(A)が、エチレン系重合体および酸変性エチレン系樹脂を含むエチレン系樹脂組成物である、請求項11〜15のいずれか1項に記載の成形体。
- 成形体がフィルム状である、請求項11〜16 のいずれか1項に記載の成形体。
- 請求項11〜17のいずれか1項に記載の成形体を蓄電要素が封入された容器の中に含む非水電解質二次電池。
- 請求項11〜17のいずれか1項に記載の成形体を蓄電要素が封入された容器の中に含む電気二重層キャパシタ。
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