JPS61174103A - 金属酸化物からなる多孔質真球状微粒子粉末の製造法 - Google Patents
金属酸化物からなる多孔質真球状微粒子粉末の製造法Info
- Publication number
- JPS61174103A JPS61174103A JP60011718A JP1171885A JPS61174103A JP S61174103 A JPS61174103 A JP S61174103A JP 60011718 A JP60011718 A JP 60011718A JP 1171885 A JP1171885 A JP 1171885A JP S61174103 A JPS61174103 A JP S61174103A
- Authority
- JP
- Japan
- Prior art keywords
- powder
- particle size
- oxide
- slurry
- size distribution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 89
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 229910044991 metal oxide Inorganic materials 0.000 title 1
- 238000000034 method Methods 0.000 claims abstract description 37
- 239000007788 liquid Substances 0.000 claims abstract description 26
- 239000011148 porous material Substances 0.000 claims abstract description 26
- 239000002002 slurry Substances 0.000 claims abstract description 21
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 8
- 238000005507 spraying Methods 0.000 claims abstract description 4
- 239000011164 primary particle Substances 0.000 claims abstract description 3
- 239000002245 particle Substances 0.000 claims description 81
- 238000001035 drying Methods 0.000 claims description 26
- 239000010419 fine particle Substances 0.000 claims description 11
- 229910052809 inorganic oxide Inorganic materials 0.000 claims description 8
- 229910052787 antimony Inorganic materials 0.000 claims description 3
- 229910052749 magnesium Inorganic materials 0.000 claims description 3
- 229910052718 tin Inorganic materials 0.000 claims description 3
- 229910052725 zinc Inorganic materials 0.000 claims description 3
- 229910052742 iron Inorganic materials 0.000 claims description 2
- 229910052726 zirconium Inorganic materials 0.000 claims description 2
- 239000000084 colloidal system Substances 0.000 abstract description 7
- 239000000203 mixture Substances 0.000 abstract description 7
- 239000000945 filler Substances 0.000 abstract description 6
- 229910052814 silicon oxide Inorganic materials 0.000 abstract 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 34
- 238000000635 electron micrograph Methods 0.000 description 24
- 230000000052 comparative effect Effects 0.000 description 14
- 239000000499 gel Substances 0.000 description 12
- 239000007789 gas Substances 0.000 description 11
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 10
- AYOOGWWGECJQPI-NSHDSACASA-N n-[(1s)-1-(5-fluoropyrimidin-2-yl)ethyl]-3-(3-propan-2-yloxy-1h-pyrazol-5-yl)imidazo[4,5-b]pyridin-5-amine Chemical compound N1C(OC(C)C)=CC(N2C3=NC(N[C@@H](C)C=4N=CC(F)=CN=4)=CC=C3N=C2)=N1 AYOOGWWGECJQPI-NSHDSACASA-N 0.000 description 10
- 239000012530 fluid Substances 0.000 description 9
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 9
- 239000000377 silicon dioxide Substances 0.000 description 9
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 9
- 229910002012 Aerosil® Inorganic materials 0.000 description 6
- 239000000017 hydrogel Substances 0.000 description 6
- 238000001694 spray drying Methods 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 239000010936 titanium Substances 0.000 description 6
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 5
- 239000000049 pigment Substances 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 229910002016 Aerosil® 200 Inorganic materials 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- XULSCZPZVQIMFM-IPZQJPLYSA-N odevixibat Chemical compound C12=CC(SC)=C(OCC(=O)N[C@@H](C(=O)N[C@@H](CC)C(O)=O)C=3C=CC(O)=CC=3)C=C2S(=O)(=O)NC(CCCC)(CCCC)CN1C1=CC=CC=C1 XULSCZPZVQIMFM-IPZQJPLYSA-N 0.000 description 3
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 3
- 238000010298 pulverizing process Methods 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- QIVUCLWGARAQIO-OLIXTKCUSA-N (3s)-n-[(3s,5s,6r)-6-methyl-2-oxo-1-(2,2,2-trifluoroethyl)-5-(2,3,6-trifluorophenyl)piperidin-3-yl]-2-oxospiro[1h-pyrrolo[2,3-b]pyridine-3,6'-5,7-dihydrocyclopenta[b]pyridine]-3'-carboxamide Chemical compound C1([C@H]2[C@H](N(C(=O)[C@@H](NC(=O)C=3C=C4C[C@]5(CC4=NC=3)C3=CC=CN=C3NC5=O)C2)CC(F)(F)F)C)=C(F)C=CC(F)=C1F QIVUCLWGARAQIO-OLIXTKCUSA-N 0.000 description 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- 239000011324 bead Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000010304 firing Methods 0.000 description 2
- 239000000417 fungicide Substances 0.000 description 2
- 230000003301 hydrolyzing effect Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- 239000012798 spherical particle Substances 0.000 description 2
- LLZRNZOLAXHGLL-UHFFFAOYSA-J titanic acid Chemical compound O[Ti](O)(O)O LLZRNZOLAXHGLL-UHFFFAOYSA-J 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- UXHQLGLGLZKHTC-CUNXSJBXSA-N 4-[(3s,3ar)-3-cyclopentyl-7-(4-hydroxypiperidine-1-carbonyl)-3,3a,4,5-tetrahydropyrazolo[3,4-f]quinolin-2-yl]-2-chlorobenzonitrile Chemical compound C1CC(O)CCN1C(=O)C1=CC=C(C=2[C@@H]([C@H](C3CCCC3)N(N=2)C=2C=C(Cl)C(C#N)=CC=2)CC2)C2=N1 UXHQLGLGLZKHTC-CUNXSJBXSA-N 0.000 description 1
- HFGHRUCCKVYFKL-UHFFFAOYSA-N 4-ethoxy-2-piperazin-1-yl-7-pyridin-4-yl-5h-pyrimido[5,4-b]indole Chemical compound C1=C2NC=3C(OCC)=NC(N4CCNCC4)=NC=3C2=CC=C1C1=CC=NC=C1 HFGHRUCCKVYFKL-UHFFFAOYSA-N 0.000 description 1
- 239000004606 Fillers/Extenders Substances 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- BOTDANWDWHJENH-UHFFFAOYSA-N Tetraethyl orthosilicate Chemical class CCO[Si](OCC)(OCC)OCC BOTDANWDWHJENH-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000003082 abrasive agent Substances 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052910 alkali metal silicate Inorganic materials 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 239000000976 ink Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000003094 microcapsule Substances 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 239000011707 mineral Chemical class 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- DCKVFVYPWDKYDN-UHFFFAOYSA-L oxygen(2-);titanium(4+);sulfate Chemical compound [O-2].[Ti+4].[O-]S([O-])(=O)=O DCKVFVYPWDKYDN-UHFFFAOYSA-L 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 239000011163 secondary particle Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 150000003608 titanium Chemical class 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 229910000348 titanium sulfate Inorganic materials 0.000 description 1
- KMIOJWCYOHBUJS-HAKPAVFJSA-N vorolanib Chemical compound C1N(C(=O)N(C)C)CC[C@@H]1NC(=O)C1=C(C)NC(\C=C/2C3=CC(F)=CC=C3NC\2=O)=C1C KMIOJWCYOHBUJS-HAKPAVFJSA-N 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
- C01B13/14—Methods for preparing oxides or hydroxides in general
- C01B13/36—Methods for preparing oxides or hydroxides in general by precipitation reactions in aqueous solutions
- C01B13/363—Mixtures of oxides or hydroxides by precipitation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Silicon Compounds (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60011718A JPS61174103A (ja) | 1985-01-23 | 1985-01-23 | 金属酸化物からなる多孔質真球状微粒子粉末の製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60011718A JPS61174103A (ja) | 1985-01-23 | 1985-01-23 | 金属酸化物からなる多孔質真球状微粒子粉末の製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61174103A true JPS61174103A (ja) | 1986-08-05 |
| JPH0261406B2 JPH0261406B2 (enrdf_load_stackoverflow) | 1990-12-20 |
Family
ID=11785819
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60011718A Granted JPS61174103A (ja) | 1985-01-23 | 1985-01-23 | 金属酸化物からなる多孔質真球状微粒子粉末の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61174103A (enrdf_load_stackoverflow) |
Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6279841A (ja) * | 1985-10-02 | 1987-04-13 | Teikoku Kako Kk | 無機球状体の製造方法 |
| US4837011A (en) * | 1987-09-08 | 1989-06-06 | Revlon, Inc. | Cosmetic powder employing spherical silica particles |
| JPH01246130A (ja) * | 1987-11-30 | 1989-10-02 | Rhone Poulenc Chim | 酸化チタン、酸化ジルコニウムまたは酸化セリウムを主体とする顆粒の製造方法及びそれより得られる顆粒 |
| JPH02302315A (ja) * | 1989-05-15 | 1990-12-14 | Nichias Corp | 多孔質球状アルミナの製造法 |
| US5304382A (en) * | 1989-08-18 | 1994-04-19 | Monsanto Company | Ferritin analogs |
| JPH0867505A (ja) * | 1994-08-26 | 1996-03-12 | Catalysts & Chem Ind Co Ltd | 無機酸化物粒子 |
| US5998329A (en) * | 1994-06-17 | 1999-12-07 | Bio-Technical Resources | Method for making spherical adsorbent particles |
| WO2001072634A1 (fr) * | 2000-03-28 | 2001-10-04 | Pechiney Electrometallurgie | Procede de recuperation de l'energie thermique des gaz d'un four d'electrometallurgie et application a la fabrication de poudre de silice |
| US6313061B1 (en) | 1998-12-22 | 2001-11-06 | W. R. Grace & Co.-Conn. | Method of making frangible spray dried agglomerated supports and olefin polymerization catalysts supported thereon |
| EP2128880A2 (en) | 2008-05-30 | 2009-12-02 | JGC Catalysts and Chemicals Ltd. | Coating material for forming porous metal oxide semiconductor film for photovoltaic cell |
| JP2010064218A (ja) * | 2008-09-12 | 2010-03-25 | Jgc Catalysts & Chemicals Ltd | 研磨用砥石 |
| WO2011155536A1 (ja) * | 2010-06-09 | 2011-12-15 | 日揮触媒化成株式会社 | 蛋白質固定化用担体、固定化蛋白質及びそれらの製造方法 |
| JP2012106893A (ja) * | 2010-11-18 | 2012-06-07 | Jgc Catalysts & Chemicals Ltd | 貫通孔に繊維状バクテリアセルロースが貫通したマイクロリング状無機酸化物粒子 |
| JP2014240350A (ja) * | 2008-12-26 | 2014-12-25 | 日揮触媒化成株式会社 | 貫通孔を有するマイクロリング状無機酸化物粒子の製造方法 |
| KR20160148724A (ko) | 2014-06-30 | 2016-12-26 | 닛키 쇼쿠바이카세이 가부시키가이샤 | 다공질 실리카계 입자, 그 제조 방법 및 그것을 배합한 화장료 |
| CN107498059A (zh) * | 2017-08-28 | 2017-12-22 | 西北有色金属研究院 | 一种气雾化制备粒径细化钛基球形粉末的方法 |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4911814B2 (ja) * | 2000-11-22 | 2012-04-04 | 日揮触媒化成株式会社 | 球状多孔質粒子およびその製造方法 |
| JP4731053B2 (ja) * | 2001-06-28 | 2011-07-20 | 日揮触媒化成株式会社 | 樹脂被覆球状多孔質粒子、その製造方法、および該粒子を配合した化粧料 |
| EP1541115B1 (en) | 2002-07-11 | 2011-06-01 | JGC Catalysts and Chemicals Ltd. | Cosmetic |
| TWI761649B (zh) | 2017-12-27 | 2022-04-21 | 日商日揮觸媒化成股份有限公司 | 多孔二氧化矽粒子及其製造方法 |
-
1985
- 1985-01-23 JP JP60011718A patent/JPS61174103A/ja active Granted
Cited By (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6279841A (ja) * | 1985-10-02 | 1987-04-13 | Teikoku Kako Kk | 無機球状体の製造方法 |
| US4837011A (en) * | 1987-09-08 | 1989-06-06 | Revlon, Inc. | Cosmetic powder employing spherical silica particles |
| JPH01246130A (ja) * | 1987-11-30 | 1989-10-02 | Rhone Poulenc Chim | 酸化チタン、酸化ジルコニウムまたは酸化セリウムを主体とする顆粒の製造方法及びそれより得られる顆粒 |
| JPH02302315A (ja) * | 1989-05-15 | 1990-12-14 | Nichias Corp | 多孔質球状アルミナの製造法 |
| US5304382A (en) * | 1989-08-18 | 1994-04-19 | Monsanto Company | Ferritin analogs |
| US5998329A (en) * | 1994-06-17 | 1999-12-07 | Bio-Technical Resources | Method for making spherical adsorbent particles |
| US6074983A (en) * | 1994-06-17 | 2000-06-13 | Derolf; Mahlon Robert | Method for making spherical adsorbent particles |
| JPH0867505A (ja) * | 1994-08-26 | 1996-03-12 | Catalysts & Chem Ind Co Ltd | 無機酸化物粒子 |
| US6313061B1 (en) | 1998-12-22 | 2001-11-06 | W. R. Grace & Co.-Conn. | Method of making frangible spray dried agglomerated supports and olefin polymerization catalysts supported thereon |
| WO2001072634A1 (fr) * | 2000-03-28 | 2001-10-04 | Pechiney Electrometallurgie | Procede de recuperation de l'energie thermique des gaz d'un four d'electrometallurgie et application a la fabrication de poudre de silice |
| EP2128880A2 (en) | 2008-05-30 | 2009-12-02 | JGC Catalysts and Chemicals Ltd. | Coating material for forming porous metal oxide semiconductor film for photovoltaic cell |
| JP2010064218A (ja) * | 2008-09-12 | 2010-03-25 | Jgc Catalysts & Chemicals Ltd | 研磨用砥石 |
| JP2014240350A (ja) * | 2008-12-26 | 2014-12-25 | 日揮触媒化成株式会社 | 貫通孔を有するマイクロリング状無機酸化物粒子の製造方法 |
| WO2011155536A1 (ja) * | 2010-06-09 | 2011-12-15 | 日揮触媒化成株式会社 | 蛋白質固定化用担体、固定化蛋白質及びそれらの製造方法 |
| JP2012016351A (ja) * | 2010-06-09 | 2012-01-26 | Jgc Catalysts & Chemicals Ltd | 蛋白質固定化用担体、固定化蛋白質及びそれらの製造方法 |
| JP2012106893A (ja) * | 2010-11-18 | 2012-06-07 | Jgc Catalysts & Chemicals Ltd | 貫通孔に繊維状バクテリアセルロースが貫通したマイクロリング状無機酸化物粒子 |
| KR20160148724A (ko) | 2014-06-30 | 2016-12-26 | 닛키 쇼쿠바이카세이 가부시키가이샤 | 다공질 실리카계 입자, 그 제조 방법 및 그것을 배합한 화장료 |
| US9808407B2 (en) | 2014-06-30 | 2017-11-07 | Jgc Catalysts And Chemicals Ltd. | Porous silica particle, method for producing the same, and cosmetic containing the same |
| CN107498059A (zh) * | 2017-08-28 | 2017-12-22 | 西北有色金属研究院 | 一种气雾化制备粒径细化钛基球形粉末的方法 |
| CN107498059B (zh) * | 2017-08-28 | 2019-01-22 | 西北有色金属研究院 | 一种气雾化制备粒径细化钛基球形粉末的方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0261406B2 (enrdf_load_stackoverflow) | 1990-12-20 |
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