JPS61106414A - 導電性低次酸化チタン微粉末及びその製造方法 - Google Patents
導電性低次酸化チタン微粉末及びその製造方法Info
- Publication number
- JPS61106414A JPS61106414A JP14296884A JP14296884A JPS61106414A JP S61106414 A JPS61106414 A JP S61106414A JP 14296884 A JP14296884 A JP 14296884A JP 14296884 A JP14296884 A JP 14296884A JP S61106414 A JPS61106414 A JP S61106414A
- Authority
- JP
- Japan
- Prior art keywords
- titanium oxide
- fine powder
- powder
- fine
- titanium dioxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 title claims abstract description 101
- 239000000843 powder Substances 0.000 title claims abstract description 34
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 title claims abstract description 32
- 230000003647 oxidation Effects 0.000 title claims abstract description 12
- 238000007254 oxidation reaction Methods 0.000 title claims abstract description 12
- 239000002245 particle Substances 0.000 claims abstract description 24
- 239000010936 titanium Substances 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims abstract description 14
- 229910003087 TiOx Inorganic materials 0.000 claims abstract description 7
- 238000001354 calcination Methods 0.000 claims abstract description 7
- HLLICFJUWSZHRJ-UHFFFAOYSA-N tioxidazole Chemical compound CCCOC1=CC=C2N=C(NC(=O)OC)SC2=C1 HLLICFJUWSZHRJ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004408 titanium dioxide Substances 0.000 claims description 33
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 18
- 229910052719 titanium Inorganic materials 0.000 claims description 12
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 abstract description 13
- 238000002156 mixing Methods 0.000 abstract description 8
- 239000000463 material Substances 0.000 abstract description 5
- 238000000576 coating method Methods 0.000 abstract description 4
- 239000011248 coating agent Substances 0.000 abstract description 3
- 229910052782 aluminium Inorganic materials 0.000 abstract description 2
- 239000011261 inert gas Substances 0.000 abstract description 2
- 229910052758 niobium Inorganic materials 0.000 abstract description 2
- 229910052721 tungsten Inorganic materials 0.000 abstract description 2
- 239000000654 additive Substances 0.000 abstract 3
- 230000000996 additive effect Effects 0.000 abstract 3
- 238000004040 coloring Methods 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 description 14
- 239000010419 fine particle Substances 0.000 description 9
- 239000004115 Sodium Silicate Substances 0.000 description 7
- 229910052751 metal Inorganic materials 0.000 description 7
- 239000002184 metal Substances 0.000 description 7
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 7
- 229910052911 sodium silicate Inorganic materials 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
- 239000012752 auxiliary agent Substances 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 5
- 238000006722 reduction reaction Methods 0.000 description 5
- 239000002002 slurry Substances 0.000 description 5
- 239000006229 carbon black Substances 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 238000010304 firing Methods 0.000 description 4
- 238000005245 sintering Methods 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 230000003301 hydrolyzing effect Effects 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- -1 titanium oxide compound Chemical class 0.000 description 3
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 239000003929 acidic solution Substances 0.000 description 2
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 2
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 2
- 239000002216 antistatic agent Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 229910052681 coesite Inorganic materials 0.000 description 2
- 229910052906 cristobalite Inorganic materials 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000011859 microparticle Substances 0.000 description 2
- 230000003472 neutralizing effect Effects 0.000 description 2
- ZKATWMILCYLAPD-UHFFFAOYSA-N niobium pentoxide Chemical compound O=[Nb](=O)O[Nb](=O)=O ZKATWMILCYLAPD-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000000049 pigment Substances 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 150000003377 silicon compounds Chemical class 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- 235000012239 silicon dioxide Nutrition 0.000 description 2
- 229910052682 stishovite Inorganic materials 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910000349 titanium oxysulfate Inorganic materials 0.000 description 2
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 2
- 229910052905 tridymite Inorganic materials 0.000 description 2
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 description 1
- IOHGCXDWUOZSRD-UHFFFAOYSA-N Cl.Cl.Cl.Cl.[Ti] Chemical compound Cl.Cl.Cl.Cl.[Ti] IOHGCXDWUOZSRD-UHFFFAOYSA-N 0.000 description 1
- 229910019704 Nb2O Inorganic materials 0.000 description 1
- 239000006057 Non-nutritive feed additive Substances 0.000 description 1
- 239000004614 Process Aid Substances 0.000 description 1
- 239000006087 Silane Coupling Agent Substances 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- CZSABVBCTRZESY-UHFFFAOYSA-N [O-2].[O-2].[Ti+4].OS(O)(=O)=O Chemical compound [O-2].[O-2].[Ti+4].OS(O)(=O)=O CZSABVBCTRZESY-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- IJKVHSBPTUYDLN-UHFFFAOYSA-N dihydroxy(oxo)silane Chemical compound O[Si](O)=O IJKVHSBPTUYDLN-UHFFFAOYSA-N 0.000 description 1
- 239000004205 dimethyl polysiloxane Substances 0.000 description 1
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 239000000976 ink Substances 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 150000002821 niobium Chemical class 0.000 description 1
- 239000010955 niobium Substances 0.000 description 1
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 1
- 150000002822 niobium compounds Chemical class 0.000 description 1
- 229910000484 niobium oxide Inorganic materials 0.000 description 1
- URLJKFSTXLNXLG-UHFFFAOYSA-N niobium(5+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Nb+5].[Nb+5] URLJKFSTXLNXLG-UHFFFAOYSA-N 0.000 description 1
- WPCMRGJTLPITMF-UHFFFAOYSA-I niobium(5+);pentahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[Nb+5] WPCMRGJTLPITMF-UHFFFAOYSA-I 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- DCKVFVYPWDKYDN-UHFFFAOYSA-L oxygen(2-);titanium(4+);sulfate Chemical compound [O-2].[Ti+4].[O-]S([O-])(=O)=O DCKVFVYPWDKYDN-UHFFFAOYSA-L 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000003608 titanium Chemical class 0.000 description 1
- 150000003609 titanium compounds Chemical class 0.000 description 1
- 229910000348 titanium sulfate Inorganic materials 0.000 description 1
- HDUMBHAAKGUHAR-UHFFFAOYSA-J titanium(4+);disulfate Chemical class [Ti+4].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O HDUMBHAAKGUHAR-UHFFFAOYSA-J 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 150000003658 tungsten compounds Chemical class 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
- Conductive Materials (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14296884A JPS61106414A (ja) | 1984-07-10 | 1984-07-10 | 導電性低次酸化チタン微粉末及びその製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14296884A JPS61106414A (ja) | 1984-07-10 | 1984-07-10 | 導電性低次酸化チタン微粉末及びその製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61106414A true JPS61106414A (ja) | 1986-05-24 |
| JPS6411572B2 JPS6411572B2 (enrdf_load_stackoverflow) | 1989-02-27 |
Family
ID=15327840
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP14296884A Granted JPS61106414A (ja) | 1984-07-10 | 1984-07-10 | 導電性低次酸化チタン微粉末及びその製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61106414A (enrdf_load_stackoverflow) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6317221A (ja) * | 1986-07-03 | 1988-01-25 | Taki Chem Co Ltd | 結晶質酸化チタンゾル及びその製造方法 |
| JPH0292824A (ja) * | 1988-09-30 | 1990-04-03 | Ishihara Sangyo Kaisha Ltd | 針状低次酸化チタン及びその製造方法 |
| US5173215A (en) * | 1991-02-21 | 1992-12-22 | Atraverda Limited | Conductive titanium suboxide particulates |
| US5320782A (en) * | 1990-10-19 | 1994-06-14 | Ishihara Sangyo Kaisha, Ltd. | Acicular or platy titanium suboxides and process for producing same |
| EP0707050A3 (en) * | 1994-10-11 | 1996-06-12 | Shiseido Co Ltd | Pigment containing a titanium suboxide and process for its preparation |
| US5582773A (en) * | 1987-01-23 | 1996-12-10 | Cass; Richard B. | Electrically-conductive titanium suboxides |
| US6524750B1 (en) | 2000-06-17 | 2003-02-25 | Eveready Battery Company, Inc. | Doped titanium oxide additives |
| WO2018159420A1 (ja) * | 2017-03-01 | 2018-09-07 | 堺化学工業株式会社 | 導電性材料及び電極材料 |
| JP2018177553A (ja) * | 2017-04-04 | 2018-11-15 | 東京印刷機材トレーディング株式会社 | 亜酸化チタン粒子を製造する方法及び亜酸化チタン粒子 |
| WO2022039111A1 (ja) * | 2020-08-21 | 2022-02-24 | デンカ株式会社 | 特定の低次酸化チタンの結晶組成を有する粒子、並びにその製造方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5891037A (ja) * | 1981-11-27 | 1983-05-30 | Mitsubishi Metal Corp | 酸化チタン粉末の製造法 |
-
1984
- 1984-07-10 JP JP14296884A patent/JPS61106414A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5891037A (ja) * | 1981-11-27 | 1983-05-30 | Mitsubishi Metal Corp | 酸化チタン粉末の製造法 |
Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6317221A (ja) * | 1986-07-03 | 1988-01-25 | Taki Chem Co Ltd | 結晶質酸化チタンゾル及びその製造方法 |
| US5582773A (en) * | 1987-01-23 | 1996-12-10 | Cass; Richard B. | Electrically-conductive titanium suboxides |
| US5585041A (en) * | 1987-01-23 | 1996-12-17 | Cass; Richard B. | Electrically-conductive titanium suboxides |
| JPH0292824A (ja) * | 1988-09-30 | 1990-04-03 | Ishihara Sangyo Kaisha Ltd | 針状低次酸化チタン及びその製造方法 |
| US5320782A (en) * | 1990-10-19 | 1994-06-14 | Ishihara Sangyo Kaisha, Ltd. | Acicular or platy titanium suboxides and process for producing same |
| US5173215A (en) * | 1991-02-21 | 1992-12-22 | Atraverda Limited | Conductive titanium suboxide particulates |
| US5281496A (en) * | 1991-02-21 | 1994-01-25 | Atraverda Limited | Electrochemical cell containing a titanium suboxide electrode |
| EP0707050A3 (en) * | 1994-10-11 | 1996-06-12 | Shiseido Co Ltd | Pigment containing a titanium suboxide and process for its preparation |
| US6524750B1 (en) | 2000-06-17 | 2003-02-25 | Eveready Battery Company, Inc. | Doped titanium oxide additives |
| WO2018159420A1 (ja) * | 2017-03-01 | 2018-09-07 | 堺化学工業株式会社 | 導電性材料及び電極材料 |
| JP2018147569A (ja) * | 2017-03-01 | 2018-09-20 | 堺化学工業株式会社 | 導電性材料及び電極材料 |
| US11094944B2 (en) | 2017-03-01 | 2021-08-17 | Sakai Chemical Industry Co., Ltd. | Electrically conductive material and electrode material |
| JP2018177553A (ja) * | 2017-04-04 | 2018-11-15 | 東京印刷機材トレーディング株式会社 | 亜酸化チタン粒子を製造する方法及び亜酸化チタン粒子 |
| WO2022039111A1 (ja) * | 2020-08-21 | 2022-02-24 | デンカ株式会社 | 特定の低次酸化チタンの結晶組成を有する粒子、並びにその製造方法 |
| JPWO2022039111A1 (enrdf_load_stackoverflow) * | 2020-08-21 | 2022-02-24 | ||
| CN115835912A (zh) * | 2020-08-21 | 2023-03-21 | 电化株式会社 | 具有特定的低价氧化钛的晶体组成的粒子及其制造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6411572B2 (enrdf_load_stackoverflow) | 1989-02-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |