JPS61286221A - 白色導電性粉末の製造方法 - Google Patents

Info

Publication number

JPS61286221A

JPS61286221A JP12390085A JP12390085A JPS61286221A JP S61286221 A JPS61286221 A JP S61286221A JP 12390085 A JP12390085 A JP 12390085A JP 12390085 A JP12390085 A JP 12390085A JP S61286221 A JPS61286221 A JP S61286221A

Authority

JP

Japan

Prior art keywords

powder

suspension

antimony

chloride

oxide

Prior art date

1985-06-07

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Granted

Links

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• 239000000843 powder Substances 0.000 title claims abstract description 64
• 239000000725 suspension Substances 0.000 claims abstract description 32
• XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims abstract description 24
• 150000004706 metal oxides Chemical class 0.000 claims abstract description 21
• 229910001361 White metal Inorganic materials 0.000 claims abstract description 20
• 239000010969 white metal Substances 0.000 claims abstract description 20
• 229910001887 tin oxide Inorganic materials 0.000 claims abstract description 18
• FAPDDOBMIUGHIN-UHFFFAOYSA-K antimony trichloride Chemical compound Cl[Sb](Cl)Cl FAPDDOBMIUGHIN-UHFFFAOYSA-K 0.000 claims abstract description 17
• HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 claims abstract description 17
• 229910000410 antimony oxide Inorganic materials 0.000 claims abstract description 16
• VTRUBDSFZJNXHI-UHFFFAOYSA-N oxoantimony Chemical compound [Sb]=O VTRUBDSFZJNXHI-UHFFFAOYSA-N 0.000 claims abstract description 16
• 239000002245 particle Substances 0.000 claims abstract description 10
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 25
• 239000011247 coating layer Substances 0.000 claims description 14
• 239000000243 solution Substances 0.000 claims description 13
• 239000007864 aqueous solution Substances 0.000 claims description 12
• 238000004519 manufacturing process Methods 0.000 claims description 6
• 239000007900 aqueous suspension Substances 0.000 claims description 3
• 239000003513 alkali Substances 0.000 abstract description 5
• 150000004677 hydrates Chemical class 0.000 abstract description 2
• 239000000463 material Substances 0.000 abstract description 2
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
• GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 51
• 238000000034 method Methods 0.000 description 25
• 239000004408 titanium dioxide Substances 0.000 description 24
• 238000006386 neutralization reaction Methods 0.000 description 21
• 230000000052 comparative effect Effects 0.000 description 19
• HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
• 238000010438 heat treatment Methods 0.000 description 4
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
• KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
• 239000003795 chemical substances by application Substances 0.000 description 3
• 238000010304 firing Methods 0.000 description 3
• 230000007062 hydrolysis Effects 0.000 description 3
• 238000006460 hydrolysis reaction Methods 0.000 description 3
• 239000000049 pigment Substances 0.000 description 3
• 238000001556 precipitation Methods 0.000 description 3
• QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
• CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 2
• VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
• CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
• MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
• 229910052787 antimony Inorganic materials 0.000 description 2
• WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 2
• 239000002585 base Substances 0.000 description 2
• 238000000151 deposition Methods 0.000 description 2
• 238000001914 filtration Methods 0.000 description 2
• 229910044991 metal oxide Inorganic materials 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
• XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 1
• 239000002253 acid Substances 0.000 description 1
• 230000002378 acidificating effect Effects 0.000 description 1
• 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
• 239000012670 alkaline solution Substances 0.000 description 1
• PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
• 229910021529 ammonia Inorganic materials 0.000 description 1
• 239000002216 antistatic agent Substances 0.000 description 1
• 230000000711 cancerogenic effect Effects 0.000 description 1
• 239000006229 carbon black Substances 0.000 description 1
• 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
• 231100000315 carcinogenic Toxicity 0.000 description 1
• 239000004927 clay Substances 0.000 description 1
• 229910052570 clay Inorganic materials 0.000 description 1
• 238000000576 coating method Methods 0.000 description 1
• 230000008021 deposition Effects 0.000 description 1
• 230000000694 effects Effects 0.000 description 1
• 238000011156 evaluation Methods 0.000 description 1
• 239000000835 fiber Substances 0.000 description 1
• 239000000706 filtrate Substances 0.000 description 1
• 239000010410 layer Substances 0.000 description 1
• 239000000395 magnesium oxide Substances 0.000 description 1
• 239000011259 mixed solution Substances 0.000 description 1
• 230000003472 neutralizing effect Effects 0.000 description 1
• 239000003960 organic solvent Substances 0.000 description 1
• WMHSAFDEIXKKMV-UHFFFAOYSA-N oxoantimony;oxotin Chemical compound [Sn]=O.[Sb]=O WMHSAFDEIXKKMV-UHFFFAOYSA-N 0.000 description 1
• 239000004033 plastic Substances 0.000 description 1
• 229920003023 plastic Polymers 0.000 description 1
• 229910000027 potassium carbonate Inorganic materials 0.000 description 1
• 238000010298 pulverizing process Methods 0.000 description 1
• 238000011084 recovery Methods 0.000 description 1
• 239000000377 silicon dioxide Substances 0.000 description 1
• 229910000029 sodium carbonate Inorganic materials 0.000 description 1
• 239000006104 solid solution Substances 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 239000000126 substance Substances 0.000 description 1
• 238000009283 thermal hydrolysis Methods 0.000 description 1
• 238000005406 washing Methods 0.000 description 1
• 239000012463 white pigment Substances 0.000 description 1
• 239000011787 zinc oxide Substances 0.000 description 1
• 235000014692 zinc oxide Nutrition 0.000 description 1

Cited By (4)