JPS6214145A

JPS6214145A - ポジ画像形成方法

ポジ画像形成方法

Info

Publication number: JPS6214145A
Authority: JP; Japan
Prior art keywords: silver; silver halide; emulsion; dye; group
Prior art date: 1985-07-11
Legal status : Granted

Application number

JP15280385A

Other languages

English (en)

Japanese (ja)

Other versions

JPH0555029B2 (enrdf_load_stackoverflow

Inventor

Sohei Goto

後藤　宗平

Tatsuhiko Kobayashi

小林　龍彦

Ken Okauchi

謙岡内

Current Assignee

Konica Minolta Inc

Original Assignee

Konica Minolta Inc

Priority date

1985-07-11

Filing date

1985-07-11

Publication date

1987-01-22

1985-07-11 Application filed by Konica Minolta Inc filed Critical Konica Minolta Inc

1985-07-11 Priority to JP15280385A priority Critical patent/JPS6214145A/ja

1985-12-30 Priority to DE8585309538T priority patent/DE3586719T2/de

1985-12-30 Priority to EP85309538A priority patent/EP0190512B1/en

1987-01-22 Publication of JPS6214145A publication Critical patent/JPS6214145A/ja

1988-04-13 Priority to US07/183,432 priority patent/US4868089A/en

1993-08-16 Publication of JPH0555029B2 publication Critical patent/JPH0555029B2/ja

Status Granted legal-status Critical Current

Links

229910052709 silver Inorganic materials 0.000 claims abstract description 303
239000004332 silver Substances 0.000 claims abstract description 302
-1 silver halide Chemical class 0.000 claims abstract description 278
239000000839 emulsion Substances 0.000 claims abstract description 176
239000000463 material Substances 0.000 claims abstract description 131
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 81
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 40
230000035945 sensitivity Effects 0.000 claims abstract description 28
239000001257 hydrogen Substances 0.000 claims abstract description 11
229910052739 hydrogen Inorganic materials 0.000 claims abstract description 11
125000004435 hydrogen atom Chemical class [H]* 0.000 claims abstract description 5
BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 105
238000000034 method Methods 0.000 claims description 82
206010070834 Sensitisation Diseases 0.000 claims description 38
230000008313 sensitization Effects 0.000 claims description 37
230000008569 process Effects 0.000 claims description 26
230000001235 sensitizing effect Effects 0.000 claims description 17
230000015572 biosynthetic process Effects 0.000 claims description 5
230000026030 halogenation Effects 0.000 claims description 2
238000005658 halogenation reaction Methods 0.000 claims description 2
239000007789 gas Substances 0.000 abstract description 13
239000012298 atmosphere Substances 0.000 abstract description 9
229910021529 ammonia Inorganic materials 0.000 abstract description 7
RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 abstract description 4
229910000037 hydrogen sulfide Inorganic materials 0.000 abstract description 3
LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 abstract 1
230000000284 resting effect Effects 0.000 abstract 1
239000000243 solution Substances 0.000 description 101
239000000975 dye Substances 0.000 description 98
239000010410 layer Substances 0.000 description 78
108010010803 Gelatin Proteins 0.000 description 60
239000008273 gelatin Substances 0.000 description 60
229920000159 gelatin Polymers 0.000 description 60
235000019322 gelatine Nutrition 0.000 description 60
235000011852 gelatine desserts Nutrition 0.000 description 60
239000000126 substance Substances 0.000 description 59
150000001875 compounds Chemical class 0.000 description 51
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 46
238000011161 development Methods 0.000 description 46
230000018109 developmental process Effects 0.000 description 46
239000007864 aqueous solution Substances 0.000 description 45
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 40
239000003795 chemical substances by application Substances 0.000 description 38
239000002245 particle Substances 0.000 description 30
ZUNKMNLKJXRCDM-UHFFFAOYSA-N silver bromoiodide Chemical compound [Ag].IBr ZUNKMNLKJXRCDM-UHFFFAOYSA-N 0.000 description 30
GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 28
229910052751 metal Inorganic materials 0.000 description 27
239000002184 metal Substances 0.000 description 27
238000000576 coating method Methods 0.000 description 24
239000002253 acid Substances 0.000 description 23
229920000642 polymer Polymers 0.000 description 23
239000011248 coating agent Substances 0.000 description 21
150000003839 salts Chemical class 0.000 description 21
239000000203 mixture Substances 0.000 description 20
IOLCXVTUBQKXJR-UHFFFAOYSA-M potassium bromide Chemical compound [K+].[Br-] IOLCXVTUBQKXJR-UHFFFAOYSA-M 0.000 description 20
ADZWSOLPGZMUMY-UHFFFAOYSA-M silver bromide Chemical compound [Ag]Br ADZWSOLPGZMUMY-UHFFFAOYSA-M 0.000 description 20
238000012545 processing Methods 0.000 description 19
239000000049 pigment Substances 0.000 description 18
SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 18
238000007792 addition Methods 0.000 description 17
239000003638 chemical reducing agent Substances 0.000 description 17
125000001424 substituent group Chemical group 0.000 description 17
238000012546 transfer Methods 0.000 description 17
239000006185 dispersion Substances 0.000 description 16
NDVLTYZPCACLMA-UHFFFAOYSA-N silver oxide Chemical compound [O-2].[Ag+].[Ag+] NDVLTYZPCACLMA-UHFFFAOYSA-N 0.000 description 16
SJOOOZPMQAWAOP-UHFFFAOYSA-N [Ag].BrCl Chemical compound [Ag].BrCl SJOOOZPMQAWAOP-UHFFFAOYSA-N 0.000 description 15
238000006243 chemical reaction Methods 0.000 description 15
230000003287 optical effect Effects 0.000 description 14
230000002829 reductive effect Effects 0.000 description 14
239000004698 Polyethylene Substances 0.000 description 13
229910021612 Silver iodide Inorganic materials 0.000 description 13
125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 13
229920000573 polyethylene Polymers 0.000 description 13
239000004094 surface-active agent Substances 0.000 description 13
239000011230 binding agent Substances 0.000 description 12
238000005859 coupling reaction Methods 0.000 description 12
239000004848 polyfunctional curative Substances 0.000 description 12
HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 12
JKFYKCYQEWQPTM-UHFFFAOYSA-N 2-azaniumyl-2-(4-fluorophenyl)acetate Chemical compound OC(=O)C(N)C1=CC=C(F)C=C1 JKFYKCYQEWQPTM-UHFFFAOYSA-N 0.000 description 11
239000002202 Polyethylene glycol Substances 0.000 description 11
229910021607 Silver chloride Inorganic materials 0.000 description 11
125000000217 alkyl group Chemical group 0.000 description 11
239000012153 distilled water Substances 0.000 description 11
150000004820 halides Chemical group 0.000 description 11
DZVCFNFOPIZQKX-LTHRDKTGSA-M merocyanine Chemical compound [Na+].O=C1N(CCCC)C(=O)N(CCCC)C(=O)C1=C\C=C\C=C/1N(CCCS([O-])(=O)=O)C2=CC=CC=C2O\1 DZVCFNFOPIZQKX-LTHRDKTGSA-M 0.000 description 11
238000002156 mixing Methods 0.000 description 11
229920001223 polyethylene glycol Polymers 0.000 description 11
229940045105 silver iodide Drugs 0.000 description 11
ANRHNWWPFJCPAZ-UHFFFAOYSA-M thionine Chemical compound [Cl-].C1=CC(N)=CC2=[S+]C3=CC(N)=CC=C3N=C21 ANRHNWWPFJCPAZ-UHFFFAOYSA-M 0.000 description 11
229920002554 vinyl polymer Polymers 0.000 description 11
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 10
WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 10
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 10
230000000694 effects Effects 0.000 description 10
239000002904 solvent Substances 0.000 description 10
125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 10
SJVGFKBLUYAEOK-SFHVURJKSA-N 6-[4-[(3S)-3-(3,5-difluorophenyl)-3,4-dihydropyrazole-2-carbonyl]piperidin-1-yl]pyrimidine-4-carbonitrile Chemical compound FC=1C=C(C=C(C=1)F)[C@@H]1CC=NN1C(=O)C1CCN(CC1)C1=CC(=NC=N1)C#N SJVGFKBLUYAEOK-SFHVURJKSA-N 0.000 description 9
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 9
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 9
125000003118 aryl group Chemical group 0.000 description 9
230000008878 coupling Effects 0.000 description 9
238000010168 coupling process Methods 0.000 description 9
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 9
238000011160 research Methods 0.000 description 9
229910001961 silver nitrate Inorganic materials 0.000 description 9
RSIWALKZYXPAGW-NSHDSACASA-N 6-(3-fluorophenyl)-3-methyl-7-[(1s)-1-(7h-purin-6-ylamino)ethyl]-[1,3]thiazolo[3,2-a]pyrimidin-5-one Chemical compound C=1([C@@H](NC=2C=3N=CNC=3N=CN=2)C)N=C2SC=C(C)N2C(=O)C=1C1=CC=CC(F)=C1 RSIWALKZYXPAGW-NSHDSACASA-N 0.000 description 8
150000003863 ammonium salts Chemical class 0.000 description 8
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 8
229910052736 halogen Inorganic materials 0.000 description 8
239000003112 inhibitor Substances 0.000 description 8
229910021645 metal ion Inorganic materials 0.000 description 8
VZUGBLTVBZJZOE-KRWDZBQOSA-N n-[3-[(4s)-2-amino-1,4-dimethyl-6-oxo-5h-pyrimidin-4-yl]phenyl]-5-chloropyrimidine-2-carboxamide Chemical compound N1=C(N)N(C)C(=O)C[C@@]1(C)C1=CC=CC(NC(=O)C=2N=CC(Cl)=CN=2)=C1 VZUGBLTVBZJZOE-KRWDZBQOSA-N 0.000 description 8
239000005020 polyethylene terephthalate Substances 0.000 description 8
229920000139 polyethylene terephthalate Polymers 0.000 description 8
238000002360 preparation method Methods 0.000 description 8
229910001923 silver oxide Inorganic materials 0.000 description 8
159000000000 sodium salts Chemical class 0.000 description 8
239000003381 stabilizer Substances 0.000 description 8
238000003756 stirring Methods 0.000 description 8
IBWXIFXUDGADCV-UHFFFAOYSA-N 2h-benzotriazole;silver Chemical compound [Ag].C1=CC=C2NN=NC2=C1 IBWXIFXUDGADCV-UHFFFAOYSA-N 0.000 description 7
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 7
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 7
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 7
125000003277 amino group Chemical group 0.000 description 7
229920002678 cellulose Polymers 0.000 description 7
239000000084 colloidal system Substances 0.000 description 7
150000002367 halogens Chemical class 0.000 description 7
125000000623 heterocyclic group Chemical group 0.000 description 7
150000003378 silver Chemical class 0.000 description 7
239000011734 sodium Substances 0.000 description 7
229910052708 sodium Inorganic materials 0.000 description 7
239000011593 sulfur Substances 0.000 description 7
229910052717 sulfur Inorganic materials 0.000 description 7
CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 6
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 6
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 6
RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 6
125000002777 acetyl group Chemical group [H]C([H])([H])C(*)=O 0.000 description 6
150000007513 acids Chemical class 0.000 description 6
125000003545 alkoxy group Chemical group 0.000 description 6
229960000510 ammonia Drugs 0.000 description 6
239000001913 cellulose Substances 0.000 description 6
229920001577 copolymer Polymers 0.000 description 6
238000010438 heat treatment Methods 0.000 description 6
150000002431 hydrogen Chemical group 0.000 description 6
QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 6
229940063557 methacrylate Drugs 0.000 description 6
229910052757 nitrogen Inorganic materials 0.000 description 6
XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 6
229920000515 polycarbonate Polymers 0.000 description 6
239000004417 polycarbonate Substances 0.000 description 6
229920000036 polyvinylpyrrolidone Polymers 0.000 description 6
239000001267 polyvinylpyrrolidone Substances 0.000 description 6
235000013855 polyvinylpyrrolidone Nutrition 0.000 description 6
NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 description 6
HMGKNQRMNITOOM-UHFFFAOYSA-M silver;2h-benzotriazole-4-sulfonate Chemical compound [Ag+].[O-]S(=O)(=O)C1=CC=CC2=NNN=C12 HMGKNQRMNITOOM-UHFFFAOYSA-M 0.000 description 6
XGMYMWYPSYIPQB-UHFFFAOYSA-J tetrasodium;2-(1,2-dicarboxylatoethoxy)butanedioate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CC(C([O-])=O)OC(C([O-])=O)CC([O-])=O XGMYMWYPSYIPQB-UHFFFAOYSA-J 0.000 description 6
ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 5
CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 5
CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 5
125000004429 atom Chemical group 0.000 description 5
125000003917 carbamoyl group Chemical group [H]N([H])C(*)=O 0.000 description 5
125000004432 carbon atom Chemical group C* 0.000 description 5
239000013256 coordination polymer Substances 0.000 description 5
239000011521 glass Substances 0.000 description 5
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 5
229910052737 gold Inorganic materials 0.000 description 5
239000010931 gold Substances 0.000 description 5
125000002887 hydroxy group Chemical group [H]O* 0.000 description 5
239000011630 iodine Substances 0.000 description 5
229910052740 iodine Inorganic materials 0.000 description 5
150000002736 metal compounds Chemical class 0.000 description 5
235000013336 milk Nutrition 0.000 description 5
239000008267 milk Substances 0.000 description 5
210000004080 milk Anatomy 0.000 description 5
125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 5
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 5
229920000728 polyester Polymers 0.000 description 5
239000011591 potassium Substances 0.000 description 5
229910052700 potassium Inorganic materials 0.000 description 5
239000001103 potassium chloride Substances 0.000 description 5
235000011164 potassium chloride Nutrition 0.000 description 5
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 5
KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 4
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 4
OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 4
229910019142 PO4 Inorganic materials 0.000 description 4
239000004952 Polyamide Substances 0.000 description 4
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 4
SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 4
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 4
239000000654 additive Substances 0.000 description 4
229910052782 aluminium Inorganic materials 0.000 description 4
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 4
125000004397 aminosulfonyl group Chemical group NS(=O)(=O)* 0.000 description 4
KXNQKOAQSGJCQU-UHFFFAOYSA-N benzo[e][1,3]benzothiazole Chemical class C1=CC=C2C(N=CS3)=C3C=CC2=C1 KXNQKOAQSGJCQU-UHFFFAOYSA-N 0.000 description 4
QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 description 4
239000012964 benzotriazole Substances 0.000 description 4
150000001565 benzotriazoles Chemical class 0.000 description 4
150000002148 esters Chemical class 0.000 description 4
239000004744 fabric Substances 0.000 description 4
230000006870 function Effects 0.000 description 4
239000007788 liquid Substances 0.000 description 4
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 4
125000000962 organic group Chemical group 0.000 description 4
235000021317 phosphate Nutrition 0.000 description 4
229920002647 polyamide Polymers 0.000 description 4
239000004800 polyvinyl chloride Substances 0.000 description 4
229920000915 polyvinyl chloride Polymers 0.000 description 4
238000006722 reduction reaction Methods 0.000 description 4
AKHNMLFCWUSKQB-UHFFFAOYSA-L sodium thiosulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=S AKHNMLFCWUSKQB-UHFFFAOYSA-L 0.000 description 4
235000019345 sodium thiosulphate Nutrition 0.000 description 4
238000005406 washing Methods 0.000 description 4
QIVUCLWGARAQIO-OLIXTKCUSA-N (3s)-n-[(3s,5s,6r)-6-methyl-2-oxo-1-(2,2,2-trifluoroethyl)-5-(2,3,6-trifluorophenyl)piperidin-3-yl]-2-oxospiro[1h-pyrrolo[2,3-b]pyridine-3,6'-5,7-dihydrocyclopenta[b]pyridine]-3'-carboxamide Chemical compound C1([C@H]2[C@H](N(C(=O)[C@@H](NC(=O)C=3C=C4C[C@]5(CC4=NC=3)C3=CC=CN=C3NC5=O)C2)CC(F)(F)F)C)=C(F)C=CC(F)=C1F QIVUCLWGARAQIO-OLIXTKCUSA-N 0.000 description 3
CDAWCLOXVUBKRW-UHFFFAOYSA-N 2-aminophenol Chemical class NC1=CC=CC=C1O CDAWCLOXVUBKRW-UHFFFAOYSA-N 0.000 description 3
PLYFWZGSBMDRKW-UHFFFAOYSA-N 2h-benzotriazole-4-sulfonic acid;silver Chemical compound [Ag].OS(=O)(=O)C1=CC=CC2=NNN=C12 PLYFWZGSBMDRKW-UHFFFAOYSA-N 0.000 description 3
AHHQDHCTHYTBSV-UHFFFAOYSA-N 3-methylpentane-1,3,5-triol Chemical compound OCCC(O)(C)CCO AHHQDHCTHYTBSV-UHFFFAOYSA-N 0.000 description 3
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 3
KXDAEFPNCMNJSK-UHFFFAOYSA-N Benzamide Chemical compound NC(=O)C1=CC=CC=C1 KXDAEFPNCMNJSK-UHFFFAOYSA-N 0.000 description 3
WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 3
ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 3
239000001856 Ethyl cellulose Substances 0.000 description 3
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
229920003171 Poly (ethylene oxide) Polymers 0.000 description 3
239000004793 Polystyrene Substances 0.000 description 3
KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
XOXLDCZKFZMLML-UHFFFAOYSA-N [4-(diethylamino)-2-methylphenyl]sulfamic acid Chemical compound CCN(CC)C1=CC=C(NS(O)(=O)=O)C(C)=C1 XOXLDCZKFZMLML-UHFFFAOYSA-N 0.000 description 3
XCFIVNQHHFZRNR-UHFFFAOYSA-N [Ag].Cl[IH]Br Chemical compound [Ag].Cl[IH]Br XCFIVNQHHFZRNR-UHFFFAOYSA-N 0.000 description 3
150000001412 amines Chemical class 0.000 description 3
150000001413 amino acids Chemical group 0.000 description 3
239000002216 antistatic agent Substances 0.000 description 3
235000010323 ascorbic acid Nutrition 0.000 description 3
229960005070 ascorbic acid Drugs 0.000 description 3
239000011668 ascorbic acid Substances 0.000 description 3
229920002301 cellulose acetate Polymers 0.000 description 3
239000000460 chlorine Substances 0.000 description 3
239000003086 colorant Substances 0.000 description 3
239000000470 constituent Substances 0.000 description 3
239000013078 crystal Substances 0.000 description 3
125000004093 cyano group Chemical group *C#N 0.000 description 3
235000014113 dietary fatty acids Nutrition 0.000 description 3
238000009792 diffusion process Methods 0.000 description 3
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